Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBF

Laser powder bed fusion (LPBF) is a typical additive manufacturing technology that offers significant advantages in the production of complex components. With the rapid heating and cooling characteristics of LPBF, a large amount of solid solution of alloying elements in the matrix can be achieved to...

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Main Authors: Yuxian Lu, Hao Zhang, Peng Xue, Lihui Wu, Fengchao Liu, Luanluan Jia, Dingrui Ni, Bolv Xiao, Zongyi Ma
Format: Article
Language:English
Published: MDPI AG 2023-06-01
Series:Crystals
Subjects:
Online Access:https://www.mdpi.com/2073-4352/13/6/913
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author Yuxian Lu
Hao Zhang
Peng Xue
Lihui Wu
Fengchao Liu
Luanluan Jia
Dingrui Ni
Bolv Xiao
Zongyi Ma
author_facet Yuxian Lu
Hao Zhang
Peng Xue
Lihui Wu
Fengchao Liu
Luanluan Jia
Dingrui Ni
Bolv Xiao
Zongyi Ma
author_sort Yuxian Lu
collection DOAJ
description Laser powder bed fusion (LPBF) is a typical additive manufacturing technology that offers significant advantages in the production of complex components. With the rapid heating and cooling characteristics of LPBF, a large amount of solid solution of alloying elements in the matrix can be achieved to form supersaturated solid solutions, thus enhancing the properties of LPBF alloys. For the unique microstructure, the heat treatment process needs to be adjusted accordingly. In this work, a Zr/Sc-modified Al-Mg alloy processed by laser powder bed fusion (LPBF) with relatively low cost and good mechanical properties was investigated. The fine microstructure was obtained under rapid solidification conditions. The nanoscale Al<sub>3</sub>(Sc,Zr) particles precipitated at the molten pool boundary during solidification. These particles, as effective heterogeneous nucleators, further refined the α-Al grains and improved the mechanical properties of the alloy. As a result, the alloy exhibited a heterogeneous microstructure consisting of columnar grains in the center of the molten pool and equiaxed grains at the boundaries. The rapid solidification resulted in the supersaturation of solute atoms in the α-Al matrix, which significantly enhanced the solid solution strengthening effect. With the LPBF processing parameters of a combination of a laser power of 250 W, a laser scanning speed of 833 mm/s, and stripe scanning mode, the tensile strength of the alloy reached 401.4 ± 5.7 MPa, which was significantly higher than that of the cast alloys with aging treatment (281.1 ± 1.3 MPa). The heat treatment promoted the formation of secondary Al<sub>3</sub>(Sc,Zr), Mn/Mg-rich phases. The ultimate tensile strength and elongation at fracture after aging at 325 °C for 2 h were 536.0 ± 1.7 MPa and 14.8 ± 0.8%, respectively. The results provide insight into the preparation of aluminum alloys with relatively low cost and excellent mechanical properties.
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spelling doaj.art-402f8ceeddf0425c833ee2859f7378682023-11-18T09:56:30ZengMDPI AGCrystals2073-43522023-06-0113691310.3390/cryst13060913Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBFYuxian Lu0Hao Zhang1Peng Xue2Lihui Wu3Fengchao Liu4Luanluan Jia5Dingrui Ni6Bolv Xiao7Zongyi Ma8Shi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShandong Key Laboratory of Advanced Aluminum Materials and Technology, Binzhou Institute of Technology, Weiqiao—UCAS Science and Technology Park, Binzhou 256606, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaShi-changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, ChinaLaser powder bed fusion (LPBF) is a typical additive manufacturing technology that offers significant advantages in the production of complex components. With the rapid heating and cooling characteristics of LPBF, a large amount of solid solution of alloying elements in the matrix can be achieved to form supersaturated solid solutions, thus enhancing the properties of LPBF alloys. For the unique microstructure, the heat treatment process needs to be adjusted accordingly. In this work, a Zr/Sc-modified Al-Mg alloy processed by laser powder bed fusion (LPBF) with relatively low cost and good mechanical properties was investigated. The fine microstructure was obtained under rapid solidification conditions. The nanoscale Al<sub>3</sub>(Sc,Zr) particles precipitated at the molten pool boundary during solidification. These particles, as effective heterogeneous nucleators, further refined the α-Al grains and improved the mechanical properties of the alloy. As a result, the alloy exhibited a heterogeneous microstructure consisting of columnar grains in the center of the molten pool and equiaxed grains at the boundaries. The rapid solidification resulted in the supersaturation of solute atoms in the α-Al matrix, which significantly enhanced the solid solution strengthening effect. With the LPBF processing parameters of a combination of a laser power of 250 W, a laser scanning speed of 833 mm/s, and stripe scanning mode, the tensile strength of the alloy reached 401.4 ± 5.7 MPa, which was significantly higher than that of the cast alloys with aging treatment (281.1 ± 1.3 MPa). The heat treatment promoted the formation of secondary Al<sub>3</sub>(Sc,Zr), Mn/Mg-rich phases. The ultimate tensile strength and elongation at fracture after aging at 325 °C for 2 h were 536.0 ± 1.7 MPa and 14.8 ± 0.8%, respectively. The results provide insight into the preparation of aluminum alloys with relatively low cost and excellent mechanical properties.https://www.mdpi.com/2073-4352/13/6/913additive manufacturinglaser powder bed fusionAl-Mg-Sc-Zr alloyfine grain strengtheningsolution strengthening
spellingShingle Yuxian Lu
Hao Zhang
Peng Xue
Lihui Wu
Fengchao Liu
Luanluan Jia
Dingrui Ni
Bolv Xiao
Zongyi Ma
Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBF
Crystals
additive manufacturing
laser powder bed fusion
Al-Mg-Sc-Zr alloy
fine grain strengthening
solution strengthening
title Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBF
title_full Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBF
title_fullStr Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBF
title_full_unstemmed Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBF
title_short Microstructural Evaluation and Tensile Properties of Al-Mg-Sc-Zr Alloys Prepared by LPBF
title_sort microstructural evaluation and tensile properties of al mg sc zr alloys prepared by lpbf
topic additive manufacturing
laser powder bed fusion
Al-Mg-Sc-Zr alloy
fine grain strengthening
solution strengthening
url https://www.mdpi.com/2073-4352/13/6/913
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