Thermal Annealing and Phase Transformation of Serpentine-Like Garnierite

This study is focused on the vibrational and microstructural aspects of the thermally induced transformation of serpentine-like garnierite into quartz, forsterite, and enstatite occurring at about 620 °C. Powder specimens of garnierite were annealed in static air between room temperature and 1000 °C...

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Bibliographic Details
Main Authors: Arun Kumar, Michele Cassetta, Marco Giarola, Marco Zanatta, Monique Le Guen, Gian Domenico Soraru, Gino Mariotto
Format: Article
Language:English
Published: MDPI AG 2021-02-01
Series:Minerals
Subjects:
Online Access:https://www.mdpi.com/2075-163X/11/2/188
Description
Summary:This study is focused on the vibrational and microstructural aspects of the thermally induced transformation of serpentine-like garnierite into quartz, forsterite, and enstatite occurring at about 620 °C. Powder specimens of garnierite were annealed in static air between room temperature and 1000 °C. The kinetic of the transformation was investigated by means of thermogravimetric and differential thermal analysis, and the final product was extensively characterized via micro-Raman spectroscopy and X-ray diffraction. Our study shows that serpentine-like garnierite consists of a mixture of different mineral species. Furthermore, these garnierites and their composition can provide details based on the mineralogy and the crystalline phases resulting from the thermal treatment.
ISSN:2075-163X