Improved Ammonia Sensing by Solution Processed Dodecyl Benzene Sulfonic Acid Doped Polyaniline Nanorod Networks

Dodecyl benzene sulphonic acid (DBSA) doped polyaniline (PANI) nanorods have been synthesized by a templateless route via in-situ emulsion polymerization of aniline in aqueous DBSA solution. XRD patterns, UV-Visible Spectroscopy, and FTIR analysis confirm the formation of PANI and PANI-DBSA, whereas...

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Main Authors: Anju Yadav, Jitendra Kumar, Md. Shahabuddin, Ajay Agarwal, Parveen Saini
Format: Article
Language:English
Published: IEEE 2019-01-01
Series:IEEE Access
Subjects:
Online Access:https://ieeexplore.ieee.org/document/8844731/
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author Anju Yadav
Jitendra Kumar
Md. Shahabuddin
Ajay Agarwal
Parveen Saini
author_facet Anju Yadav
Jitendra Kumar
Md. Shahabuddin
Ajay Agarwal
Parveen Saini
author_sort Anju Yadav
collection DOAJ
description Dodecyl benzene sulphonic acid (DBSA) doped polyaniline (PANI) nanorods have been synthesized by a templateless route via in-situ emulsion polymerization of aniline in aqueous DBSA solution. XRD patterns, UV-Visible Spectroscopy, and FTIR analysis confirm the formation of PANI and PANI-DBSA, whereas FESEM images revealed their elongated rod shaped morphology. The chloroform dispersion of synthesized PANI-DBSA was spin coated over prefabricated interdigitated Pt patterned glass substrate to realize porous gas sensing active layer. The sensor displays good response in 1-1200 ppm ammonia concentration range and can repeatedly detect 300 ppm of ammonia with response time of 6 s, recovery time of 37 s and relative response value of 9.57. Besides, its response was found to be linear for 1-50 ppm ammonia concentration with relative response per ppm value of 0.01675.
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spelling doaj.art-3da55836ec6244789501326c4fe5dcdc2022-12-21T18:30:44ZengIEEEIEEE Access2169-35362019-01-01713957113957910.1109/ACCESS.2019.29423618844731Improved Ammonia Sensing by Solution Processed Dodecyl Benzene Sulfonic Acid Doped Polyaniline Nanorod NetworksAnju Yadav0https://orcid.org/0000-0003-3960-4111Jitendra Kumar1Md. Shahabuddin2Ajay Agarwal3Parveen Saini4Nano Bio Sensors Group, CSIR - Central Electronics Engineering Research Institute, Pilani, IndiaDepartment of Physics, Jamia Millia Islamia, New Delhi, IndiaDepartment of Physics, Allama Iqbal College, Patliputra University, Patna, IndiaNano Bio Sensors Group, CSIR - Central Electronics Engineering Research Institute, Pilani, IndiaAcademy of Scientific and Innovative Research (AcSIR), New Delhi, IndiaDodecyl benzene sulphonic acid (DBSA) doped polyaniline (PANI) nanorods have been synthesized by a templateless route via in-situ emulsion polymerization of aniline in aqueous DBSA solution. XRD patterns, UV-Visible Spectroscopy, and FTIR analysis confirm the formation of PANI and PANI-DBSA, whereas FESEM images revealed their elongated rod shaped morphology. The chloroform dispersion of synthesized PANI-DBSA was spin coated over prefabricated interdigitated Pt patterned glass substrate to realize porous gas sensing active layer. The sensor displays good response in 1-1200 ppm ammonia concentration range and can repeatedly detect 300 ppm of ammonia with response time of 6 s, recovery time of 37 s and relative response value of 9.57. Besides, its response was found to be linear for 1-50 ppm ammonia concentration with relative response per ppm value of 0.01675.https://ieeexplore.ieee.org/document/8844731/Ammonia gas sensorconducting polymerdodecyl benzene sulfonic acid doped polyaniline
spellingShingle Anju Yadav
Jitendra Kumar
Md. Shahabuddin
Ajay Agarwal
Parveen Saini
Improved Ammonia Sensing by Solution Processed Dodecyl Benzene Sulfonic Acid Doped Polyaniline Nanorod Networks
IEEE Access
Ammonia gas sensor
conducting polymer
dodecyl benzene sulfonic acid doped polyaniline
title Improved Ammonia Sensing by Solution Processed Dodecyl Benzene Sulfonic Acid Doped Polyaniline Nanorod Networks
title_full Improved Ammonia Sensing by Solution Processed Dodecyl Benzene Sulfonic Acid Doped Polyaniline Nanorod Networks
title_fullStr Improved Ammonia Sensing by Solution Processed Dodecyl Benzene Sulfonic Acid Doped Polyaniline Nanorod Networks
title_full_unstemmed Improved Ammonia Sensing by Solution Processed Dodecyl Benzene Sulfonic Acid Doped Polyaniline Nanorod Networks
title_short Improved Ammonia Sensing by Solution Processed Dodecyl Benzene Sulfonic Acid Doped Polyaniline Nanorod Networks
title_sort improved ammonia sensing by solution processed dodecyl benzene sulfonic acid doped polyaniline nanorod networks
topic Ammonia gas sensor
conducting polymer
dodecyl benzene sulfonic acid doped polyaniline
url https://ieeexplore.ieee.org/document/8844731/
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AT mdshahabuddin improvedammoniasensingbysolutionprocesseddodecylbenzenesulfonicaciddopedpolyanilinenanorodnetworks
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