Analysis of Volatile Compounds in Processed Cream Cheese Models for the Prediction of “Fresh Cream” Aroma Perception

Controlling flavor perception by analyzing volatile and taste compounds is a key challenge for food industries, as flavor is the result of a complex mix of components. Machine-learning methodologies are already used to predict odor perception, but they are used to a lesser extent to predict aroma pe...

Full description

Bibliographic Details
Main Authors: Coline Caille, Mariem Boukraâ, Cécile Rannou, Angélique Villière, Clément Catanéo, Laurent Lethuaut, Araceli Lagadec-Marquez, Julia Bechaux, Carole Prost
Format: Article
Language:English
Published: MDPI AG 2023-10-01
Series:Molecules
Subjects:
Online Access:https://www.mdpi.com/1420-3049/28/20/7224
_version_ 1797572766308761600
author Coline Caille
Mariem Boukraâ
Cécile Rannou
Angélique Villière
Clément Catanéo
Laurent Lethuaut
Araceli Lagadec-Marquez
Julia Bechaux
Carole Prost
author_facet Coline Caille
Mariem Boukraâ
Cécile Rannou
Angélique Villière
Clément Catanéo
Laurent Lethuaut
Araceli Lagadec-Marquez
Julia Bechaux
Carole Prost
author_sort Coline Caille
collection DOAJ
description Controlling flavor perception by analyzing volatile and taste compounds is a key challenge for food industries, as flavor is the result of a complex mix of components. Machine-learning methodologies are already used to predict odor perception, but they are used to a lesser extent to predict aroma perception. The objectives of this work were, for the processed cream cheese models studied, to (1) analyze the impact of the composition and process on the sensory perception and VOC release and (2) predict “fresh cream” aroma perception from the VOC characteristics. Sixteen processed cream cheese models were produced according to a three-factor experimental design: the texturing agent type (κ-carrageenan, agar-agar) and level and the heating time. A R-A-T-A test on 59 consumers was carried out to describe the sensory perception of the cheese models. VOC release from the cheese model boli during swallowing was investigated with an in vitro masticator (Oniris device patent), followed by HS-SPME-GC-(ToF)MS analysis. Regression trees and random forests were used to predict “fresh cream” aroma perception, i.e., one of the main drivers of liking of processed cheeses, from the VOC release during swallowing. Agar-agar cheese models were perceived as having a “milk” odor and favored the release of a greater number of VOCs; κ-carrageenan samples were perceived as having a “granular” and “brittle” texture and a “salty” and “sour” taste and displayed a VOC retention capacity. Heating induced firmer cheese models and promoted Maillard VOCs responsible for “cooked” and “chemical” aroma perceptions. Octa-3,5-dien-2-one and octane-2,3-dione were the two main VOCs that contributed positively to the “fresh cream” aroma perception. Thus, regression trees and random forests are powerful statistical tools to provide a first insight into predicting the aroma of cheese models based on VOC characteristics.
first_indexed 2024-03-10T21:00:31Z
format Article
id doaj.art-45e9ae85ac5645f298b12154b9095be7
institution Directory Open Access Journal
issn 1420-3049
language English
last_indexed 2024-03-10T21:00:31Z
publishDate 2023-10-01
publisher MDPI AG
record_format Article
series Molecules
spelling doaj.art-45e9ae85ac5645f298b12154b9095be72023-11-19T17:34:33ZengMDPI AGMolecules1420-30492023-10-012820722410.3390/molecules28207224Analysis of Volatile Compounds in Processed Cream Cheese Models for the Prediction of “Fresh Cream” Aroma PerceptionColine Caille0Mariem Boukraâ1Cécile Rannou2Angélique Villière3Clément Catanéo4Laurent Lethuaut5Araceli Lagadec-Marquez6Julia Bechaux7Carole Prost8Oniris—UMR CNRS 6144 GEPEA—MA(PS)2/USC INRAE 1498 TRANSFORM, 44322 Nantes, FranceOniris—UMR CNRS 6144 GEPEA—MA(PS)2/USC INRAE 1498 TRANSFORM, 44322 Nantes, FranceOniris—UMR CNRS 6144 GEPEA—MA(PS)2/USC INRAE 1498 TRANSFORM, 44322 Nantes, FranceOniris—UMR CNRS 6144 GEPEA—MA(PS)2/USC INRAE 1498 TRANSFORM, 44322 Nantes, FranceOniris—UMR CNRS 6144 GEPEA—MA(PS)2/USC INRAE 1498 TRANSFORM, 44322 Nantes, FranceOniris—UMR CNRS 6144 GEPEA—MA(PS)2/USC INRAE 1498 TRANSFORM, 44322 Nantes, FranceBel Group—Bio-Engineering Team, 41100 Vendôme, FranceBel Group—Bio-Engineering