Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applications

The alloy 21-6-9 is a nitrogen-strengthened austenitic stainless steel often used in aerospace applications due to its high strength, good fabrication properties, and toughness at cryogenic temperatures. However, minimal research has been conducted on alloy 21-6-9 using the additive manufacturing pr...

Full description

Bibliographic Details
Main Authors: Pragya Mishra, Pia Åkerfeldt, Fredrik Svahn, Erik Nilsson, Farnoosh Forouzan, Marta-Lena Antti
Format: Article
Language:English
Published: Elsevier 2023-07-01
Series:Journal of Materials Research and Technology
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2238785423012954
_version_ 1797745247152766976
author Pragya Mishra
Pia Åkerfeldt
Fredrik Svahn
Erik Nilsson
Farnoosh Forouzan
Marta-Lena Antti
author_facet Pragya Mishra
Pia Åkerfeldt
Fredrik Svahn
Erik Nilsson
Farnoosh Forouzan
Marta-Lena Antti
author_sort Pragya Mishra
collection DOAJ
description The alloy 21-6-9 is a nitrogen-strengthened austenitic stainless steel often used in aerospace applications due to its high strength, good fabrication properties, and toughness at cryogenic temperatures. However, minimal research has been conducted on alloy 21-6-9 using the additive manufacturing process laser powder-bed fusion (L-PBF). The L-PBF technique has been seen as a key to reducing production time and avoiding costly machining. Therefore, there is an interest in investigating L-PBF-processed 21-6-9 to determine the effects of L-PBF on properties at elevated and cryogenic temperatures. In this study, prior to tensile testing the alloy 21-6-9 underwent heat treatments that simulated aerospace applications and the alloy was analyzed and characterized to evaluate phase stability. The effects of elevated and cryogenic temperatures (77 K) on the tensile behavior and microstructure were investigated using X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). The tensile tests showed that the yield strength and ultimate tensile strength improved, while ductility varied depending on the conditions and test environment. The ultimate tensile strength was approximately 80% higher at 77 K than at room temperature, although the elongation decreased by around 90%, possibly due to the formation of strain-induced martensite.
first_indexed 2024-03-12T15:20:39Z
format Article
id doaj.art-451fa39ffbad4dfe983e6804857df4b4
institution Directory Open Access Journal
issn 2238-7854
language English
last_indexed 2024-03-12T15:20:39Z
publishDate 2023-07-01
publisher Elsevier
record_format Article
series Journal of Materials Research and Technology
spelling doaj.art-451fa39ffbad4dfe983e6804857df4b42023-08-11T05:33:22ZengElsevierJournal of Materials Research and Technology2238-78542023-07-012514831494Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applicationsPragya Mishra0Pia Åkerfeldt1Fredrik Svahn2Erik Nilsson3Farnoosh Forouzan4Marta-Lena Antti5Materials Science, Department of Engineering Sciences and Mathematics, Luleå University of Technology, 97187 Luleå, Sweden; Corresponding author.Materials Science, Department of Engineering Sciences and Mathematics, Luleå University of Technology, 97187 Luleå, SwedenGKN Aerospace Sweden AB, 46130 Trollhättan, SwedenMaterials Science, Department of Engineering Sciences and Mathematics, Luleå University of Technology, 97187 Luleå, SwedenMaterials Science, Department of Engineering Sciences and Mathematics, Luleå University of Technology, 97187 Luleå, Sweden; Höganäs AB, 263 39 Höganäs, SwedenMaterials Science, Department of Engineering Sciences and Mathematics, Luleå University of Technology, 97187 Luleå, SwedenThe alloy 21-6-9 is a nitrogen-strengthened austenitic stainless steel often used in aerospace applications due to its high strength, good fabrication properties, and toughness at cryogenic temperatures. However, minimal research has been conducted on alloy 21-6-9 using the additive manufacturing process laser powder-bed fusion (L-PBF). The L-PBF technique has been seen as a key to reducing production time and avoiding costly machining. Therefore, there is an interest in investigating L-PBF-processed 21-6-9 to determine the effects of L-PBF on properties at elevated and cryogenic temperatures. In this study, prior to tensile testing the alloy 21-6-9 underwent heat treatments that simulated aerospace applications and the alloy was analyzed and characterized to evaluate phase stability. The effects of elevated and cryogenic temperatures (77 K) on the tensile behavior and microstructure were investigated using X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). The tensile tests showed that the yield strength and ultimate tensile strength improved, while ductility varied depending on the conditions and test environment. The ultimate tensile strength was approximately 80% higher at 77 K than at room temperature, although the elongation decreased by around 90%, possibly due to the formation of strain-induced martensite.http://www.sciencedirect.com/science/article/pii/S2238785423012954L-PBF21-6-9 stainless steelElevated temperatureCryogenic temperatureMicrostructural characterizationMechanical properties
spellingShingle Pragya Mishra
Pia Åkerfeldt
Fredrik Svahn
Erik Nilsson
Farnoosh Forouzan
Marta-Lena Antti
Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applications
Journal of Materials Research and Technology
L-PBF
21-6-9 stainless steel
Elevated temperature
Cryogenic temperature
Microstructural characterization
Mechanical properties
title Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applications
title_full Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applications
title_fullStr Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applications
title_full_unstemmed Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applications
title_short Microstructural characterization and mechanical properties of additively manufactured 21-6-9 stainless steel for aerospace applications
title_sort microstructural characterization and mechanical properties of additively manufactured 21 6 9 stainless steel for aerospace applications
topic L-PBF
21-6-9 stainless steel
Elevated temperature
Cryogenic temperature
Microstructural characterization
Mechanical properties
url http://www.sciencedirect.com/science/article/pii/S2238785423012954
work_keys_str_mv AT pragyamishra microstructuralcharacterizationandmechanicalpropertiesofadditivelymanufactured2169stainlesssteelforaerospaceapplications
AT piaakerfeldt microstructuralcharacterizationandmechanicalpropertiesofadditivelymanufactured2169stainlesssteelforaerospaceapplications
AT fredriksvahn microstructuralcharacterizationandmechanicalpropertiesofadditivelymanufactured2169stainlesssteelforaerospaceapplications
AT eriknilsson microstructuralcharacterizationandmechanicalpropertiesofadditivelymanufactured2169stainlesssteelforaerospaceapplications
AT farnooshforouzan microstructuralcharacterizationandmechanicalpropertiesofadditivelymanufactured2169stainlesssteelforaerospaceapplications
AT martalenaantti microstructuralcharacterizationandmechanicalpropertiesofadditivelymanufactured2169stainlesssteelforaerospaceapplications