Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer

Depth sensing indentation holds the promise of local mechanical properties determination. However, the number of studies on materials that exhibit time-dependent and hydrostatic pressure-dependent behavior is still scarce. This paper aims to understand the effect of loading strain rate on the nano-i...

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Main Authors: Laura Alejandra Fasce, Lucas Sánchez Fellay, Patricia María Frontini
Format: Article
Language:English
Published: Budapest University of Technology 2023-06-01
Series:eXPRESS Polymer Letters
Subjects:
Online Access:http://www.expresspolymlett.com/letolt.php?file=EPL-0012327&mi=cd
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author Laura Alejandra Fasce
Lucas Sánchez Fellay
Patricia María Frontini
author_facet Laura Alejandra Fasce
Lucas Sánchez Fellay
Patricia María Frontini
author_sort Laura Alejandra Fasce
collection DOAJ
description Depth sensing indentation holds the promise of local mechanical properties determination. However, the number of studies on materials that exhibit time-dependent and hydrostatic pressure-dependent behavior is still scarce. This paper aims to understand the effect of loading strain rate on the nano-indentation response of an aerospace epoxy resin by combining physical measurements and numerical simulations. Physical nano-indentation tests were carried out using a Berkovich indenter at different constant loading strain rates (0.01 to 1.25 s–1). It was observed that as the loading strain rate increases, the penetration displacement at which the target load is reached decreases while the maximum displacement attained at the end of the load-hold period increases. The indentation response was numerically simulated to get insight into the phenomenon by finite element analysis. The polymer behavior was described by a nine-parameter elastic-viscoplastic constitutive model (EVP-9). Constitutive parameters were calibrated from uniaxial tensile and compression experimental data. Simulations agreed reasonably well with physical experiments being able to reproduce the loading strain rate effect observed in physical nano-indentation tests.
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spelling doaj.art-458feb5d735646649ac3069fd3f856c82023-04-03T09:32:16ZengBudapest University of TechnologyeXPRESS Polymer Letters1788-618X2023-06-0117664765910.3144/expresspolymlett.2023.47Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymerLaura Alejandra FasceLucas Sánchez FellayPatricia María FrontiniDepth sensing indentation holds the promise of local mechanical properties determination. However, the number of studies on materials that exhibit time-dependent and hydrostatic pressure-dependent behavior is still scarce. This paper aims to understand the effect of loading strain rate on the nano-indentation response of an aerospace epoxy resin by combining physical measurements and numerical simulations. Physical nano-indentation tests were carried out using a Berkovich indenter at different constant loading strain rates (0.01 to 1.25 s–1). It was observed that as the loading strain rate increases, the penetration displacement at which the target load is reached decreases while the maximum displacement attained at the end of the load-hold period increases. The indentation response was numerically simulated to get insight into the phenomenon by finite element analysis. The polymer behavior was described by a nine-parameter elastic-viscoplastic constitutive model (EVP-9). Constitutive parameters were calibrated from uniaxial tensile and compression experimental data. Simulations agreed reasonably well with physical experiments being able to reproduce the loading strain rate effect observed in physical nano-indentation tests.http://www.expresspolymlett.com/letolt.php?file=EPL-0012327&mi=cdmaterial testingthermosetting resinsnanoindentationmodelling and simulationmechanical properties
spellingShingle Laura Alejandra Fasce
Lucas Sánchez Fellay
Patricia María Frontini
Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
eXPRESS Polymer Letters
material testing
thermosetting resins
nanoindentation
modelling and simulation
mechanical properties
title Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_full Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_fullStr Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_full_unstemmed Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_short Effect of loading strain rate on nano-indentation response of an aerospace grade epoxy polymer
title_sort effect of loading strain rate on nano indentation response of an aerospace grade epoxy polymer
topic material testing
thermosetting resins
nanoindentation
modelling and simulation
mechanical properties
url http://www.expresspolymlett.com/letolt.php?file=EPL-0012327&mi=cd
work_keys_str_mv AT lauraalejandrafasce effectofloadingstrainrateonnanoindentationresponseofanaerospacegradeepoxypolymer
AT lucassanchezfellay effectofloadingstrainrateonnanoindentationresponseofanaerospacegradeepoxypolymer
AT patriciamariafrontini effectofloadingstrainrateonnanoindentationresponseofanaerospacegradeepoxypolymer