Thermal and Modern, Non-Thermal Method Induction as a Factor of Modification of Inulin Hydrogel Properties

The aim of the study was to compare the properties of inulin hydrogels obtained with different methods, e.g., the traditional–thermal method and new, non-thermal methods, used in food production, like ultrasonic, high-pressure homogenization (HPH), and high hydrostatic pressures (HHPs). It was found...

Full description

Bibliographic Details
Main Authors: Anna Florowska, Tomasz Florowski, Bartosz Kruszewski, Emilia Janiszewska-Turak, Weronika Bykowska, Nour Ksibi
Format: Article
Language:English
Published: MDPI AG 2023-11-01
Series:Foods
Subjects:
Online Access:https://www.mdpi.com/2304-8158/12/22/4154
_version_ 1827639837662904320
author Anna Florowska
Tomasz Florowski
Bartosz Kruszewski
Emilia Janiszewska-Turak
Weronika Bykowska
Nour Ksibi
author_facet Anna Florowska
Tomasz Florowski
Bartosz Kruszewski
Emilia Janiszewska-Turak
Weronika Bykowska
Nour Ksibi
author_sort Anna Florowska
collection DOAJ
description The aim of the study was to compare the properties of inulin hydrogels obtained with different methods, e.g., the traditional–thermal method and new, non-thermal methods, used in food production, like ultrasonic, high-pressure homogenization (HPH), and high hydrostatic pressures (HHPs). It was found that each of the compared induction methods allowed for obtaining inulin hydrogels. However, the use of non-thermal induction methods allows for obtaining a gel structure faster than in the case of thermal induction. In addition, hydrogels obtained with new, non-thermal methods differ from gels obtained with thermal treatment. They were characterized by higher stability (from 1.7 percent point-of-stability parameters for HHP 150 MPa to 18.8 for HPH II cycles) and in most cases, by improved microrheological properties–lower solid–liquid balance toward the solid phase, increased elasticity and viscosity indexes, and lowering the flow index. The gels obtained with the new, non-thermal method were also characterized by a more delicate structure, including lower firmness (the differences between thermal and non-thermal inductions were from 0.73 N for HHP at 500 MPa to 2.39 N for HHP at 150 MPa) and spreadability (the differences between thermal and non-thermal inductions were from 7.60 Ns for HHP at 500 MPa to 15.08 Ns for HHP at 150 MPa). The color of ultrasound-induced inulin gels, regarding the HPH and HHP technique, was darker (the differences in the L* parameter between thermal and non-thermal inductions were from 1.92 for HHP at 500 MPa to 4.37 for 10 min ultrasounds) and with a lower a* color parameter (the differences in the a* parameter between thermal and non-thermal inductions were from 0.16 for HHP at 500 MPa to 0.39 for HPH II cycles) and b* color parameter (the differences in the b* parameter between thermal and non-thermal inductions were from 1.69 for 5 min ultrasounds to 2.68 for HPH II cycles). It was also found that among the compared induction methods, the high-pressure technique has the greatest potential for modifying the properties of the created inulin hydrogels. Thanks to its application, depending on the amount of applied pressure, it was possible to obtain gels with very different characteristics, both delicate (i.e., soft and spreadable), using HHP at 150 MPa, and hard, using HHP at 500 MPa, the closest in characteristics to gels induced with the thermal method. This may allow the properties of hydrogels to be matched to the characteristics of the food matrix being created.
first_indexed 2024-03-09T16:49:40Z
format Article
id doaj.art-392e4ff2ad224e46b6cc413fde872069
institution Directory Open Access Journal
issn 2304-8158
language English
last_indexed 2024-03-09T16:49:40Z
publishDate 2023-11-01
publisher MDPI AG
record_format Article
series Foods
spelling doaj.art-392e4ff2ad224e46b6cc413fde8720692023-11-24T14:42:14ZengMDPI AGFoods2304-81582023-11-011222415410.3390/foods12224154Thermal and Modern, Non-Thermal Method Induction as a Factor of Modification of Inulin Hydrogel PropertiesAnna Florowska0Tomasz Florowski1Bartosz Kruszewski2Emilia Janiszewska-Turak3Weronika Bykowska4Nour Ksibi5Department of Food Technology and Assessment, Institute of Food Sciences, Warsaw University of Life Sciences-SGGW, 159c Nowoursynowska Street, 02-787 Warsaw, PolandDepartment of Food Technology and Assessment, Institute of Food Sciences, Warsaw University of Life Sciences-SGGW, 159c Nowoursynowska Street, 02-787 Warsaw, PolandDepartment of Food Technology and Assessment, Institute of Food Sciences, Warsaw University of Life Sciences-SGGW, 159c Nowoursynowska Street, 02-787 Warsaw, PolandDepartment of Food Engineering and Process