Fabrication, Characterization and Photocatalytic Activity of Copper Oxide Nanowires Formed by Anodization of Copper Foams

In recent paper anodization of copper foams in 0.1 M K<sub>2</sub>CO<sub>3</sub> is reported. Anodization was performed in the voltage range of 5–25 V and in all the cases oxides with a developed surface area were obtained. However, anodizing only at 20 and 25 V resulted in t...

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Main Authors: Alaa M. Abd-Elnaiem, Moustafa A. Abdel-Rahim, Atta Y. Abdel-Latief, Ahmed Abdel-Rahim Mohamed, Kristina Mojsilović, Wojciech Jerzy Stępniowski
Format: Article
Language:English
Published: MDPI AG 2021-09-01
Series:Materials
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Online Access:https://www.mdpi.com/1996-1944/14/17/5030
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author Alaa M. Abd-Elnaiem
Moustafa A. Abdel-Rahim
Atta Y. Abdel-Latief
Ahmed Abdel-Rahim Mohamed
Kristina Mojsilović
Wojciech Jerzy Stępniowski
author_facet Alaa M. Abd-Elnaiem
Moustafa A. Abdel-Rahim
Atta Y. Abdel-Latief
Ahmed Abdel-Rahim Mohamed
Kristina Mojsilović
Wojciech Jerzy Stępniowski
author_sort Alaa M. Abd-Elnaiem
collection DOAJ
description In recent paper anodization of copper foams in 0.1 M K<sub>2</sub>CO<sub>3</sub> is reported. Anodization was performed in the voltage range of 5–25 V and in all the cases oxides with a developed surface area were obtained. However, anodizing only at 20 and 25 V resulted in the formation of nanostruc-tures. In all the cases, the products of anodizing consisted of crystalline phases like cuprite (Cu<sub>2</sub>O), tenorite (CuO), parameconite (Cu<sub>4</sub>O<sub>3</sub>) as well as spertiniite (Cu(OH)<sub>2</sub>). Copper foams after ano-dizing were applied as catalysts in the photocatalytic decolorization of a model organic compound such as methylene blue. The highest photocatalytic activity was observed for samples anodized at 25 V and closely followed by samples anodized at 5 V. The anodized copper foams proved to be a useful material in enhancing the photocatalytic efficiency of organic dye decomposition.
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spelling doaj.art-3a469993240c4eb09cd1f370d3343aa52023-11-22T10:55:14ZengMDPI AGMaterials1996-19442021-09-011417503010.3390/ma14175030Fabrication, Characterization and Photocatalytic Activity of Copper Oxide Nanowires Formed by Anodization of Copper FoamsAlaa M. Abd-Elnaiem0Moustafa A. Abdel-Rahim1Atta Y. Abdel-Latief2Ahmed Abdel-Rahim Mohamed3Kristina Mojsilović4Wojciech Jerzy Stępniowski5Physics Department, Faculty of Science, Assiut University, Assiut 71516, EgyptPhysics Department, Faculty of Science, Assiut University, Assiut 71516, EgyptPhysics Department, Faculty of Science, Assiut University, Assiut 71516, EgyptPhysics Department, Faculty of Science, Assiut University, Assiut 71516, EgyptFaculty of Physics, University of Belgrade, Studentski trg 12–16, 11000 Belgrade, SerbiaFaculty of Advanced Technology and Chemistry, Institute of Materials Science & Engineering, Military University of Technology, Kaliskiego 2 Str., 00908 Warszawa, PolandIn recent paper anodization of copper foams in 0.1 M K<sub>2</sub>CO<sub>3</sub> is reported. Anodization was performed in the voltage range of 5–25 V and in all the cases oxides with a developed surface area were obtained. However, anodizing only at 20 and 25 V resulted in the formation of nanostruc-tures. In all the cases, the products of anodizing consisted of crystalline phases like cuprite (Cu<sub>2</sub>O), tenorite (CuO), parameconite (Cu<sub>4</sub>O<sub>3</sub>) as well as spertiniite (Cu(OH)<sub>2</sub>). Copper foams after ano-dizing were applied as catalysts in the photocatalytic decolorization of a model organic compound such as methylene blue. The highest photocatalytic activity was observed for samples anodized at 25 V and closely followed by samples anodized at 5 V. The anodized copper foams proved to be a useful material in enhancing the photocatalytic efficiency of organic dye decomposition.https://www.mdpi.com/1996-1944/14/17/5030copper oxidesanodizationnanowiresFTIRphotocatalytic decolorizationnanostructures
spellingShingle Alaa M. Abd-Elnaiem
Moustafa A. Abdel-Rahim
Atta Y. Abdel-Latief
Ahmed Abdel-Rahim Mohamed
Kristina Mojsilović
Wojciech Jerzy Stępniowski
Fabrication, Characterization and Photocatalytic Activity of Copper Oxide Nanowires Formed by Anodization of Copper Foams
Materials
copper oxides
anodization
nanowires
FTIR
photocatalytic decolorization
nanostructures
title Fabrication, Characterization and Photocatalytic Activity of Copper Oxide Nanowires Formed by Anodization of Copper Foams
title_full Fabrication, Characterization and Photocatalytic Activity of Copper Oxide Nanowires Formed by Anodization of Copper Foams
title_fullStr Fabrication, Characterization and Photocatalytic Activity of Copper Oxide Nanowires Formed by Anodization of Copper Foams
title_full_unstemmed Fabrication, Characterization and Photocatalytic Activity of Copper Oxide Nanowires Formed by Anodization of Copper Foams
title_short Fabrication, Characterization and Photocatalytic Activity of Copper Oxide Nanowires Formed by Anodization of Copper Foams
title_sort fabrication characterization and photocatalytic activity of copper oxide nanowires formed by anodization of copper foams
topic copper oxides
anodization
nanowires
FTIR
photocatalytic decolorization
nanostructures
url https://www.mdpi.com/1996-1944/14/17/5030
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AT moustafaaabdelrahim fabricationcharacterizationandphotocatalyticactivityofcopperoxidenanowiresformedbyanodizationofcopperfoams
AT attayabdellatief fabricationcharacterizationandphotocatalyticactivityofcopperoxidenanowiresformedbyanodizationofcopperfoams
AT ahmedabdelrahimmohamed fabricationcharacterizationandphotocatalyticactivityofcopperoxidenanowiresformedbyanodizationofcopperfoams
AT kristinamojsilovic fabricationcharacterizationandphotocatalyticactivityofcopperoxidenanowiresformedbyanodizationofcopperfoams
AT wojciechjerzystepniowski fabricationcharacterizationandphotocatalyticactivityofcopperoxidenanowiresformedbyanodizationofcopperfoams