X-Ray Diffraction and Microstructure of Tin Dioxide with Addition of Fe
Preparation and characterization of tin dioxide, SnO2, had been carried out by precipitation process of SnCl2.2H2O in ammonia and aqua solutions with comparison of 1 : 7. FeCl3 was added to solution with variation of 0, 0,1, 0.2, 0.5 and 1.0 gram respectively and then sintered at 900°C. The X-ray di...
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| Format: | Article |
| Language: | English |
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Fakultas MIPA Universitas Jember
2013-01-01
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| Series: | Jurnal Ilmu Dasar |
| Subjects: | |
| Online Access: | https://jurnal.unej.ac.id/index.php/JID/article/view/359 |
| _version_ | 1830144817358700544 |
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| author | Posman Manurung |
| author_facet | Posman Manurung |
| author_sort | Posman Manurung |
| collection | DOAJ |
| description | Preparation and characterization of tin dioxide, SnO2, had been carried out by precipitation process of SnCl2.2H2O in ammonia and aqua solutions with comparison of 1 : 7. FeCl3 was added to solution with variation of 0, 0,1, 0.2, 0.5 and 1.0 gram respectively and then sintered at 900°C. The X-ray diffraction (XRD) analysis shows that the intensity of diffraction increases with the addition of Fe. The addition of Fe does not cause the new phase. Generally, the Bragg angle is relative same for all samples that means Fe does not change significantly the cell parameters. Scanning electron microscopy (SEM) image shows the microstructure changed with the addition of Fe. On the small addition, the microstructure tends to oval and on the larger addition to plateau. |
| first_indexed | 2024-12-17T10:13:38Z |
| format | Article |
| id | doaj.art-3ee1b08c08e2453893f650a3865956f6 |
| institution | Directory Open Access Journal |
| issn | 1411-5735 2442-5613 |
| language | English |
| last_indexed | 2024-12-17T10:13:38Z |
| publishDate | 2013-01-01 |
| publisher | Fakultas MIPA Universitas Jember |
| record_format | Article |
| series | Jurnal Ilmu Dasar |
| spelling | doaj.art-3ee1b08c08e2453893f650a3865956f62022-12-21T21:52:58ZengFakultas MIPA Universitas JemberJurnal Ilmu Dasar1411-57352442-56132013-01-011219196359X-Ray Diffraction and Microstructure of Tin Dioxide with Addition of FePosman ManurungPreparation and characterization of tin dioxide, SnO2, had been carried out by precipitation process of SnCl2.2H2O in ammonia and aqua solutions with comparison of 1 : 7. FeCl3 was added to solution with variation of 0, 0,1, 0.2, 0.5 and 1.0 gram respectively and then sintered at 900°C. The X-ray diffraction (XRD) analysis shows that the intensity of diffraction increases with the addition of Fe. The addition of Fe does not cause the new phase. Generally, the Bragg angle is relative same for all samples that means Fe does not change significantly the cell parameters. Scanning electron microscopy (SEM) image shows the microstructure changed with the addition of Fe. On the small addition, the microstructure tends to oval and on the larger addition to plateau.https://jurnal.unej.ac.id/index.php/JID/article/view/359tin dioxidediffractionmicrostructure |
| spellingShingle | Posman Manurung X-Ray Diffraction and Microstructure of Tin Dioxide with Addition of Fe Jurnal Ilmu Dasar tin dioxide diffraction microstructure |
| title | X-Ray Diffraction and Microstructure of Tin Dioxide with Addition of Fe |
| title_full | X-Ray Diffraction and Microstructure of Tin Dioxide with Addition of Fe |
| title_fullStr | X-Ray Diffraction and Microstructure of Tin Dioxide with Addition of Fe |
| title_full_unstemmed | X-Ray Diffraction and Microstructure of Tin Dioxide with Addition of Fe |
| title_short | X-Ray Diffraction and Microstructure of Tin Dioxide with Addition of Fe |
| title_sort | x ray diffraction and microstructure of tin dioxide with addition of fe |
| topic | tin dioxide diffraction microstructure |
| url | https://jurnal.unej.ac.id/index.php/JID/article/view/359 |
| work_keys_str_mv | AT posmanmanurung xraydiffractionandmicrostructureoftindioxidewithadditionoffe |