Preparation and characterization of AgNPs@SNC nanocomposites

Starch nanocrystal (SNC) was prepared by 40°C weak sulfuric acid hydrolysis method. Silver nanoparticles (AgNPs) were simply and quickly reduced in situ on starch nanocrystal by ultrasonic assisted reduction method. UV-vis absorption spectrum verified the existence of AgNPs. The surface modification...

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Main Authors: Zhu Jiang, Ni Haitao, Luo Liu, Yang Heshan
Format: Article
Language:English
Published: EDP Sciences 2023-01-01
Series:E3S Web of Conferences
Online Access:https://www.e3s-conferences.org/articles/e3sconf/pdf/2023/22/e3sconf_isesce2023_04029.pdf
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author Zhu Jiang
Ni Haitao
Luo Liu
Yang Heshan
author_facet Zhu Jiang
Ni Haitao
Luo Liu
Yang Heshan
author_sort Zhu Jiang
collection DOAJ
description Starch nanocrystal (SNC) was prepared by 40°C weak sulfuric acid hydrolysis method. Silver nanoparticles (AgNPs) were simply and quickly reduced in situ on starch nanocrystal by ultrasonic assisted reduction method. UV-vis absorption spectrum verified the existence of AgNPs. The surface modification of AgNPs@SNC was carried out by using 3-aminopropyltriethoxysilane (APTES) with simple structure and low cost to improve its dispersivity in the hydrophobic polymer matrix. Then the success of modification was preliminarily confirmed by the Fourier-transform infrared spectroscopy. Taking Staphylococcus aureus and Escherichia coli bacteria as objects of the study, the antibacterial properties of AgNPs@SNC were also explored, and the test results showed that AgNPs@SNC had certain inhibitory effect on Escherichia coli.
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spelling doaj.art-3de9b715961744adbd04a7e966ea895d2023-05-11T09:09:12ZengEDP SciencesE3S Web of Conferences2267-12422023-01-013850402910.1051/e3sconf/202338504029e3sconf_isesce2023_04029Preparation and characterization of AgNPs@SNC nanocompositesZhu Jiang0Ni Haitao1Luo Liu2Yang Heshan3Chongqing Key Laboratory of Environmental Materials & Remediation Technologies, Chongqing University of Arts and SciencesChongqing Key Laboratory of Environmental Materials & Remediation Technologies, Chongqing University of Arts and SciencesCollege of Chemistry and Environmental Engineering, Chongqing University of Arts and SciencesCollege of Chemistry and Environmental Engineering, Chongqing University of Arts and SciencesStarch nanocrystal (SNC) was prepared by 40°C weak sulfuric acid hydrolysis method. Silver nanoparticles (AgNPs) were simply and quickly reduced in situ on starch nanocrystal by ultrasonic assisted reduction method. UV-vis absorption spectrum verified the existence of AgNPs. The surface modification of AgNPs@SNC was carried out by using 3-aminopropyltriethoxysilane (APTES) with simple structure and low cost to improve its dispersivity in the hydrophobic polymer matrix. Then the success of modification was preliminarily confirmed by the Fourier-transform infrared spectroscopy. Taking Staphylococcus aureus and Escherichia coli bacteria as objects of the study, the antibacterial properties of AgNPs@SNC were also explored, and the test results showed that AgNPs@SNC had certain inhibitory effect on Escherichia coli.https://www.e3s-conferences.org/articles/e3sconf/pdf/2023/22/e3sconf_isesce2023_04029.pdf
spellingShingle Zhu Jiang
Ni Haitao
Luo Liu
Yang Heshan
Preparation and characterization of AgNPs@SNC nanocomposites
E3S Web of Conferences
title Preparation and characterization of AgNPs@SNC nanocomposites
title_full Preparation and characterization of AgNPs@SNC nanocomposites
title_fullStr Preparation and characterization of AgNPs@SNC nanocomposites
title_full_unstemmed Preparation and characterization of AgNPs@SNC nanocomposites
title_short Preparation and characterization of AgNPs@SNC nanocomposites
title_sort preparation and characterization of agnps snc nanocomposites
url https://www.e3s-conferences.org/articles/e3sconf/pdf/2023/22/e3sconf_isesce2023_04029.pdf
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AT nihaitao preparationandcharacterizationofagnpssncnanocomposites
AT luoliu preparationandcharacterizationofagnpssncnanocomposites
AT yangheshan preparationandcharacterizationofagnpssncnanocomposites