Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis

An optimum route to synthesis the W-based composite powders with homogeneous dispersion of oxide nanoparticles was investigated. The La2O3 dispersed W powder was synthesized by ultrasonic spray pyrolysis using ammonium metatungstate hydrate and lanthanum nitrate. The dispersion of Y2O3 nanoparticles...

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Main Authors: Youn Ji Heo, Eui Seon Lee, Jeong Hyun Kim, Young-In Lee, Young-Keun Jeong, Sung-Tag Oh
Format: Article
Language:English
Published: Polish Academy of Sciences 2022-11-01
Series:Archives of Metallurgy and Materials
Subjects:
Online Access:https://journals.pan.pl/Content/125123/PDF/AMM-2022-4-41-Sung-Tag%20Oh.pdf
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author Youn Ji Heo
Eui Seon Lee
Jeong Hyun Kim
Young-In Lee
Young-Keun Jeong
Sung-Tag Oh
author_facet Youn Ji Heo
Eui Seon Lee
Jeong Hyun Kim
Young-In Lee
Young-Keun Jeong
Sung-Tag Oh
author_sort Youn Ji Heo
collection DOAJ
description An optimum route to synthesis the W-based composite powders with homogeneous dispersion of oxide nanoparticles was investigated. The La2O3 dispersed W powder was synthesized by ultrasonic spray pyrolysis using ammonium metatungstate hydrate and lanthanum nitrate. The dispersion of Y2O3 nanoparticles in W- La2O3 powder was carried out by a polymer addition solution method using yttrium nitrate. XPS and TEM analyses for the composite powder showed that the nano-sized La2O3 and Y2O3 particles were well distributed in W powder. This study suggests that the combination processing of ultrasonic spray pyrolysis and polymeric additive solution is a promising way to synthesis W-based composite powders.
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spelling doaj.art-3c5a55f415b04743a5e165a7354ecb822022-12-22T02:47:33ZengPolish Academy of SciencesArchives of Metallurgy and Materials2300-19092022-11-01vol. 67No 415071510https://doi.org/10.24425/amm.2022.141083Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray PyrolysisYoun Ji Heo0https://orcid.org/0000-0003-3932-3491Eui Seon Lee1https://orcid.org/0000-0001-6405-7303Jeong Hyun Kim2https://orcid.org/0000-0002-0998-7732Young-In Lee3https://orcid.org/0000-0002-9830-8294Young-Keun Jeong4https://orcid.org/0000-0002-1842-4528Sung-Tag Oh5https://orcid.org/0000-0003-4556-4291Seoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaSeoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaSeoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaSeoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaPusan National University, Graduate School of Convergence Science, Busan 46241, Republic of KoreaSeoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of KoreaAn optimum route to synthesis the W-based composite powders with homogeneous dispersion of oxide nanoparticles was investigated. The La2O3 dispersed W powder was synthesized by ultrasonic spray pyrolysis using ammonium metatungstate hydrate and lanthanum nitrate. The dispersion of Y2O3 nanoparticles in W- La2O3 powder was carried out by a polymer addition solution method using yttrium nitrate. XPS and TEM analyses for the composite powder showed that the nano-sized La2O3 and Y2O3 particles were well distributed in W powder. This study suggests that the combination processing of ultrasonic spray pyrolysis and polymeric additive solution is a promising way to synthesis W-based composite powders.https://journals.pan.pl/Content/125123/PDF/AMM-2022-4-41-Sung-Tag%20Oh.pdfw composite powderla2o3-y2o3 dispersionultrasonic spray pyrolysispolymeric additive solution method
spellingShingle Youn Ji Heo
Eui Seon Lee
Jeong Hyun Kim
Young-In Lee
Young-Keun Jeong
Sung-Tag Oh
Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis
Archives of Metallurgy and Materials
w composite powder
la2o3-y2o3 dispersion
ultrasonic spray pyrolysis
polymeric additive solution method
title Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis
title_full Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis
title_fullStr Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis
title_full_unstemmed Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis
title_short Synthesis and Characterization of W Composite Powder with La 2O 3-Y 2O 3 Nano-Dispersoids by Ultrasonic Spray Pyrolysis
title_sort synthesis and characterization of w composite powder with la 2o 3 y 2o 3 nano dispersoids by ultrasonic spray pyrolysis
topic w composite powder
la2o3-y2o3 dispersion
ultrasonic spray pyrolysis
polymeric additive solution method
url https://journals.pan.pl/Content/125123/PDF/AMM-2022-4-41-Sung-Tag%20Oh.pdf
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