Effect of experimental parameters on the synthesis of Fe3O4 nanoparticles by ascorbic acid mediated reduction of Fe(acac)3
Synthesis of Fe3O4 nanoparticles was carried out by ascorbic acid mediated reduction of Fe(acac)3. In order to achieve control over size, synthesis was carried out at different synthesis conditions. Small (8 nm, 9 nm and 15 nm), medium (22 nm, 29 nm, 33 nm and 42 nm) and large (76 nm, 108 nm) sized...
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| Format: | Article |
| Language: | English |
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Applied Science Innovations Private Limited
2019-09-01
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| Series: | Carbon: Science and Technology |
| Subjects: | |
| Online Access: | http://www.applied-science-innovations.com/cst-web-site/CST-11-3-2019/CST-367-11-3-2019-6-26.pdf |
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| author | Ajinkya G. Nene Prakash R. Somani M. Takahashi M. Umeno |
| author_facet | Ajinkya G. Nene Prakash R. Somani M. Takahashi M. Umeno |
| author_sort | Ajinkya G. Nene |
| collection | DOAJ |
| description | Synthesis of Fe3O4 nanoparticles was carried out by ascorbic acid mediated reduction of Fe(acac)3. In order to achieve control over size, synthesis was carried out at different synthesis conditions. Small (8 nm, 9 nm and 15 nm), medium (22 nm, 29 nm, 33 nm and 42 nm) and large (76 nm, 108 nm) sized Fe3O4 nanoparticles have been synthesized by varying and controlling the experimental conditions. Mechanism for the formation of Fe3O4 nanoparticles is proposed. Our method is observed to yield reproducible results, confirmed by doing the repeated synthesis several times. |
| first_indexed | 2024-12-13T18:43:42Z |
| format | Article |
| id | doaj.art-3b10e2828df94ac8a99a273067f9ff97 |
| institution | Directory Open Access Journal |
| issn | 0974-0546 0974-0546 |
| language | English |
| last_indexed | 2024-12-13T18:43:42Z |
| publishDate | 2019-09-01 |
| publisher | Applied Science Innovations Private Limited |
| record_format | Article |
| series | Carbon: Science and Technology |
| spelling | doaj.art-3b10e2828df94ac8a99a273067f9ff972022-12-21T23:35:08ZengApplied Science Innovations Private LimitedCarbon: Science and Technology0974-05460974-05462019-09-01113626Effect of experimental parameters on the synthesis of Fe3O4 nanoparticles by ascorbic acid mediated reduction of Fe(acac)3Ajinkya G. Nene0Prakash R. Somani1M. Takahashi2M. Umeno 3Department of Applied Chemistry, Chubu University, 1200 Matsumoto-cho, Kasugai-shi, AichiKen, 487-8501, Japan.Center for Grand Challenges and Green Technologies, Applied Science Innovations Pvt. Ltd., Pune - 411041, Maharashtra, India.Department of Applied Chemistry, Chubu University, 1200 Matsumoto-cho, Kasugai-shi, AichiKen, 487-8501, Japan.Institute for General Research of Science, Chubu University, 1200 Matsumoto-cho, Kasugai-shi, Aichi-Ken 487-8501, Japan.Synthesis of Fe3O4 nanoparticles was carried out by ascorbic acid mediated reduction of Fe(acac)3. In order to achieve control over size, synthesis was carried out at different synthesis conditions. Small (8 nm, 9 nm and 15 nm), medium (22 nm, 29 nm, 33 nm and 42 nm) and large (76 nm, 108 nm) sized Fe3O4 nanoparticles have been synthesized by varying and controlling the experimental conditions. Mechanism for the formation of Fe3O4 nanoparticles is proposed. Our method is observed to yield reproducible results, confirmed by doing the repeated synthesis several times.http://www.applied-science-innovations.com/cst-web-site/CST-11-3-2019/CST-367-11-3-2019-6-26.pdf: Fe3O4 nanoparticlesSize controlreproducibility |
| spellingShingle | Ajinkya G. Nene Prakash R. Somani M. Takahashi M. Umeno Effect of experimental parameters on the synthesis of Fe3O4 nanoparticles by ascorbic acid mediated reduction of Fe(acac)3 Carbon: Science and Technology : Fe3O4 nanoparticles Size control reproducibility |
| title | Effect of experimental parameters on the synthesis of Fe3O4 nanoparticles by ascorbic acid mediated reduction of Fe(acac)3 |
| title_full | Effect of experimental parameters on the synthesis of Fe3O4 nanoparticles by ascorbic acid mediated reduction of Fe(acac)3 |
| title_fullStr | Effect of experimental parameters on the synthesis of Fe3O4 nanoparticles by ascorbic acid mediated reduction of Fe(acac)3 |
| title_full_unstemmed | Effect of experimental parameters on the synthesis of Fe3O4 nanoparticles by ascorbic acid mediated reduction of Fe(acac)3 |
| title_short | Effect of experimental parameters on the synthesis of Fe3O4 nanoparticles by ascorbic acid mediated reduction of Fe(acac)3 |
| title_sort | effect of experimental parameters on the synthesis of fe3o4 nanoparticles by ascorbic acid mediated reduction of fe acac 3 |
| topic | : Fe3O4 nanoparticles Size control reproducibility |
| url | http://www.applied-science-innovations.com/cst-web-site/CST-11-3-2019/CST-367-11-3-2019-6-26.pdf |
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