Management, Institute of Food Sciences, Warsaw University of Life Sciences-SGGW, 159c Nowoursynowska Street, 02-787 Warsaw, PolandDepartment of Food Technology and Assessment, Institute of Food Sciences, Warsaw University of Life Sciences-SGGW, 159c Nowoursynowska Street, 02-787 Warsaw, PolandFaculty of Sciences of Tunis, Tunis El Manar University, El Manar Tunis 2092, TunisiaThe aim of the study was to compare the properties of inulin hydrogels obtained with different methods, e.g., the traditional–thermal method and new, non-thermal methods, used in food production, like ultrasonic, high-pressure homogenization (HPH), and high hydrostatic pressures (HHPs). It was found that each of the compared induction methods allowed for obtaining inulin hydrogels. However, the use of non-thermal induction methods allows for obtaining a gel structure faster than in the case of thermal induction. In addition, hydrogels obtained with new, non-thermal methods differ from gels obtained with thermal treatment. They were characterized by higher stability (from 1.7 percent point-of-stability parameters for HHP 150 MPa to 18.8 for HPH II cycles) and in most cases, by improved microrheological properties–lower solid–liquid balance toward the solid phase, increased elasticity and viscosity indexes, and lowering the flow index. The gels obtained with the new, non-thermal method were also characterized by a more delicate structure, including lower firmness (the differences between thermal and non-thermal inductions were from 0.73 N for HHP at 500 MPa to 2.39 N for HHP at 150 MPa) and spreadability (the differences between thermal and non-thermal inductions were from 7.60 Ns for HHP at 500 MPa to 15.08 Ns for HHP at 150 MPa). The color of ultrasound-induced inulin gels, regarding the HPH and HHP technique, was darker (the differences in the L* parameter between thermal and non-thermal inductions were from 1.92 for HHP at 500 MPa to 4.37 for 10 min ultrasounds) and with a lower a* color parameter (the differences in the a* parameter between thermal and non-thermal inductions were from 0.16 for HHP at 500 MPa to 0.39 for HPH II cycles) and b* color parameter (the differences in the b* parameter between thermal and non-thermal inductions were from 1.69 for 5 min ultrasounds to 2.68 for HPH II cycles). It was also found that among the compared induction methods, the high-pressure technique has the greatest potential for modifying the properties of the created inulin hydrogels. Thanks to its application, depending on the amount of applied pressure, it was possible to obtain gels with very different characteristics, both delicate (i.e., soft and spreadable), using HHP at 150 MPa, and hard, using HHP at 500 MPa, the closest in characteristics to gels induced with the thermal method. This may allow the properties of hydrogels to be matched to the characteristics of the food matrix being created.https://www.mdpi.com/2304-8158/12/22/4154inulin hydrogelultrasoundsHPHHHP
spellingShingle Anna Florowska
Tomasz Florowski
Bartosz Kruszewski
Emilia Janiszewska-Turak
Weronika Bykowska
Nour Ksibi
Thermal and Modern, Non-Thermal Method Induction as a Factor of Modification of Inulin Hydrogel Properties
Foods
inulin hydrogel
ultrasounds
HPH
HHP
title Thermal and Modern, Non-Thermal Method Induction as a Factor of Modification of Inulin Hydrogel Properties
title_full Thermal and Modern, Non-Thermal Method Induction as a Factor of Modification of Inulin Hydrogel Properties
title_fullStr Thermal and Modern, Non-Thermal Method Induction as a Factor of Modification of Inulin Hydrogel Properties
title_full_unstemmed Thermal and Modern, Non-Thermal Method Induction as a Factor of Modification of Inulin Hydrogel Properties
title_short Thermal and Modern, Non-Thermal Method Induction as a Factor of Modification of Inulin Hydrogel Properties
title_sort thermal and modern non thermal method induction as a factor of modification of inulin hydrogel properties
topic inulin hydrogel
ultrasounds
HPH
HHP
url https://www.mdpi.com/2304-8158/12/22/4154
work_keys_str_mv AT annaflorowska thermalandmodernnonthermalmethodinductionasafactorofmodificationofinulinhydrogelproperties
AT tomaszflorowski thermalandmodernnonthermalmethodinductionasafactorofmodificationofinulinhydrogelproperties
AT bartoszkruszewski thermalandmodernnonthermalmethodinductionasafactorofmodificationofinulinhydrogelproperties
AT emiliajaniszewskaturak thermalandmodernnonthermalmethodinductionasafactorofmodificationofinulinhydrogelproperties
AT weronikabykowska thermalandmodernnonthermalmethodinductionasafactorofmodificationofinulinhydrogelproperties
AT nourksibi thermalandmodernnonthermalmethodinductionasafactorofmodificationofinulinhydrogelproperties