Team, 41100 Vendôme, FranceOniris—UMR CNRS 6144 GEPEA—MA(PS)2/USC INRAE 1498 TRANSFORM, 44322 Nantes, FranceControlling flavor perception by analyzing volatile and taste compounds is a key challenge for food industries, as flavor is the result of a complex mix of components. Machine-learning methodologies are already used to predict odor perception, but they are used to a lesser extent to predict aroma perception. The objectives of this work were, for the processed cream cheese models studied, to (1) analyze the impact of the composition and process on the sensory perception and VOC release and (2) predict “fresh cream” aroma perception from the VOC characteristics. Sixteen processed cream cheese models were produced according to a three-factor experimental design: the texturing agent type (κ-carrageenan, agar-agar) and level and the heating time. A R-A-T-A test on 59 consumers was carried out to describe the sensory perception of the cheese models. VOC release from the cheese model boli during swallowing was investigated with an in vitro masticator (Oniris device patent), followed by HS-SPME-GC-(ToF)MS analysis. Regression trees and random forests were used to predict “fresh cream” aroma perception, i.e., one of the main drivers of liking of processed cheeses, from the VOC release during swallowing. Agar-agar cheese models were perceived as having a “milk” odor and favored the release of a greater number of VOCs; κ-carrageenan samples were perceived as having a “granular” and “brittle” texture and a “salty” and “sour” taste and displayed a VOC retention capacity. Heating induced firmer cheese models and promoted Maillard VOCs responsible for “cooked” and “chemical” aroma perceptions. Octa-3,5-dien-2-one and octane-2,3-dione were the two main VOCs that contributed positively to the “fresh cream” aroma perception. Thus, regression trees and random forests are powerful statistical tools to provide a first insight into predicting the aroma of cheese models based on VOC characteristics.https://www.mdpi.com/1420-3049/28/20/7224processed cream cheese modelsĸ-carrageenanagar-agarvolatile compound releasesensory analysisrate all that apply
spellingShingle Coline Caille
Mariem Boukraâ
Cécile Rannou
Angélique Villière
Clément Catanéo
Laurent Lethuaut
Araceli Lagadec-Marquez
Julia Bechaux
Carole Prost
Analysis of Volatile Compounds in Processed Cream Cheese Models for the Prediction of “Fresh Cream” Aroma Perception
Molecules
processed cream cheese models
ĸ-carrageenan
agar-agar
volatile compound release
sensory analysis
rate all that apply
title Analysis of Volatile Compounds in Processed Cream Cheese Models for the Prediction of “Fresh Cream” Aroma Perception
title_full Analysis of Volatile Compounds in Processed Cream Cheese Models for the Prediction of “Fresh Cream” Aroma Perception
title_fullStr Analysis of Volatile Compounds in Processed Cream Cheese Models for the Prediction of “Fresh Cream” Aroma Perception
title_full_unstemmed Analysis of Volatile Compounds in Processed Cream Cheese Models for the Prediction of “Fresh Cream” Aroma Perception
title_short Analysis of Volatile Compounds in Processed Cream Cheese Models for the Prediction of “Fresh Cream” Aroma Perception
title_sort analysis of volatile compounds in processed cream cheese models for the prediction of fresh cream aroma perception
topic processed cream cheese models
ĸ-carrageenan
agar-agar
volatile compound release
sensory analysis
rate all that apply
url https://www.mdpi.com/1420-3049/28/20/7224
work_keys_str_mv AT colinecaille analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception
AT mariemboukraa analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception
AT cecilerannou analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception
AT angeliquevilliere analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception
AT clementcataneo analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception
AT laurentlethuaut analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception
AT aracelilagadecmarquez analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception
AT juliabechaux analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception
AT caroleprost analysisofvolatilecompoundsinprocessedcreamcheesemodelsforthepredictionoffreshcreamaromaperception