Fabrication of porous alumina using a paraffin pore-forming agent for laser pump cavity applications

Abstract Paraffin was employed as a pore-forming agent to achieve porous alumina. Trichloroethylene, toluene, and chloroform were utilized for dissolving paraffin to explore the impact of the solvent on the properties of porous alumina. The influence of the paraffin ratio (1, 3, 5, and 7 wt%) was al...

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Main Authors: S. Afroushteh, F. Soleimani
Format: Article
Language:English
Published: Associação Brasileira de Cerâmica 2023-12-01
Series:Cerâmica
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132023000300181&tlng=en
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author S. Afroushteh
F. Soleimani
author_facet S. Afroushteh
F. Soleimani
author_sort S. Afroushteh
collection DOAJ
description Abstract Paraffin was employed as a pore-forming agent to achieve porous alumina. Trichloroethylene, toluene, and chloroform were utilized for dissolving paraffin to explore the impact of the solvent on the properties of porous alumina. The influence of the paraffin ratio (1, 3, 5, and 7 wt%) was also examined on the properties of porous alumina. The samples were compacted under different pressures ranging from 30 to 50 MPa. The samples were then sintered at 1400 °C. The density of the samples was examined by the Archimedes method. The porosity percentage depended on the content of the pore-forming agent and the initial pressure of the compaction process. Based on the X-ray diffraction results, the size of the crystallites was about 230 nm. The sample with 3 wt% paraffin showed the highest strength (155 MPa) which can be assigned to its proper pore size distribution. The distribution and size of the pores were investigated by a field emission scanning electron microscope. Finally, the sample prepared with 5 wt% paraffin in toluene and compacted at 40 MPa was utilized as a laser pump reflector in an Nd-YAG laser cavity. Based on the results, the reflection of the porous alumina was above 99% at the wavelength of 430 nm.
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spelling doaj.art-42905bb1034c4e6ea0a13754eeea4b042023-12-12T07:45:29ZengAssociação Brasileira de CerâmicaCerâmica1678-45532023-12-016939118118810.1590/0366-69132023693913449Fabrication of porous alumina using a paraffin pore-forming agent for laser pump cavity applicationsS. AfroushtehF. Soleimanihttps://orcid.org/0000-0003-0008-3400Abstract Paraffin was employed as a pore-forming agent to achieve porous alumina. Trichloroethylene, toluene, and chloroform were utilized for dissolving paraffin to explore the impact of the solvent on the properties of porous alumina. The influence of the paraffin ratio (1, 3, 5, and 7 wt%) was also examined on the properties of porous alumina. The samples were compacted under different pressures ranging from 30 to 50 MPa. The samples were then sintered at 1400 °C. The density of the samples was examined by the Archimedes method. The porosity percentage depended on the content of the pore-forming agent and the initial pressure of the compaction process. Based on the X-ray diffraction results, the size of the crystallites was about 230 nm. The sample with 3 wt% paraffin showed the highest strength (155 MPa) which can be assigned to its proper pore size distribution. The distribution and size of the pores were investigated by a field emission scanning electron microscope. Finally, the sample prepared with 5 wt% paraffin in toluene and compacted at 40 MPa was utilized as a laser pump reflector in an Nd-YAG laser cavity. Based on the results, the reflection of the porous alumina was above 99% at the wavelength of 430 nm.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132023000300181&tlng=enporous aluminapore-forminglaser cavity
spellingShingle S. Afroushteh
F. Soleimani
Fabrication of porous alumina using a paraffin pore-forming agent for laser pump cavity applications
Cerâmica
porous alumina
pore-forming
laser cavity
title Fabrication of porous alumina using a paraffin pore-forming agent for laser pump cavity applications
title_full Fabrication of porous alumina using a paraffin pore-forming agent for laser pump cavity applications
title_fullStr Fabrication of porous alumina using a paraffin pore-forming agent for laser pump cavity applications
title_full_unstemmed Fabrication of porous alumina using a paraffin pore-forming agent for laser pump cavity applications
title_short Fabrication of porous alumina using a paraffin pore-forming agent for laser pump cavity applications
title_sort fabrication of porous alumina using a paraffin pore forming agent for laser pump cavity applications
topic porous alumina
pore-forming
laser cavity
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0366-69132023000300181&tlng=en
work_keys_str_mv AT safroushteh fabricationofporousaluminausingaparaffinporeformingagentforlaserpumpcavityapplications
AT fsoleimani fabricationofporousaluminausingaparaffinporeformingagentforlaserpumpcavityapplications