Molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samples

Phenolic environmental estrogens (PEEs) are representative of environmental estrogens, which are commonly known as bisphenol, alkyl phenols, triazine herbicides, and non-steroidal estrogens such as diethylstilbestrol. Diethylstilbestrol is on the list of drugs and other compounds prohibited in food...

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Main Authors: Zhao Xuan, Rong Fei
Format: Article
Language:English
Published: EDP Sciences 2023-01-01
Series:E3S Web of Conferences
Online Access:https://www.e3s-conferences.org/articles/e3sconf/pdf/2023/30/e3sconf_eppct2023_01014.pdf
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author Zhao Xuan
Rong Fei
author_facet Zhao Xuan
Rong Fei
author_sort Zhao Xuan
collection DOAJ
description Phenolic environmental estrogens (PEEs) are representative of environmental estrogens, which are commonly known as bisphenol, alkyl phenols, triazine herbicides, and non-steroidal estrogens such as diethylstilbestrol. Diethylstilbestrol is on the list of drugs and other compounds prohibited in food animals. Therefore, the control of its illegal use has become a very urgent problem, and it is very necessary to analyze the estrogen residue in environmental water samples. In this study, molecularly imprinted nanofiber membrane was prepared by electrospinning, and samples were pre-treated with solid phase extraction technology, which was applied to the detection of estrostilbestrol in the environment. For the detection degree of diethylstilbestrol in different water samples, the recovery rate of molecularly imprinted nanofibers was significantly higher than that of blank nanofibers and C18 column. The combination of molecular imprinting and solid phase extraction is effective for the enrichment of trace substances. This study provides an effective method for screening and identification of estrogen in environmental water samples, and further improves the accuracy of detection of corresponding estrogen.
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spelling doaj.art-4373b38f75324aec9b87b960ff5d18c42023-06-09T09:12:43ZengEDP SciencesE3S Web of Conferences2267-12422023-01-013930101410.1051/e3sconf/202339301014e3sconf_eppct2023_01014Molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samplesZhao Xuan0Rong Fei1School of Biological Sciences and Medical Engineering, Southeast UniversitySchool of Biological Sciences and Medical Engineering, Southeast UniversityPhenolic environmental estrogens (PEEs) are representative of environmental estrogens, which are commonly known as bisphenol, alkyl phenols, triazine herbicides, and non-steroidal estrogens such as diethylstilbestrol. Diethylstilbestrol is on the list of drugs and other compounds prohibited in food animals. Therefore, the control of its illegal use has become a very urgent problem, and it is very necessary to analyze the estrogen residue in environmental water samples. In this study, molecularly imprinted nanofiber membrane was prepared by electrospinning, and samples were pre-treated with solid phase extraction technology, which was applied to the detection of estrostilbestrol in the environment. For the detection degree of diethylstilbestrol in different water samples, the recovery rate of molecularly imprinted nanofibers was significantly higher than that of blank nanofibers and C18 column. The combination of molecular imprinting and solid phase extraction is effective for the enrichment of trace substances. This study provides an effective method for screening and identification of estrogen in environmental water samples, and further improves the accuracy of detection of corresponding estrogen.https://www.e3s-conferences.org/articles/e3sconf/pdf/2023/30/e3sconf_eppct2023_01014.pdf
spellingShingle Zhao Xuan
Rong Fei
Molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samples
E3S Web of Conferences
title Molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samples
title_full Molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samples
title_fullStr Molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samples
title_full_unstemmed Molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samples
title_short Molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samples
title_sort molecular imprinted solid phase extraction combined with determination of diethylstilbestrol in environmental water samples
url https://www.e3s-conferences.org/articles/e3sconf/pdf/2023/30/e3sconf_eppct2023_01014.pdf
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AT rongfei molecularimprintedsolidphaseextractioncombinedwithdeterminationofdiethylstilbestrolinenvironmentalwatersamples