Image-Based Analysis of Dense Particle Mixtures via Mask R-CNN

Powders and their mixtures are elemental for many industries (e.g., food, pharmaceutical, mining, agricultural, and chemical). The properties of the manufactured products are often directly linked to the particle properties (e.g., particle size and shape distribution) of the utilized powder mixtures...

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Main Authors: Max Frei, Frank Einar Kruis
Format: Article
Language:English
Published: MDPI AG 2022-01-01
Series:Eng
Subjects:
Online Access:https://www.mdpi.com/2673-4117/3/1/7
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author Max Frei
Frank Einar Kruis
author_facet Max Frei
Frank Einar Kruis
author_sort Max Frei
collection DOAJ
description Powders and their mixtures are elemental for many industries (e.g., food, pharmaceutical, mining, agricultural, and chemical). The properties of the manufactured products are often directly linked to the particle properties (e.g., particle size and shape distribution) of the utilized powder mixtures. The most straightforward approach to acquire information concerning these particle properties is image capturing. However, the analysis of the resulting images often requires manual labor and is therefore time-consuming and costly. Therefore, the work at hand evaluates the suitability of Mask R-CNN—one of the best-known deep learning architectures for object detection—for the fully automated image-based analysis of particle mixtures, by comparing it to a conventional, i.e., not machine learning-based, image analysis method, as well as the results of a trifold manual analysis. To avoid the need of a laborious manual annotation, the training data required by Mask R-CNN are produced via image synthesis. As an example for an industrially relevant particle mixture, endoscopic images from a fluid catalytic cracking reactor are used as a test case for the evaluation of the tested methods. According to the results of the evaluation, Mask R-CNN is a well-suited method for the fully automatic image-based analysis of particle mixtures. It allows for the detection and classification of particles with an accuracy of <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mn>42.7</mn></mrow></semantics></math></inline-formula>% for the utilized data, as well as the characterization of the particle shape. Also, it enables the measurement of the mixture component particle size distributions with errors (relative to the manual reference) as low as <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo>−</mo><mn>2</mn><mo>±</mo><mn>5</mn></mrow></semantics></math></inline-formula> for the geometric mean diameter and <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo>−</mo><mn>6</mn><mo>±</mo><mn>5</mn><mo>%</mo></mrow></semantics></math></inline-formula> for the geometric standard deviation of the <i>dark</i> particle class of the utilized data, as well as <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo>−</mo><mn>8</mn><mo>±</mo><mn>4</mn><mo>%</mo></mrow></semantics></math></inline-formula> for the geometric mean diameter and <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo>−</mo><mn>6</mn><mo>±</mo><mn>2</mn><mo>%</mo></mrow></semantics></math></inline-formula> for the geometric standard deviation of the <i>light</i> particle class of the utilized data. Source code, as well as training, validation, and test data publicly available.
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spelling doaj.art-436b304e7c56421897fe6ea4cc82805c2023-11-30T21:04:14ZengMDPI AGEng2673-41172022-01-0131789810.3390/eng3010007Image-Based Analysis of Dense Particle Mixtures via Mask R-CNNMax Frei0Frank Einar Kruis1Institute of Technology for Nanostructures (NST) and Center for Nanointegration Duisburg-Essen (CENIDE), University of Duisburg-Essen, D-47057 Duisburg, GermanyInstitute of Technology for Nanostructures (NST) and Center for Nanointegration Duisburg-Essen (CENIDE), University of Duisburg-Essen, D-47057 Duisburg, GermanyPowders and their mixtures are elemental for many industries (e.g., food, pharmaceutical, mining, agricultural, and chemical). The properties of the manufactured products are often directly linked to the particle properties (e.g., particle size and shape distribution) of the utilized powder mixtures. The most straightforward approach to acquire information concerning these particle properties is image capturing. However, the analysis of the resulting images often requires manual labor and is therefore time-consuming and costly. Therefore, the work at hand evaluates the suitability of Mask R-CNN—one of the best-known deep learning architectures for object detection—for the fully automated image-based analysis of particle mixtures, by comparing it to a conventional, i.e., not machine learning-based, image analysis method, as well as the results of a trifold manual analysis. To avoid the need of a laborious manual annotation, the training data required by Mask R-CNN are produced via image synthesis. As an example for an industrially relevant particle mixture, endoscopic images from a fluid catalytic cracking reactor are used as a test case for the evaluation of the tested methods. According to the results of the evaluation, Mask R-CNN is a well-suited method for the fully automatic image-based analysis of particle mixtures. It allows for the detection and classification of particles with an accuracy of <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mn>42.7</mn></mrow></semantics></math></inline-formula>% for the utilized data, as well as the characterization of the particle shape. Also, it enables the measurement of the mixture component particle size distributions with errors (relative to the manual reference) as low as <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo>−</mo><mn>2</mn><mo>±</mo><mn>5</mn></mrow></semantics></math></inline-formula> for the geometric mean diameter and <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo>−</mo><mn>6</mn><mo>±</mo><mn>5</mn><mo>%</mo></mrow></semantics></math></inline-formula> for the geometric standard deviation of the <i>dark</i> particle class of the utilized data, as well as <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo>−</mo><mn>8</mn><mo>±</mo><mn>4</mn><mo>%</mo></mrow></semantics></math></inline-formula> for the geometric mean diameter and <inline-formula><math xmlns="http://www.w3.org/1998/Math/MathML" display="inline"><semantics><mrow><mo>−</mo><mn>6</mn><mo>±</mo><mn>2</mn><mo>%</mo></mrow></semantics></math></inline-formula> for the geometric standard deviation of the <i>light</i> particle class of the utilized data. Source code, as well as training, validation, and test data publicly available.https://www.mdpi.com/2673-4117/3/1/7imaging particle analysisfluid catalytic crackingautomatic particle mixture analysisMask R-CNNimage synthesisHough transform
spellingShingle Max Frei
Frank Einar Kruis
Image-Based Analysis of Dense Particle Mixtures via Mask R-CNN
Eng
imaging particle analysis
fluid catalytic cracking
automatic particle mixture analysis
Mask R-CNN
image synthesis
Hough transform
title Image-Based Analysis of Dense Particle Mixtures via Mask R-CNN
title_full Image-Based Analysis of Dense Particle Mixtures via Mask R-CNN
title_fullStr Image-Based Analysis of Dense Particle Mixtures via Mask R-CNN
title_full_unstemmed Image-Based Analysis of Dense Particle Mixtures via Mask R-CNN
title_short Image-Based Analysis of Dense Particle Mixtures via Mask R-CNN
title_sort image based analysis of dense particle mixtures via mask r cnn
topic imaging particle analysis
fluid catalytic cracking
automatic particle mixture analysis
Mask R-CNN
image synthesis
Hough transform
url https://www.mdpi.com/2673-4117/3/1/7
work_keys_str_mv AT maxfrei imagebasedanalysisofdenseparticlemixturesviamaskrcnn
AT frankeinarkruis imagebasedanalysisofdenseparticlemixturesviamaskrcnn