Evolution of Microstructure, Mechanical Properties, and Corrosion Resistance of Mg–2.2Gd–2.2Zn–0.2Ca (wt%) Alloy by Extrusion at Various Temperatures

The current investigation involved casting the Mg–2.2Gd–2.2Zn–0.2Ca (wt%) alloy (GZX220) through permanent mold casting, followed by homogenization at 400 °C for 24 h and extrusion at 250 °C, 300 °C, 350 °C, and 400 °C. Microstructure investigations revealed that α-Mg, Mg–Gd, and Mg–Gd–Zn intermetal...

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Main Authors: Hüseyin Zengin, Soner Ari, Muhammet Emre Turan, Achim Walter Hassel
Format: Article
Language:English
Published: MDPI AG 2023-04-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/8/3075
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author Hüseyin Zengin
Soner Ari
Muhammet Emre Turan
Achim Walter Hassel
author_facet Hüseyin Zengin
Soner Ari
Muhammet Emre Turan
Achim Walter Hassel
author_sort Hüseyin Zengin
collection DOAJ
description The current investigation involved casting the Mg–2.2Gd–2.2Zn–0.2Ca (wt%) alloy (GZX220) through permanent mold casting, followed by homogenization at 400 °C for 24 h and extrusion at 250 °C, 300 °C, 350 °C, and 400 °C. Microstructure investigations revealed that α-Mg, Mg–Gd, and Mg–Gd–Zn intermetallic phases were present in the as-cast alloy. Following the homogenization treatment, a majority of these intermetallic particles underwent partial dissolution into the matrix phase. α-Mg grains exhibited a considerable refinement by extrusion due to dynamic recrystallization (DRX). At low extrusion temperatures, higher basal texture intensities were observed. The mechanical properties were remarkably enhanced after the extrusion process. However, a consistent decline in strength was observed with the rise in extrusion temperature. The corrosion performance of the as-cast GZX220 alloy was reduced by homogenization because of the lack of corrosion barrier effect of secondary phases. A significant enhancement of corrosion resistance was achieved by the extrusion process.
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spelling doaj.art-3a4864420840429880675d7f8dbc6f382023-11-17T20:12:44ZengMDPI AGMaterials1996-19442023-04-01168307510.3390/ma16083075Evolution of Microstructure, Mechanical Properties, and Corrosion Resistance of Mg–2.2Gd–2.2Zn–0.2Ca (wt%) Alloy by Extrusion at Various TemperaturesHüseyin Zengin0Soner Ari1Muhammet Emre Turan2Achim Walter Hassel3Institute of Chemical Technology of Inorganic Materials (TIM), Johannes Kepler University Linz, 4040 Linz, AustriaValfsel Armatür Sanayi A.S., 45030 Manisa, TürkiyeIron & Steel Institute, Karabuk University, 78100 Karabük, TürkiyeInstitute of Chemical Technology of Inorganic Materials (TIM), Johannes Kepler University Linz, 4040 Linz, AustriaThe current investigation involved casting the Mg–2.2Gd–2.2Zn–0.2Ca (wt%) alloy (GZX220) through permanent mold casting, followed by homogenization at 400 °C for 24 h and extrusion at 250 °C, 300 °C, 350 °C, and 400 °C. Microstructure investigations revealed that α-Mg, Mg–Gd, and Mg–Gd–Zn intermetallic phases were present in the as-cast alloy. Following the homogenization treatment, a majority of these intermetallic particles underwent partial dissolution into the matrix phase. α-Mg grains exhibited a considerable refinement by extrusion due to dynamic recrystallization (DRX). At low extrusion temperatures, higher basal texture intensities were observed. The mechanical properties were remarkably enhanced after the extrusion process. However, a consistent decline in strength was observed with the rise in extrusion temperature. The corrosion performance of the as-cast GZX220 alloy was reduced by homogenization because of the lack of corrosion barrier effect of secondary phases. A significant enhancement of corrosion resistance was achieved by the extrusion process.https://www.mdpi.com/1996-1944/16/8/3075magnesiumhomogenizationextrusiondynamic recrystallizationtensile propertiescorrosion
spellingShingle Hüseyin Zengin
Soner Ari
Muhammet Emre Turan
Achim Walter Hassel
Evolution of Microstructure, Mechanical Properties, and Corrosion Resistance of Mg–2.2Gd–2.2Zn–0.2Ca (wt%) Alloy by Extrusion at Various Temperatures
Materials
magnesium
homogenization
extrusion
dynamic recrystallization
tensile properties
corrosion
title Evolution of Microstructure, Mechanical Properties, and Corrosion Resistance of Mg–2.2Gd–2.2Zn–0.2Ca (wt%) Alloy by Extrusion at Various Temperatures
title_full Evolution of Microstructure, Mechanical Properties, and Corrosion Resistance of Mg–2.2Gd–2.2Zn–0.2Ca (wt%) Alloy by Extrusion at Various Temperatures
title_fullStr Evolution of Microstructure, Mechanical Properties, and Corrosion Resistance of Mg–2.2Gd–2.2Zn–0.2Ca (wt%) Alloy by Extrusion at Various Temperatures
title_full_unstemmed Evolution of Microstructure, Mechanical Properties, and Corrosion Resistance of Mg–2.2Gd–2.2Zn–0.2Ca (wt%) Alloy by Extrusion at Various Temperatures
title_short Evolution of Microstructure, Mechanical Properties, and Corrosion Resistance of Mg–2.2Gd–2.2Zn–0.2Ca (wt%) Alloy by Extrusion at Various Temperatures
title_sort evolution of microstructure mechanical properties and corrosion resistance of mg 2 2gd 2 2zn 0 2ca wt alloy by extrusion at various temperatures
topic magnesium
homogenization
extrusion
dynamic recrystallization
tensile properties
corrosion
url https://www.mdpi.com/1996-1944/16/8/3075
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