Spatially Resolved Cross-Linking Characterization by Imaging Low-Coherence Interferometry

A method to characterize cross-linking differences in polymers such as waveguide polymers has been developed. The method is based on the scan-free information acquisition utilizing a low-coherence interferometer in conjunction with an imaging spectrometer. By the introduction of a novel analyzing al...

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Main Authors: Christopher Taudt, Bryan Nelsen, Elisabeth Rossegger, Sandra Schlögl, Edmund Koch, Peter Hartmann
Format: Article
Language:English
Published: MDPI AG 2019-03-01
Series:Sensors
Subjects:
Online Access:http://www.mdpi.com/1424-8220/19/5/1152
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author Christopher Taudt
Bryan Nelsen
Elisabeth Rossegger
Sandra Schlögl
Edmund Koch
Peter Hartmann
author_facet Christopher Taudt
Bryan Nelsen
Elisabeth Rossegger
Sandra Schlögl
Edmund Koch
Peter Hartmann
author_sort Christopher Taudt
collection DOAJ
description A method to characterize cross-linking differences in polymers such as waveguide polymers has been developed. The method is based on the scan-free information acquisition utilizing a low-coherence interferometer in conjunction with an imaging spectrometer. By the introduction of a novel analyzing algorithm, the recorded spectral-phase data was interpreted as wavelength-dependent optical thickness which is matchable with the refractive index and therefore with the degree of cross-linking. In the course of this work, the method was described in its hardware and algorithmic implementation as well as in its accuracy. Comparative measurements and error estimations showed an accuracy in the range of 10−6 in terms of the refractive index. Finally, photo-lithographically produced samples with laterally defined cross-linking differences have been characterized. It could be shown, that differences in the optical thickness of ±1.5 μm are distinguishable.
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spelling doaj.art-408c078851f7497aaec9e3357eea4aaa2022-12-22T02:54:30ZengMDPI AGSensors1424-82202019-03-01195115210.3390/s19051152s19051152Spatially Resolved Cross-Linking Characterization by Imaging Low-Coherence InterferometryChristopher Taudt0Bryan Nelsen1Elisabeth Rossegger2Sandra Schlögl3Edmund Koch4Peter Hartmann5Faculty of Physical Engineering/Computer Sciences, University of Applied Sciences Zwickau, D-08056 Zwickau, GermanyFaculty of Physical Engineering/Computer Sciences, University of Applied Sciences Zwickau, D-08056 Zwickau, GermanyPolymer Competence Center Leoben, AT-8700 Leoben, AustriaPolymer Competence Center Leoben, AT-8700 Leoben, AustriaFaculty of Electrical and Computer Engineering, Technical University Dresden, D-01307 Dresden, GermanyFaculty of Physical Engineering/Computer Sciences, University of Applied Sciences Zwickau, D-08056 Zwickau, GermanyA method to characterize cross-linking differences in polymers such as waveguide polymers has been developed. The method is based on the scan-free information acquisition utilizing a low-coherence interferometer in conjunction with an imaging spectrometer. By the introduction of a novel analyzing algorithm, the recorded spectral-phase data was interpreted as wavelength-dependent optical thickness which is matchable with the refractive index and therefore with the degree of cross-linking. In the course of this work, the method was described in its hardware and algorithmic implementation as well as in its accuracy. Comparative measurements and error estimations showed an accuracy in the range of 10−6 in terms of the refractive index. Finally, photo-lithographically produced samples with laterally defined cross-linking differences have been characterized. It could be shown, that differences in the optical thickness of ±1.5 μm are distinguishable.http://www.mdpi.com/1424-8220/19/5/1152interferometrycross-linking characterizationwhite-light interferometrydispersion-enhanced low-coherence interferometryphotoresistsemiconductor manufacturing
spellingShingle Christopher Taudt
Bryan Nelsen
Elisabeth Rossegger
Sandra Schlögl
Edmund Koch
Peter Hartmann
Spatially Resolved Cross-Linking Characterization by Imaging Low-Coherence Interferometry
Sensors
interferometry
cross-linking characterization
white-light interferometry
dispersion-enhanced low-coherence interferometry
photoresist
semiconductor manufacturing
title Spatially Resolved Cross-Linking Characterization by Imaging Low-Coherence Interferometry
title_full Spatially Resolved Cross-Linking Characterization by Imaging Low-Coherence Interferometry
title_fullStr Spatially Resolved Cross-Linking Characterization by Imaging Low-Coherence Interferometry
title_full_unstemmed Spatially Resolved Cross-Linking Characterization by Imaging Low-Coherence Interferometry
title_short Spatially Resolved Cross-Linking Characterization by Imaging Low-Coherence Interferometry
title_sort spatially resolved cross linking characterization by imaging low coherence interferometry
topic interferometry
cross-linking characterization
white-light interferometry
dispersion-enhanced low-coherence interferometry
photoresist
semiconductor manufacturing
url http://www.mdpi.com/1424-8220/19/5/1152
work_keys_str_mv AT christophertaudt spatiallyresolvedcrosslinkingcharacterizationbyimaginglowcoherenceinterferometry
AT bryannelsen spatiallyresolvedcrosslinkingcharacterizationbyimaginglowcoherenceinterferometry
AT elisabethrossegger spatiallyresolvedcrosslinkingcharacterizationbyimaginglowcoherenceinterferometry
AT sandraschlogl spatiallyresolvedcrosslinkingcharacterizationbyimaginglowcoherenceinterferometry
AT edmundkoch spatiallyresolvedcrosslinkingcharacterizationbyimaginglowcoherenceinterferometry
AT peterhartmann spatiallyresolvedcrosslinkingcharacterizationbyimaginglowcoherenceinterferometry