Identificação de resíduos de disparos de armas de fogo por meio da técnica de espectrometria de massas de alta resolução com fonte de plasma indutivo Identification of gunshot residues by high resolution inductively coupled plasma mass spectrometry
<abstract language="eng">The violence derived from crimes involving firearms represents one of the main concerns of society. For this reason modern techniques have emerged in forensic science to identify suspects at crime scenes. This work describes a methodology to identify residues...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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Sociedade Brasileira de Química
2004-06-01
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| Series: | Química Nova |
| Subjects: | |
| Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422004000300009 |
| _version_ | 1818193474097250304 |
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| author | Edson Luis Tocaia dos Reis Jorge Eduardo de Souza Sarkis Cláudio Rodrigues Oswaldo Negrini Neto Sônia Viebig |
| author_facet | Edson Luis Tocaia dos Reis Jorge Eduardo de Souza Sarkis Cláudio Rodrigues Oswaldo Negrini Neto Sônia Viebig |
| author_sort | Edson Luis Tocaia dos Reis |
| collection | DOAJ |
| description | <abstract language="eng">The violence derived from crimes involving firearms represents one of the main concerns of society. For this reason modern techniques have emerged in forensic science to identify suspects at crime scenes. This work describes a methodology to identify residues present in the hands of suspect by using a high resolution inductively coupled plasma mass spectrometry and collection procedure based on ethylenediaminetetraacetic acid (EDTA) solution as a complexing agent in moistened swabs. In order to distinguish real gunshot residues from others types of residues present in the hand of suspect, ternary ratio per cent diagrams were developed for antimony (Sb), barium (Ba) and lead (Pb) detected on the hands of volunteers, before and immediately after shooting tests, revealing a remarkable difference in both situations. |
| first_indexed | 2024-12-12T00:46:58Z |
| format | Article |
| id | doaj.art-3ff762a2481c4453be3d3f424968da04 |
| institution | Directory Open Access Journal |
| issn | 0100-4042 1678-7064 |
| language | English |
| last_indexed | 2024-12-12T00:46:58Z |
| publishDate | 2004-06-01 |
| publisher | Sociedade Brasileira de Química |
| record_format | Article |
| series | Química Nova |
| spelling | doaj.art-3ff762a2481c4453be3d3f424968da042022-12-22T00:44:06ZengSociedade Brasileira de QuímicaQuímica Nova0100-40421678-70642004-06-0127340941310.1590/S0100-40422004000300009Identificação de resíduos de disparos de armas de fogo por meio da técnica de espectrometria de massas de alta resolução com fonte de plasma indutivo Identification of gunshot residues by high resolution inductively coupled plasma mass spectrometryEdson Luis Tocaia dos ReisJorge Eduardo de Souza SarkisCláudio RodriguesOswaldo Negrini NetoSônia Viebig<abstract language="eng">The violence derived from crimes involving firearms represents one of the main concerns of society. For this reason modern techniques have emerged in forensic science to identify suspects at crime scenes. This work describes a methodology to identify residues present in the hands of suspect by using a high resolution inductively coupled plasma mass spectrometry and collection procedure based on ethylenediaminetetraacetic acid (EDTA) solution as a complexing agent in moistened swabs. In order to distinguish real gunshot residues from others types of residues present in the hand of suspect, ternary ratio per cent diagrams were developed for antimony (Sb), barium (Ba) and lead (Pb) detected on the hands of volunteers, before and immediately after shooting tests, revealing a remarkable difference in both situations.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422004000300009forensic sciencegunshot residuesinductively coupled plasma-mass spectrometry |
| spellingShingle | Edson Luis Tocaia dos Reis Jorge Eduardo de Souza Sarkis Cláudio Rodrigues Oswaldo Negrini Neto Sônia Viebig Identificação de resíduos de disparos de armas de fogo por meio da técnica de espectrometria de massas de alta resolução com fonte de plasma indutivo Identification of gunshot residues by high resolution inductively coupled plasma mass spectrometry Química Nova forensic science gunshot residues inductively coupled plasma-mass spectrometry |
| title | Identificação de resíduos de disparos de armas de fogo por meio da técnica de espectrometria de massas de alta resolução com fonte de plasma indutivo Identification of gunshot residues by high resolution inductively coupled plasma mass spectrometry |
| title_full | Identificação de resíduos de disparos de armas de fogo por meio da técnica de espectrometria de massas de alta resolução com fonte de plasma indutivo Identification of gunshot residues by high resolution inductively coupled plasma mass spectrometry |
| title_fullStr | Identificação de resíduos de disparos de armas de fogo por meio da técnica de espectrometria de massas de alta resolução com fonte de plasma indutivo Identification of gunshot residues by high resolution inductively coupled plasma mass spectrometry |
| title_full_unstemmed | Identificação de resíduos de disparos de armas de fogo por meio da técnica de espectrometria de massas de alta resolução com fonte de plasma indutivo Identification of gunshot residues by high resolution inductively coupled plasma mass spectrometry |
| title_short | Identificação de resíduos de disparos de armas de fogo por meio da técnica de espectrometria de massas de alta resolução com fonte de plasma indutivo Identification of gunshot residues by high resolution inductively coupled plasma mass spectrometry |
| title_sort | identificacao de residuos de disparos de armas de fogo por meio da tecnica de espectrometria de massas de alta resolucao com fonte de plasma indutivo identification of gunshot residues by high resolution inductively coupled plasma mass spectrometry |
| topic | forensic science gunshot residues inductively coupled plasma-mass spectrometry |
| url | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422004000300009 |
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