tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylate
The title compound, C13H23N3O4, was prepared starting from ethyl N-benzyl-3-oxopiperidine-4-carboxylate through a nine-step reaction, including hydrogenation, Boc (tert-butoxycarbonyl) protection, methylation, oximation, hydrolysis, esterification and ammonolysis. In the crystal structure, molecules...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2008-12-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536808036106 |
| _version_ | 1798030929851056128 |
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| author | Yucheng Wang Jue Cao Mingliang Liu Juxian Wang |
| author_facet | Yucheng Wang Jue Cao Mingliang Liu Juxian Wang |
| author_sort | Yucheng Wang |
| collection | DOAJ |
| description | The title compound, C13H23N3O4, was prepared starting from ethyl N-benzyl-3-oxopiperidine-4-carboxylate through a nine-step reaction, including hydrogenation, Boc (tert-butoxycarbonyl) protection, methylation, oximation, hydrolysis, esterification and ammonolysis. In the crystal structure, molecules are linked by intermolecular N—H...O hydrogen bonds to form a porous three-dimensional network with solvent-free hydrophobic channels extending along the c axis. |
| first_indexed | 2024-04-11T19:49:06Z |
| format | Article |
| id | doaj.art-417a9860decf40c4a9f4fe6023b74450 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-04-11T19:49:06Z |
| publishDate | 2008-12-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-417a9860decf40c4a9f4fe6023b744502022-12-22T04:06:22ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-12-016412o2294o229410.1107/S1600536808036106tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylateYucheng WangJue CaoMingliang LiuJuxian WangThe title compound, C13H23N3O4, was prepared starting from ethyl N-benzyl-3-oxopiperidine-4-carboxylate through a nine-step reaction, including hydrogenation, Boc (tert-butoxycarbonyl) protection, methylation, oximation, hydrolysis, esterification and ammonolysis. In the crystal structure, molecules are linked by intermolecular N—H...O hydrogen bonds to form a porous three-dimensional network with solvent-free hydrophobic channels extending along the c axis.http://scripts.iucr.org/cgi-bin/paper?S1600536808036106 |
| spellingShingle | Yucheng Wang Jue Cao Mingliang Liu Juxian Wang tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylate Acta Crystallographica Section E |
| title | tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylate |
| title_full | tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylate |
| title_fullStr | tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylate |
| title_full_unstemmed | tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylate |
| title_short | tert-Butyl 4-carbamoyl-3-methoxyimino-4-methylpiperidine-1-carboxylate |
| title_sort | tert butyl 4 carbamoyl 3 methoxyimino 4 methylpiperidine 1 carboxylate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536808036106 |
| work_keys_str_mv | AT yuchengwang tertbutyl4carbamoyl3methoxyimino4methylpiperidine1carboxylate AT juecao tertbutyl4carbamoyl3methoxyimino4methylpiperidine1carboxylate AT mingliangliu tertbutyl4carbamoyl3methoxyimino4methylpiperidine1carboxylate AT juxianwang tertbutyl4carbamoyl3methoxyimino4methylpiperidine1carboxylate |