Extraction, Identification and Determination of di-(2ethylhexyl) Phthalate (DEHP) Plasticizer in Some Stored Blood Samples Bags Using Different Spectroscopic Techniques.

   The di-(2-ethylhexyl) phthalate (DEHP) was extracted using different solvents from plastic blood bag. The extracted product was identified using FT-IR, NMR (1H and 13C), DEPT, COSY, HMBC and HSQC_TOCSY spectrometry. The extracted plasticizer was tested in complex formation with Fe2+ and Cr3+ usi...

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Main Authors: Daryia Jalil, Nabil A. Fakhre
Format: Article
Language:English
Published: University of Baghdad 2017-03-01
Series:Ibn Al-Haitham Journal for Pure and Applied Sciences
Subjects:
Online Access:https://jih.uobaghdad.edu.iq/index.php/j/article/view/106
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author Daryia Jalil
Nabil A. Fakhre
author_facet Daryia Jalil
Nabil A. Fakhre
author_sort Daryia Jalil
collection DOAJ
description    The di-(2-ethylhexyl) phthalate (DEHP) was extracted using different solvents from plastic blood bag. The extracted product was identified using FT-IR, NMR (1H and 13C), DEPT, COSY, HMBC and HSQC_TOCSY spectrometry. The extracted plasticizer was tested in complex formation with Fe2+ and Cr3+ using UV-visible spectrophotometric method. The migration of the plasticizer from the blood bags to the blood was studied and determined during different storage times depending upon the formation of complexes with Fe2+ and Cr3+, and the change in the concentration of Fe2+ and Cr3+. 
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spelling doaj.art-46e3654c1ede431b89cc21d8f5d5eea92022-12-22T02:51:55ZengUniversity of BaghdadIbn Al-Haitham Journal for Pure and Applied Sciences1609-40422521-34072017-03-01292Extraction, Identification and Determination of di-(2ethylhexyl) Phthalate (DEHP) Plasticizer in Some Stored Blood Samples Bags Using Different Spectroscopic Techniques.Daryia JalilNabil A. Fakhre    The di-(2-ethylhexyl) phthalate (DEHP) was extracted using different solvents from plastic blood bag. The extracted product was identified using FT-IR, NMR (1H and 13C), DEPT, COSY, HMBC and HSQC_TOCSY spectrometry. The extracted plasticizer was tested in complex formation with Fe2+ and Cr3+ using UV-visible spectrophotometric method. The migration of the plasticizer from the blood bags to the blood was studied and determined during different storage times depending upon the formation of complexes with Fe2+ and Cr3+, and the change in the concentration of Fe2+ and Cr3+.  https://jih.uobaghdad.edu.iq/index.php/j/article/view/106Extraction, identification, determination, DEHP, blood bag samples, different spectroscopic techniques.
spellingShingle Daryia Jalil
Nabil A. Fakhre
Extraction, Identification and Determination of di-(2ethylhexyl) Phthalate (DEHP) Plasticizer in Some Stored Blood Samples Bags Using Different Spectroscopic Techniques.
Ibn Al-Haitham Journal for Pure and Applied Sciences
Extraction, identification, determination, DEHP, blood bag samples, different spectroscopic techniques.
title Extraction, Identification and Determination of di-(2ethylhexyl) Phthalate (DEHP) Plasticizer in Some Stored Blood Samples Bags Using Different Spectroscopic Techniques.
title_full Extraction, Identification and Determination of di-(2ethylhexyl) Phthalate (DEHP) Plasticizer in Some Stored Blood Samples Bags Using Different Spectroscopic Techniques.
title_fullStr Extraction, Identification and Determination of di-(2ethylhexyl) Phthalate (DEHP) Plasticizer in Some Stored Blood Samples Bags Using Different Spectroscopic Techniques.
title_full_unstemmed Extraction, Identification and Determination of di-(2ethylhexyl) Phthalate (DEHP) Plasticizer in Some Stored Blood Samples Bags Using Different Spectroscopic Techniques.
title_short Extraction, Identification and Determination of di-(2ethylhexyl) Phthalate (DEHP) Plasticizer in Some Stored Blood Samples Bags Using Different Spectroscopic Techniques.
title_sort extraction identification and determination of di 2ethylhexyl phthalate dehp plasticizer in some stored blood samples bags using different spectroscopic techniques
topic Extraction, identification, determination, DEHP, blood bag samples, different spectroscopic techniques.
url https://jih.uobaghdad.edu.iq/index.php/j/article/view/106
work_keys_str_mv AT daryiajalil extractionidentificationanddeterminationofdi2ethylhexylphthalatedehpplasticizerinsomestoredbloodsamplesbagsusingdifferentspectroscopictechniques
AT nabilafakhre extractionidentificationanddeterminationofdi2ethylhexylphthalatedehpplasticizerinsomestoredbloodsamplesbagsusingdifferentspectroscopictechniques