Physico-chemical, Thermal and Tensile Properties of Alkali-treated Acacia Concinna Fiber

The fundamental properties (diameter, density, chemical composition, crystalline nature, thermal behaviors, tensile properties and Surface topography) of the raw and alkalized Acacia Concinna fiber (ACF) were investigated in this article with the intension verify the fitness of Acacia Concinna fiber...

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Main Authors: Amutha Venugopal, Senthil Kumar Boominathan
Format: Article
Language:English
Published: Taylor & Francis Group 2022-08-01
Series:Journal of Natural Fibers
Subjects:
Online Access:http://dx.doi.org/10.1080/15440478.2020.1838998
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author Amutha Venugopal
Senthil Kumar Boominathan
author_facet Amutha Venugopal
Senthil Kumar Boominathan
author_sort Amutha Venugopal
collection DOAJ
description The fundamental properties (diameter, density, chemical composition, crystalline nature, thermal behaviors, tensile properties and Surface topography) of the raw and alkalized Acacia Concinna fiber (ACF) were investigated in this article with the intension verify the fitness of Acacia Concinna fiber as reinforcement in green composites. Outcomes of the chemical analysis established that 5% (w/v) NaoH with 45 min treatment time was produced the optimistic transform in the chemical composition than other treatment timings (15, 30,60,75 min). The diminution in the lignin and hemi-cellulose content of the alkalized ACF was established through the Fourier-transform infrared (FTIR) and Nuclear magnetic resonance (NMR) spectrograms. Improvements in the crystallographic parameters (Crystallinity index (27.5% to 35.6%) and crystalline size (4.17 nm to 6.43 nm) of optimally alkalized ACF were demonstrated through the X-Ray diffraction (XRD) analysis. The mass degradation pattern (TG and DTG profile) of the untreated and optimally alkalized ACF were generated with the help of a thermal analyzer. Scanning electron microscope and atomic force microscope were used to record the impact of alkalization in surface topography of the ACF.
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spelling doaj.art-389ab64653d04fb3ab431a9b938e59ee2023-09-20T13:04:25ZengTaylor & Francis GroupJournal of Natural Fibers1544-04781544-046X2022-08-011983093310810.1080/15440478.2020.18389981838998Physico-chemical, Thermal and Tensile Properties of Alkali-treated Acacia Concinna FiberAmutha Venugopal0Senthil Kumar Boominathan1R.V.S College of EngineeringThe Gandhigram Rural Institute, (Deemed to Be University)The fundamental properties (diameter, density, chemical composition, crystalline nature, thermal behaviors, tensile properties and Surface topography) of the raw and alkalized Acacia Concinna fiber (ACF) were investigated in this article with the intension verify the fitness of Acacia Concinna fiber as reinforcement in green composites. Outcomes of the chemical analysis established that 5% (w/v) NaoH with 45 min treatment time was produced the optimistic transform in the chemical composition than other treatment timings (15, 30,60,75 min). The diminution in the lignin and hemi-cellulose content of the alkalized ACF was established through the Fourier-transform infrared (FTIR) and Nuclear magnetic resonance (NMR) spectrograms. Improvements in the crystallographic parameters (Crystallinity index (27.5% to 35.6%) and crystalline size (4.17 nm to 6.43 nm) of optimally alkalized ACF were demonstrated through the X-Ray diffraction (XRD) analysis. The mass degradation pattern (TG and DTG profile) of the untreated and optimally alkalized ACF were generated with the help of a thermal analyzer. Scanning electron microscope and atomic force microscope were used to record the impact of alkalization in surface topography of the ACF.http://dx.doi.org/10.1080/15440478.2020.1838998acacia concinna fiberalkalizationnuclear magnetic resonance spectroscopytensile strengthsurface roughnessedx analysis
spellingShingle Amutha Venugopal
Senthil Kumar Boominathan
Physico-chemical, Thermal and Tensile Properties of Alkali-treated Acacia Concinna Fiber
Journal of Natural Fibers
acacia concinna fiber
alkalization
nuclear magnetic resonance spectroscopy
tensile strength
surface roughness
edx analysis
title Physico-chemical, Thermal and Tensile Properties of Alkali-treated Acacia Concinna Fiber
title_full Physico-chemical, Thermal and Tensile Properties of Alkali-treated Acacia Concinna Fiber
title_fullStr Physico-chemical, Thermal and Tensile Properties of Alkali-treated Acacia Concinna Fiber
title_full_unstemmed Physico-chemical, Thermal and Tensile Properties of Alkali-treated Acacia Concinna Fiber
title_short Physico-chemical, Thermal and Tensile Properties of Alkali-treated Acacia Concinna Fiber
title_sort physico chemical thermal and tensile properties of alkali treated acacia concinna fiber
topic acacia concinna fiber
alkalization
nuclear magnetic resonance spectroscopy
tensile strength
surface roughness
edx analysis
url http://dx.doi.org/10.1080/15440478.2020.1838998
work_keys_str_mv AT amuthavenugopal physicochemicalthermalandtensilepropertiesofalkalitreatedacaciaconcinnafiber
AT senthilkumarboominathan physicochemicalthermalandtensilepropertiesofalkalitreatedacaciaconcinnafiber