Synthesis, Characterization Of New Schiff Base And Some Metal Complexes Derived From Glyoxylic Acid And O-Phenylenediamine
The new Schiff base, namely (2-Amino-phenylimino)-acetic acid (L) was prepared from condensation of glyoxylic acid with o-phenylene diamine. The structure (L) was characterized by, IR, 1 H, 13 C-NMR and CHN analysis. Metal complexes of the ligand (L) were synthesized and their structures were...
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| Format: | Article |
| Language: | English |
| Published: |
University of Baghdad
2017-05-01
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| Series: | Ibn Al-Haitham Journal for Pure and Applied Sciences |
| Subjects: | |
| Online Access: | https://jih.uobaghdad.edu.iq/index.php/j/article/view/592 |
| Summary: | The new Schiff base, namely (2-Amino-phenylimino)-acetic acid (L) was prepared
from condensation of glyoxylic acid with o-phenylene diamine. The structure (L) was
characterized by, IR,
1
H,
13
C-NMR and CHN analysis. Metal complexes of the ligand (L)
were synthesized and their structures were characterized by Atomic absorption, IR and UV-Visible spectra, molar conductivity, magnetic moment and molar ratio determination (Co
+2
,
Cd
+2
) complexes. All complexes showed octahedral geometries.
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| ISSN: | 1609-4042 2521-3407 |