Method for the Analysis of Respirable Airborne Particulates on Filter Using the Mineral Liberation Analyser

In recent years, the Mineral Liberation Analyser (MLA) has played a pivotal role in analysing respirable and inhalable ambient air samples collected on filters from both underground coal and metalliferous mines. Leveraging backscattered electron (BSE) image analysis and X-ray mineral identification,...

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Main Authors: Nikky LaBranche, Elaine Wightman, Kellie Teale, Kelly Johnstone, David Cliff
Format: Article
Language:English
Published: MDPI AG 2023-12-01
Series:Minerals
Subjects:
Online Access:https://www.mdpi.com/2075-163X/13/12/1526
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author Nikky LaBranche
Elaine Wightman
Kellie Teale
Kelly Johnstone
David Cliff
author_facet Nikky LaBranche
Elaine Wightman
Kellie Teale
Kelly Johnstone
David Cliff
author_sort Nikky LaBranche
collection DOAJ
description In recent years, the Mineral Liberation Analyser (MLA) has played a pivotal role in analysing respirable and inhalable ambient air samples collected on filters from both underground coal and metalliferous mines. Leveraging backscattered electron (BSE) image analysis and X-ray mineral identification, the MLA offers automated quantitative mineral characterization. The escalating prevalence and severity of mine dust lung diseases, particularly among young miners, have reignited interest in comprehensively understanding the dust’s characterization, encompassing mineralogy, particle size, and shape. Merely measuring total respirable dust exposure and its duration based on gravimetrically determined weight is no longer deemed sufficient in addressing the evolving landscape of occupational health challenges in mining environments. Since the publication of previous studies, efforts have been dedicated to refining the Mineral Liberation Analyser (MLA) methodology for respirable dust sampling. This refinement, discussed in detail in this paper, encompasses various enhancements, such as the implementation of data checks to identify carbon contamination, backscattered electron (BSE) drift, and the misclassification of X-ray spectra. Additionally, an examination of sampling efficiency led to the exploration of using smaller samples as an alternative to the time-intensive analysis of entire filters. Furthermore, this paper presents a reanalysis of paired filter sample sets previously reported using the Sarver Group Methodology. These samples are subjected to analysis using the Mineral Liberation Analyser, providing a more detailed illustration of the outputs derived from the updated methodology and compared to previously published MLA data.
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spelling doaj.art-3f8f63e122ee4df0a7552f27e2cfe0c42023-12-22T14:26:40ZengMDPI AGMinerals2075-163X2023-12-011312152610.3390/min13121526Method for the Analysis of Respirable Airborne Particulates on Filter Using the Mineral Liberation AnalyserNikky LaBranche0Elaine Wightman1Kellie Teale2Kelly Johnstone3David Cliff4Minerals Industry Safety and Health Centre, Sustainable Minerals Institute, The University of Queensland, Brisbane, QLD 4072, AustraliaJulius Kruttschnitt Mineral Research Centre, Sustainable Minerals Institute, The University of Queensland, Indooroopilly, QLD 4068, AustraliaJulius Kruttschnitt Mineral Research Centre, Sustainable Minerals Institute, The University of Queensland, Indooroopilly, QLD 4068, AustraliaMinerals Industry Safety and Health Centre, Sustainable Minerals Institute, The University of Queensland, Brisbane, QLD 4072, AustraliaMinerals Industry Safety and Health Centre, Sustainable Minerals Institute, The University of Queensland, Brisbane, QLD 4072, AustraliaIn recent years, the Mineral Liberation Analyser (MLA) has played a pivotal role in analysing respirable and inhalable ambient air samples collected on filters from both underground coal and metalliferous mines. Leveraging backscattered electron (BSE) image analysis and X-ray mineral identification, the MLA offers automated quantitative mineral characterization. The escalating prevalence and severity of mine dust lung diseases, particularly among young miners, have reignited interest in comprehensively understanding the dust’s characterization, encompassing mineralogy, particle size, and shape. Merely measuring total respirable dust exposure and its duration based on gravimetrically determined weight is no longer deemed sufficient in addressing the evolving landscape of occupational health challenges in mining environments. Since the publication of previous studies, efforts have been dedicated to refining the Mineral Liberation Analyser (MLA) methodology for respirable dust sampling. This refinement, discussed in detail in this paper, encompasses various enhancements, such as the implementation of data checks to identify carbon contamination, backscattered electron (BSE) drift, and the misclassification of X-ray spectra. Additionally, an examination of sampling efficiency led to the exploration of using smaller samples as an alternative to the time-intensive analysis of entire filters. Furthermore, this paper presents a reanalysis of paired filter sample sets previously reported using the Sarver Group Methodology. These samples are subjected to analysis using the Mineral Liberation Analyser, providing a more detailed illustration of the outputs derived from the updated methodology and compared to previously published MLA data.https://www.mdpi.com/2075-163X/13/12/1526mineral liberation analyserparticle characterizationairborne particulate monitoringrespirable dust monitoringcoal workers pneumoconiosis
spellingShingle Nikky LaBranche
Elaine Wightman
Kellie Teale
Kelly Johnstone
David Cliff
Method for the Analysis of Respirable Airborne Particulates on Filter Using the Mineral Liberation Analyser
Minerals
mineral liberation analyser
particle characterization
airborne particulate monitoring
respirable dust monitoring
coal workers pneumoconiosis
title Method for the Analysis of Respirable Airborne Particulates on Filter Using the Mineral Liberation Analyser
title_full Method for the Analysis of Respirable Airborne Particulates on Filter Using the Mineral Liberation Analyser
title_fullStr Method for the Analysis of Respirable Airborne Particulates on Filter Using the Mineral Liberation Analyser
title_full_unstemmed Method for the Analysis of Respirable Airborne Particulates on Filter Using the Mineral Liberation Analyser
title_short Method for the Analysis of Respirable Airborne Particulates on Filter Using the Mineral Liberation Analyser
title_sort method for the analysis of respirable airborne particulates on filter using the mineral liberation analyser
topic mineral liberation analyser
particle characterization
airborne particulate monitoring
respirable dust monitoring
coal workers pneumoconiosis
url https://www.mdpi.com/2075-163X/13/12/1526
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