Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis
An optimum route to synthesis the W-based composite powders with homogeneous dispersion of oxide nanoparticles was investigated. The La2O3 dispersed W powder was synthesized by ultrasonic spray pyrolysis using ammonium metatungstate hydrate and lanthanum nitrate. The dispersion of Y2O3 nanoparticles...
Main Authors: | , , , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Polish Academy of Sciences
2022-11-01
|
Series: | Archives of Metallurgy and Materials |
Subjects: | |
Online Access: | https://journals.pan.pl/Content/125123/PDF/AMM-2022-4-41-Sung-Tag%20Oh.pdf |
_version_ | 1811317500123545600 |
---|---|
author | Youn Ji Heo Eui Seon Lee Jeong Hyun Kim Young-In Lee Young-Keun Jeong Sung-Tag Oh |
author_facet | Youn Ji Heo Eui Seon Lee Jeong Hyun Kim Young-In Lee Young-Keun Jeong Sung-Tag Oh |
author_sort | Youn Ji Heo |
collection | DOAJ |
description | An optimum route to synthesis the W-based composite powders with homogeneous dispersion of oxide nanoparticles was investigated. The La2O3 dispersed W powder was synthesized by ultrasonic spray pyrolysis using ammonium metatungstate hydrate and lanthanum nitrate. The dispersion of Y2O3 nanoparticles in W- La2O3 powder was carried out by a polymer addition solution method using yttrium nitrate. XPS and TEM analyses for the composite powder showed that the nano-sized La2O3 and Y2O3 particles were well distributed in W powder. This study suggests that the combination processing of ultrasonic spray pyrolysis and polymeric additive solution is a promising way to synthesis W-based composite powders. |
first_indexed | 2024-04-13T12:09:13Z |
format | Article |
id | doaj.art-3c5a55f415b04743a5e165a7354ecb82 |
institution | Directory Open Access Journal |
issn | 2300-1909 |
language | English |
last_indexed | 2024-04-13T12:09:13Z |
publishDate | 2022-11-01 |
publisher | Polish Academy of Sciences |
record_format | Article |
series | Archives of Metallurgy and Materials |
spelling | doaj.art-3c5a55f415b04743a5e165a7354ecb822022-12-22T02:47:33ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092022-11-01vol. 67No 415071510https://doi.org/10.24425/amm.2022.141083Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray PyrolysisYoun Ji Heo0https://orcid.org/0000-0003-3932-3491Eui Seon Lee1https://orcid.org/0000-0001-6405-7303Jeong Hyun Kim2https://orcid.org/0000-0002-0998-7732Young-In Lee3https://orcid.org/0000-0002-9830-8294Young-Keun Jeong4https://orcid.org/0000-0002-1842-4528Sung-Tag Oh5https://orcid.org/0000-0003-4556-4291Seoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaSeoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaSeoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaSeoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaPusan National University, Graduate School of Convergence Science, Busan 46241, Republic of KoreaSeoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaAn optimum route to synthesis the W-based composite powders with homogeneous dispersion of oxide nanoparticles was investigated. The La2O3 dispersed W powder was synthesized by ultrasonic spray pyrolysis using ammonium metatungstate hydrate and lanthanum nitrate. The dispersion of Y2O3 nanoparticles in W- La2O3 powder was carried out by a polymer addition solution method using yttrium nitrate. XPS and TEM analyses for the composite powder showed that the nano-sized La2O3 and Y2O3 particles were well distributed in W powder. This study suggests that the combination processing of ultrasonic spray pyrolysis and polymeric additive solution is a promising way to synthesis W-based composite powders.https://journals.pan.pl/Content/125123/PDF/AMM-2022-4-41-Sung-Tag%20Oh.pdfw composite powderla2o3-y2o3 dispersionultrasonic spray pyrolysispolymeric additive solution method |
spellingShingle | Youn Ji Heo Eui Seon Lee Jeong Hyun Kim Young-In Lee Young-Keun Jeong Sung-Tag Oh Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis Archives of Metallurgy and Materials w composite powder la2o3-y2o3 dispersion ultrasonic spray pyrolysis polymeric additive solution method |
title | Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis |
title_full | Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis |
title_fullStr | Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis |
title_full_unstemmed | Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis |
title_short | Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis |
title_sort | synthesis and characterization of w composite powder with la 2o 3 y 2o 3 nano dispersoids by ultrasonic spray pyrolysis |
topic | w composite powder la2o3-y2o3 dispersion ultrasonic spray pyrolysis polymeric additive solution method |
url | https://journals.pan.pl/Content/125123/PDF/AMM-2022-4-41-Sung-Tag%20Oh.pdf |
work_keys_str_mv | AT younjiheo synthesisandcharacterizationofwcompositepowderwithla2o3y2o3nanodispersoidsbyultrasonicspraypyrolysis AT euiseonlee synthesisandcharacterizationofwcompositepowderwithla2o3y2o3nanodispersoidsbyultrasonicspraypyrolysis AT jeonghyunkim synthesisandcharacterizationofwcompositepowderwithla2o3y2o3nanodispersoidsbyultrasonicspraypyrolysis AT younginlee synthesisandcharacterizationofwcompositepowderwithla2o3y2o3nanodispersoidsbyultrasonicspraypyrolysis AT youngkeunjeong synthesisandcharacterizationofwcompositepowderwithla2o3y2o3nanodispersoidsbyultrasonicspraypyrolysis AT sungtagoh synthesisandcharacterizationofwcompositepowderwithla2o3y2o3nanodispersoidsbyultrasonicspraypyrolysis |