N-Ethyl-2-[1-(2-hydroxynaphthalen-1-yl)ethylidene]hydrazinecarbothioamide
In the title compound, C15H17N3OS, the dihedral angle between the mean planes of the 2-hydroxynapthyl ring system and the hydrazinecarbothioamide group is 73.7 (3)°. In the crystal, weak O—H...S and C—H...O interactions and π–π stacking interactions involving one of the hydroxynapthyl rings with a c...
Main Authors: | , , |
---|---|
Format: | Article |
Language: | English |
Published: |
International Union of Crystallography
2014-06-01
|
Series: | Acta Crystallographica Section E |
Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536814012057 |
_version_ | 1798026914808463360 |
---|---|
author | Brian J. Anderson Zachary A. Shalit Jerry P. Jasinski |
author_facet | Brian J. Anderson Zachary A. Shalit Jerry P. Jasinski |
author_sort | Brian J. Anderson |
collection | DOAJ |
description | In the title compound, C15H17N3OS, the dihedral angle between the mean planes of the 2-hydroxynapthyl ring system and the hydrazinecarbothioamide group is 73.7 (3)°. In the crystal, weak O—H...S and C—H...O interactions and π–π stacking interactions involving one of the hydroxynapthyl rings with a centroid–centroid distance of 3.6648 (14) Å are observed, forming infinite chains along [010]. In addition, N—H...S interactions occur. |
first_indexed | 2024-04-11T18:42:51Z |
format | Article |
id | doaj.art-42d51b7a832148c7b818334ec2617629 |
institution | Directory Open Access Journal |
issn | 1600-5368 |
language | English |
last_indexed | 2024-04-11T18:42:51Z |
publishDate | 2014-06-01 |
publisher | International Union of Crystallography |
record_format | Article |
series | Acta Crystallographica Section E |
spelling | doaj.art-42d51b7a832148c7b818334ec26176292022-12-22T04:08:56ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682014-06-01706o732o73210.1107/S1600536814012057bt6981N-Ethyl-2-[1-(2-hydroxynaphthalen-1-yl)ethylidene]hydrazinecarbothioamideBrian J. Anderson0Zachary A. Shalit1Jerry P. Jasinski2Department of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USADepartment of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USADepartment of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USAIn the title compound, C15H17N3OS, the dihedral angle between the mean planes of the 2-hydroxynapthyl ring system and the hydrazinecarbothioamide group is 73.7 (3)°. In the crystal, weak O—H...S and C—H...O interactions and π–π stacking interactions involving one of the hydroxynapthyl rings with a centroid–centroid distance of 3.6648 (14) Å are observed, forming infinite chains along [010]. In addition, N—H...S interactions occur.http://scripts.iucr.org/cgi-bin/paper?S1600536814012057 |
spellingShingle | Brian J. Anderson Zachary A. Shalit Jerry P. Jasinski N-Ethyl-2-[1-(2-hydroxynaphthalen-1-yl)ethylidene]hydrazinecarbothioamide Acta Crystallographica Section E |
title | N-Ethyl-2-[1-(2-hydroxynaphthalen-1-yl)ethylidene]hydrazinecarbothioamide |
title_full | N-Ethyl-2-[1-(2-hydroxynaphthalen-1-yl)ethylidene]hydrazinecarbothioamide |
title_fullStr | N-Ethyl-2-[1-(2-hydroxynaphthalen-1-yl)ethylidene]hydrazinecarbothioamide |
title_full_unstemmed | N-Ethyl-2-[1-(2-hydroxynaphthalen-1-yl)ethylidene]hydrazinecarbothioamide |
title_short | N-Ethyl-2-[1-(2-hydroxynaphthalen-1-yl)ethylidene]hydrazinecarbothioamide |
title_sort | n ethyl 2 1 2 hydroxynaphthalen 1 yl ethylidene hydrazinecarbothioamide |
url | http://scripts.iucr.org/cgi-bin/paper?S1600536814012057 |
work_keys_str_mv | AT brianjanderson nethyl212hydroxynaphthalen1ylethylidenehydrazinecarbothioamide AT zacharyashalit nethyl212hydroxynaphthalen1ylethylidenehydrazinecarbothioamide AT jerrypjasinski nethyl212hydroxynaphthalen1ylethylidenehydrazinecarbothioamide |