Investigation on the properties of vanadium doping WO3 nanostructures by hydrothermal method

To make tungsten trioxide nanostructures, hydrothermal methods were used. A temperature of 200 °C was used to prepare the samples. 48-hour reactions were used to examine how reaction time affected the characteristics of tungsten trioxide nanostructures. For one hour, the samples were calcined at 500...

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Main Authors: S. Karthikeyan, M. Selvapandiyan, P. Sasikumar, M. Parthibavaraman, S. Nithiyanantham, V.T. Srisuvetha
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2022-01-01
Series:Materials Science for Energy Technologies
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2589299122000283
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author S. Karthikeyan
M. Selvapandiyan
P. Sasikumar
M. Parthibavaraman
S. Nithiyanantham
V.T. Srisuvetha
author_facet S. Karthikeyan
M. Selvapandiyan
P. Sasikumar
M. Parthibavaraman
S. Nithiyanantham
V.T. Srisuvetha
author_sort S. Karthikeyan
collection DOAJ
description To make tungsten trioxide nanostructures, hydrothermal methods were used. A temperature of 200 °C was used to prepare the samples. 48-hour reactions were used to examine how reaction time affected the characteristics of tungsten trioxide nanostructures. For one hour, the samples were calcined at 500 °C. After using ammonium metavanadate to dope vanadium, the same method for making WO3 was used. Many different characterization techniques have been performed on the calcined and prepared samples. X-ray diffraction (XRD) and scanning electron microscopy (SEM) and Transmission electron microscopy (TEM) were used to examine the samples' structural and morphological characteristics (SEM). EDAX has verified that vanadium has been doped. Fourier transformed infrared spectroscopy was used to do the vibrational analysis (FTIR).
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spelling doaj.art-3d377bc07f754b738ef0fb792ad69dc62023-01-26T04:47:21ZengKeAi Communications Co., Ltd.Materials Science for Energy Technologies2589-29912022-01-015411415Investigation on the properties of vanadium doping WO3 nanostructures by hydrothermal methodS. Karthikeyan0M. Selvapandiyan1P. Sasikumar2M. Parthibavaraman3S. Nithiyanantham4V.T. Srisuvetha5Department of Physics, Periyar University Centre For PG and Research Studies, Dharmapuri 635 205, Tamil Nadu, IndiaDepartment of Physics, Periyar University Centre For PG and Research Studies, Dharmapuri 635 205, Tamil Nadu, IndiaDepartment of Physics, Periyar University Centre For PG and Research Studies, Dharmapuri 635 205, Tamil Nadu, India; Department of Physics, Saveetha Schools of Engineering, (SIMATS), Chennai 602 105, Tamilnadu, India; Corresponding authors.PG and Resaerch Department of Physics, Chikkaiah Naicker College, Erode 638 004, Tamil Nadu, IndiaPG and Research Department of Physics, Thiru. Vi. Kalyanansundaram Govt Arts & Science College, Thiruvarur 610003, Tamil Nadu, India; Corresponding authors.Department of Physics, Gonzaga College of Arts and Science for Women, Krishnagiri 635108, Tamilnadu, IndiaTo make tungsten trioxide nanostructures, hydrothermal methods were used. A temperature of 200 °C was used to prepare the samples. 48-hour reactions were used to examine how reaction time affected the characteristics of tungsten trioxide nanostructures. For one hour, the samples were calcined at 500 °C. After using ammonium metavanadate to dope vanadium, the same method for making WO3 was used. Many different characterization techniques have been performed on the calcined and prepared samples. X-ray diffraction (XRD) and scanning electron microscopy (SEM) and Transmission electron microscopy (TEM) were used to examine the samples' structural and morphological characteristics (SEM). EDAX has verified that vanadium has been doped. Fourier transformed infrared spectroscopy was used to do the vibrational analysis (FTIR).http://www.sciencedirect.com/science/article/pii/S2589299122000283VanadiumHydrothermalNanostructureCrystallinityXRDSEM
spellingShingle S. Karthikeyan
M. Selvapandiyan
P. Sasikumar
M. Parthibavaraman
S. Nithiyanantham
V.T. Srisuvetha
Investigation on the properties of vanadium doping WO3 nanostructures by hydrothermal method
Materials Science for Energy Technologies
Vanadium
Hydrothermal
Nanostructure
Crystallinity
XRD
SEM
title Investigation on the properties of vanadium doping WO3 nanostructures by hydrothermal method
title_full Investigation on the properties of vanadium doping WO3 nanostructures by hydrothermal method
title_fullStr Investigation on the properties of vanadium doping WO3 nanostructures by hydrothermal method
title_full_unstemmed Investigation on the properties of vanadium doping WO3 nanostructures by hydrothermal method
title_short Investigation on the properties of vanadium doping WO3 nanostructures by hydrothermal method
title_sort investigation on the properties of vanadium doping wo3 nanostructures by hydrothermal method
topic Vanadium
Hydrothermal
Nanostructure
Crystallinity
XRD
SEM
url http://www.sciencedirect.com/science/article/pii/S2589299122000283
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AT mselvapandiyan investigationonthepropertiesofvanadiumdopingwo3nanostructuresbyhydrothermalmethod
AT psasikumar investigationonthepropertiesofvanadiumdopingwo3nanostructuresbyhydrothermalmethod
AT mparthibavaraman investigationonthepropertiesofvanadiumdopingwo3nanostructuresbyhydrothermalmethod
AT snithiyanantham investigationonthepropertiesofvanadiumdopingwo3nanostructuresbyhydrothermalmethod
AT vtsrisuvetha investigationonthepropertiesofvanadiumdopingwo3nanostructuresbyhydrothermalmethod