Post neutron irradiation annealing and defect evolution in single crystal tungsten

Single crystal W is offered for Physics understanding of irradiation induced defects and their annealing as its structure is well defined and it is almost defect free. W(100) single crystal was neutron irradiated to a damage of 0.11 displacements per atom at 600 °C and subsequently isochronally anne...

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Main Authors: D. Papadakis, K. Mergia, E. Manios, V. Chatzikos, S. Dellis, S. Messoloras
Format: Article
Language:English
Published: Elsevier 2023-03-01
Series:Nuclear Materials and Energy
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2352179122002381
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author D. Papadakis
K. Mergia
E. Manios
V. Chatzikos
S. Dellis
S. Messoloras
author_facet D. Papadakis
K. Mergia
E. Manios
V. Chatzikos
S. Dellis
S. Messoloras
author_sort D. Papadakis
collection DOAJ
description Single crystal W is offered for Physics understanding of irradiation induced defects and their annealing as its structure is well defined and it is almost defect free. W(100) single crystal was neutron irradiated to a damage of 0.11 displacements per atom at 600 °C and subsequently isochronally annealed from 700 up to 1500 °C in 100 °C steps. Irradiation causes the formation of dislocation loops and vacancy clusters and a 45 % increase in hardness. After the annealing of 1500 °C the positron lifetime annihilation spectrum shows a defect free material and its hardness has been reverted to the pre-irradiation value and only clusters of Re, WRe and WOs2 have been detected by grazing incidence X-ray diffraction. The total line density of dislocations, number density of voids and their size versus annealing temperature have been determined. From hardness, the critical resolved stresses arising from dislocations and voids have been derived and correlated with their densities. The kinetics of defect annihilation versus annealing temperature is discussed.
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spelling doaj.art-4680a91dab0b4c78b36d4c48b1a3ce432023-03-12T04:21:26ZengElsevierNuclear Materials and Energy2352-17912023-03-0134101357Post neutron irradiation annealing and defect evolution in single crystal tungstenD. Papadakis0K. Mergia1E. Manios2V. Chatzikos3S. Dellis4S. Messoloras5Institute of Nuclear and Radiological Sciences and Technology, Energy and Safety, NCSR Demokritos, Athens 15310, Greece; Department of Physics, School of Sciences, University of Athens, Athens 15772, GreeceInstitute of Nuclear and Radiological Sciences and Technology, Energy and Safety, NCSR Demokritos, Athens 15310, Greece; Corresponding author.Institute of Nuclear and Radiological Sciences and Technology, Energy and Safety, NCSR Demokritos, Athens 15310, GreeceInstitute of Nuclear and Radiological Sciences and Technology, Energy and Safety, NCSR Demokritos, Athens 15310, GreeceInstitute of Nuclear and Radiological Sciences and Technology, Energy and Safety, NCSR Demokritos, Athens 15310, GreeceInstitute of Nuclear and Radiological Sciences and Technology, Energy and Safety, NCSR Demokritos, Athens 15310, GreeceSingle crystal W is offered for Physics understanding of irradiation induced defects and their annealing as its structure is well defined and it is almost defect free. W(100) single crystal was neutron irradiated to a damage of 0.11 displacements per atom at 600 °C and subsequently isochronally annealed from 700 up to 1500 °C in 100 °C steps. Irradiation causes the formation of dislocation loops and vacancy clusters and a 45 % increase in hardness. After the annealing of 1500 °C the positron lifetime annihilation spectrum shows a defect free material and its hardness has been reverted to the pre-irradiation value and only clusters of Re, WRe and WOs2 have been detected by grazing incidence X-ray diffraction. The total line density of dislocations, number density of voids and their size versus annealing temperature have been determined. From hardness, the critical resolved stresses arising from dislocations and voids have been derived and correlated with their densities. The kinetics of defect annihilation versus annealing temperature is discussed.http://www.sciencedirect.com/science/article/pii/S2352179122002381Radiation damageTungsten single crystalPost-irradiation annealingPositron annihilation lifetime spectroscopyElectrical resistivityHardness
spellingShingle D. Papadakis
K. Mergia
E. Manios
V. Chatzikos
S. Dellis
S. Messoloras
Post neutron irradiation annealing and defect evolution in single crystal tungsten
Nuclear Materials and Energy
Radiation damage
Tungsten single crystal
Post-irradiation annealing
Positron annihilation lifetime spectroscopy
Electrical resistivity
Hardness
title Post neutron irradiation annealing and defect evolution in single crystal tungsten
title_full Post neutron irradiation annealing and defect evolution in single crystal tungsten
title_fullStr Post neutron irradiation annealing and defect evolution in single crystal tungsten
title_full_unstemmed Post neutron irradiation annealing and defect evolution in single crystal tungsten
title_short Post neutron irradiation annealing and defect evolution in single crystal tungsten
title_sort post neutron irradiation annealing and defect evolution in single crystal tungsten
topic Radiation damage
Tungsten single crystal
Post-irradiation annealing
Positron annihilation lifetime spectroscopy
Electrical resistivity
Hardness
url http://www.sciencedirect.com/science/article/pii/S2352179122002381
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