1-Heptyl-1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-1-ium iodide
The title compound C14H29N4+·I− salt, was obtained by the reaction of cage adamanzane-type aminal 1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecane with heptyl iodide. In the cation, the bond lengths and angles are within normal ranges, except for one N—C(ring) bo...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2011-10-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536811036403 |
| _version_ | 1818974002495881216 |
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| author | Karla Fejfarová Jaime Ríos-Motta John Sadat-Bernal Augusto Rivera Michal Dušek |
| author_facet | Karla Fejfarová Jaime Ríos-Motta John Sadat-Bernal Augusto Rivera Michal Dušek |
| author_sort | Karla Fejfarová |
| collection | DOAJ |
| description | The title compound C14H29N4+·I− salt, was obtained by the reaction of cage adamanzane-type aminal 1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecane with heptyl iodide. In the cation, the bond lengths and angles are within normal ranges, except for one N—C(ring) bond distance of 1.542 (3) Å, which is unexpectedly long compared with related compounds. In the crystal, ions are linked through C—H...I hydrogen bonds. The crystal studied was a non-merohedral twin with a minor twin domain of 6.56 (5)%. |
| first_indexed | 2024-12-20T15:33:08Z |
| format | Article |
| id | doaj.art-474f5d73e8e744e6aa5705dfb5a9ef48 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-20T15:33:08Z |
| publishDate | 2011-10-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-474f5d73e8e744e6aa5705dfb5a9ef482022-12-21T19:35:33ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-10-016710o2629o262910.1107/S16005368110364031-Heptyl-1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-1-ium iodideKarla FejfarováJaime Ríos-MottaJohn Sadat-BernalAugusto RiveraMichal DušekThe title compound C14H29N4+·I− salt, was obtained by the reaction of cage adamanzane-type aminal 1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecane with heptyl iodide. In the cation, the bond lengths and angles are within normal ranges, except for one N—C(ring) bond distance of 1.542 (3) Å, which is unexpectedly long compared with related compounds. In the crystal, ions are linked through C—H...I hydrogen bonds. The crystal studied was a non-merohedral twin with a minor twin domain of 6.56 (5)%.http://scripts.iucr.org/cgi-bin/paper?S1600536811036403 |
| spellingShingle | Karla Fejfarová Jaime Ríos-Motta John Sadat-Bernal Augusto Rivera Michal Dušek 1-Heptyl-1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-1-ium iodide Acta Crystallographica Section E |
| title | 1-Heptyl-1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-1-ium iodide |
| title_full | 1-Heptyl-1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-1-ium iodide |
| title_fullStr | 1-Heptyl-1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-1-ium iodide |
| title_full_unstemmed | 1-Heptyl-1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-1-ium iodide |
| title_short | 1-Heptyl-1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-1-ium iodide |
| title_sort | 1 heptyl 1 3 6 8 tetraazatricyclo 4 3 1 13 8 undecan 1 ium iodide |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536811036403 |
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