A PRELIMINARY INVESTIGATION OF POLYANILINE/CHITOSAN COMPOSITE’S PHYSICOCHEMICAL PROPERTIES AND POTENTIAL ELECTROCHEMICAL APPLICATION
A polyaniline/chitosan (PANI/CHT) modified SPCE based sensor was developed and validated by electrochemical detection of PFOA. The PANI/CHT composite was synthesized by chemical oxidative polymerization technique. The synthesized material was characterized by scanning electron microscope (SEM)-Energ...
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Format: | Article |
Language: | English |
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Universiti Teknologi MARA, Negeri Sembilan
2022-10-01
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Series: | Journal of Academia |
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Online Access: | https://myjms.mohe.gov.my/index.php/joa/article/view/19146 |
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author | NUR FARAHIN SUHAIMI Siti Nor Atika Baharin Nurul' Ain Jamion Kavirajaa Pandian Sambasevam |
author_facet | NUR FARAHIN SUHAIMI Siti Nor Atika Baharin Nurul' Ain Jamion Kavirajaa Pandian Sambasevam |
author_sort | NUR FARAHIN SUHAIMI |
collection | DOAJ |
description | A polyaniline/chitosan (PANI/CHT) modified SPCE based sensor was developed and validated by electrochemical detection of PFOA. The PANI/CHT composite was synthesized by chemical oxidative polymerization technique. The synthesized material was characterized by scanning electron microscope (SEM)-Energy dispersive X-ray spectroscopy (EDX), Thermal gravimetric analysis (TGA) and Ultraviolet visible Spectroscopy (UV-Vis) techniques. The redox properties of the modified SPCE were examined by cyclic voltammetry studies. The investigation showed that PANI/CHT SPCE exhibit high electroactive surface area compared to unmodified SPCE. The PANI/CHT SPCE recorded lowest detection limit (LOD) of 1.60 ppb with LOQ of 4.82 ppb, in the linear range of 25-50 ppb. |
first_indexed | 2024-04-11T16:26:52Z |
format | Article |
id | doaj.art-463fd69dace246518b3ede031bd6efb2 |
institution | Directory Open Access Journal |
issn | 2289-6368 |
language | English |
last_indexed | 2024-04-24T08:01:26Z |
publishDate | 2022-10-01 |
publisher | Universiti Teknologi MARA, Negeri Sembilan |
record_format | Article |
series | Journal of Academia |
spelling | doaj.art-463fd69dace246518b3ede031bd6efb22024-04-17T16:36:03ZengUniversiti Teknologi MARA, Negeri SembilanJournal of Academia2289-63682022-10-01102175186A PRELIMINARY INVESTIGATION OF POLYANILINE/CHITOSAN COMPOSITE’S PHYSICOCHEMICAL PROPERTIES AND POTENTIAL ELECTROCHEMICAL APPLICATIONNUR FARAHIN SUHAIMI 0Siti Nor Atika Baharin 1Nurul' Ain Jamion 2Kavirajaa Pandian Sambasevam 3UNIVERSITI TEKNOLOGI MARA (UiTM ), kampus kuala pilah,72000 kuala pilah, negeri sembilanUITM CAWANGAN NEGERI SEMBILAN, KAMPUS KUALA PILAHUITM CAWANGAN NEGERI SEMBILAN, KAMPUS KUALA PILAHUITM CAWANGAN NEGERI SEMBILAN, KAMPUS KUALA PILAHA polyaniline/chitosan (PANI/CHT) modified SPCE based sensor was developed and validated by electrochemical detection of PFOA. The PANI/CHT composite was synthesized by chemical oxidative polymerization technique. The synthesized material was characterized by scanning electron microscope (SEM)-Energy dispersive X-ray spectroscopy (EDX), Thermal gravimetric analysis (TGA) and Ultraviolet visible Spectroscopy (UV-Vis) techniques. The redox properties of the modified SPCE were examined by cyclic voltammetry studies. The investigation showed that PANI/CHT SPCE exhibit high electroactive surface area compared to unmodified SPCE. The PANI/CHT SPCE recorded lowest detection limit (LOD) of 1.60 ppb with LOQ of 4.82 ppb, in the linear range of 25-50 ppb.https://myjms.mohe.gov.my/index.php/joa/article/view/19146polyanilinechitosanperfluorooctanoic acidscreen-printed carbon electrodeelectrochemical sensor. |
spellingShingle | NUR FARAHIN SUHAIMI Siti Nor Atika Baharin Nurul' Ain Jamion Kavirajaa Pandian Sambasevam A PRELIMINARY INVESTIGATION OF POLYANILINE/CHITOSAN COMPOSITE’S PHYSICOCHEMICAL PROPERTIES AND POTENTIAL ELECTROCHEMICAL APPLICATION Journal of Academia polyaniline chitosan perfluorooctanoic acid screen-printed carbon electrode electrochemical sensor. |
title | A PRELIMINARY INVESTIGATION OF POLYANILINE/CHITOSAN COMPOSITE’S PHYSICOCHEMICAL PROPERTIES AND POTENTIAL ELECTROCHEMICAL APPLICATION |
title_full | A PRELIMINARY INVESTIGATION OF POLYANILINE/CHITOSAN COMPOSITE’S PHYSICOCHEMICAL PROPERTIES AND POTENTIAL ELECTROCHEMICAL APPLICATION |
title_fullStr | A PRELIMINARY INVESTIGATION OF POLYANILINE/CHITOSAN COMPOSITE’S PHYSICOCHEMICAL PROPERTIES AND POTENTIAL ELECTROCHEMICAL APPLICATION |
title_full_unstemmed | A PRELIMINARY INVESTIGATION OF POLYANILINE/CHITOSAN COMPOSITE’S PHYSICOCHEMICAL PROPERTIES AND POTENTIAL ELECTROCHEMICAL APPLICATION |
title_short | A PRELIMINARY INVESTIGATION OF POLYANILINE/CHITOSAN COMPOSITE’S PHYSICOCHEMICAL PROPERTIES AND POTENTIAL ELECTROCHEMICAL APPLICATION |
title_sort | preliminary investigation of polyaniline chitosan composite s physicochemical properties and potential electrochemical application |
topic | polyaniline chitosan perfluorooctanoic acid screen-printed carbon electrode electrochemical sensor. |
url | https://myjms.mohe.gov.my/index.php/joa/article/view/19146 |
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