Non-Covalent Supported of l-Proline on Graphene Oxide/Fe3O4 Nanocomposite: A Novel, Highly Efficient and Superparamagnetically Separable Catalyst for the Synthesis of Bis-Pyrazole Derivatives
A superparamagnetic graphene oxide/Fe3O4/l-proline nano hybrid that was obtained from the non-covalent immobilization of l-proline on graphene oxide/Fe3O4 nanocomposite was used as a new magnetically separable catalyst for the efficient synthesis of 4,4′-(arylmethylene)bis(1H-pyrazol-5-ol) derivativ...
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| Format: | Article |
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MDPI AG
2018-02-01
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| Series: | Molecules |
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| Online Access: | http://www.mdpi.com/1420-3049/23/2/330 |
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| author | Mosadegh Keshavarz Amanollah Zarei Ahmady Luigi Vaccaro Maryam Kardani |
| author_facet | Mosadegh Keshavarz Amanollah Zarei Ahmady Luigi Vaccaro Maryam Kardani |
| author_sort | Mosadegh Keshavarz |
| collection | DOAJ |
| description | A superparamagnetic graphene oxide/Fe3O4/l-proline nano hybrid that was obtained from the non-covalent immobilization of l-proline on graphene oxide/Fe3O4 nanocomposite was used as a new magnetically separable catalyst for the efficient synthesis of 4,4′-(arylmethylene)bis(1H-pyrazol-5-ol) derivatives. The prepared heterogeneous catalyst was characterized using FTIR, TGA, DTG, XRD, TEM, SEM, and elemental analysis techniques. Short reaction times (5–15 min), excellent yields (87–98%), and simple experimental procedure with an easy work-up are some of the advantages of the introduced catalyst. |
| first_indexed | 2024-04-13T11:20:52Z |
| format | Article |
| id | doaj.art-3fe8465b80e14571974726eda08ad2b8 |
| institution | Directory Open Access Journal |
| issn | 1420-3049 |
| language | English |
| last_indexed | 2024-04-13T11:20:52Z |
| publishDate | 2018-02-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molecules |
| spelling | doaj.art-3fe8465b80e14571974726eda08ad2b82022-12-22T02:48:50ZengMDPI AGMolecules1420-30492018-02-0123233010.3390/molecules23020330molecules23020330Non-Covalent Supported of l-Proline on Graphene Oxide/Fe3O4 Nanocomposite: A Novel, Highly Efficient and Superparamagnetically Separable Catalyst for the Synthesis of Bis-Pyrazole DerivativesMosadegh Keshavarz0Amanollah Zarei Ahmady1Luigi Vaccaro2Maryam Kardani3Department of Gas and Petroleum, Yasouj University, Gachsaran 75918-74831, IranNanotechnology Research Center, Ahvaz Jundishapur University of Medical Sciences, Ahvaz 14536-33143, IranDepartment of Chemistry, Biology and Biotechnology, University of Perugia, 06123 Perugia, ItalyMarine Pharmaceutical Science Research Center, Ahvaz JundiShapur University of Medical sciences, Ahvaz 14536-33143, IranA superparamagnetic graphene oxide/Fe3O4/l-proline nano hybrid that was obtained from the non-covalent immobilization of l-proline on graphene oxide/Fe3O4 nanocomposite was used as a new magnetically separable catalyst for the efficient synthesis of 4,4′-(arylmethylene)bis(1H-pyrazol-5-ol) derivatives. The prepared heterogeneous catalyst was characterized using FTIR, TGA, DTG, XRD, TEM, SEM, and elemental analysis techniques. Short reaction times (5–15 min), excellent yields (87–98%), and simple experimental procedure with an easy work-up are some of the advantages of the introduced catalyst.http://www.mdpi.com/1420-3049/23/2/330">l-prolinenanocompositegraphene oxideheterogeneous catalystmagnetically separable catalyst |
| spellingShingle | Mosadegh Keshavarz Amanollah Zarei Ahmady Luigi Vaccaro Maryam Kardani Non-Covalent Supported of l-Proline on Graphene Oxide/Fe3O4 Nanocomposite: A Novel, Highly Efficient and Superparamagnetically Separable Catalyst for the Synthesis of Bis-Pyrazole Derivatives Molecules ">l-proline nanocomposite graphene oxide heterogeneous catalyst magnetically separable catalyst |
| title | Non-Covalent Supported of l-Proline on Graphene Oxide/Fe3O4 Nanocomposite: A Novel, Highly Efficient and Superparamagnetically Separable Catalyst for the Synthesis of Bis-Pyrazole Derivatives |
| title_full | Non-Covalent Supported of l-Proline on Graphene Oxide/Fe3O4 Nanocomposite: A Novel, Highly Efficient and Superparamagnetically Separable Catalyst for the Synthesis of Bis-Pyrazole Derivatives |
| title_fullStr | Non-Covalent Supported of l-Proline on Graphene Oxide/Fe3O4 Nanocomposite: A Novel, Highly Efficient and Superparamagnetically Separable Catalyst for the Synthesis of Bis-Pyrazole Derivatives |
| title_full_unstemmed | Non-Covalent Supported of l-Proline on Graphene Oxide/Fe3O4 Nanocomposite: A Novel, Highly Efficient and Superparamagnetically Separable Catalyst for the Synthesis of Bis-Pyrazole Derivatives |
| title_short | Non-Covalent Supported of l-Proline on Graphene Oxide/Fe3O4 Nanocomposite: A Novel, Highly Efficient and Superparamagnetically Separable Catalyst for the Synthesis of Bis-Pyrazole Derivatives |
| title_sort | non covalent supported of l proline on graphene oxide fe3o4 nanocomposite a novel highly efficient and superparamagnetically separable catalyst for the synthesis of bis pyrazole derivatives |
| topic | ">l-proline nanocomposite graphene oxide heterogeneous catalyst magnetically separable catalyst |
| url | http://www.mdpi.com/1420-3049/23/2/330 |
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