Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry

We present an in-situ energy dispersive X-ray fluorescence measurement of the content of Chromium and Nickel in the fumes produced by selective laser melting on an Inconel 625 powder. Significant variations of the intensities of the Chromium and Nickel Kα fluorescence lines were evidenced as a funct...

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Main Authors: Adrien Stolidi, Anthony Touron, Loïc Toulemonde, Hugues Paradis, Pierre Lapouge, Frédéric Coste, Jean-Paul Garandet
Format: Article
Language:English
Published: Elsevier 2023-07-01
Series:Additive Manufacturing Letters
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2772369023000348
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author Adrien Stolidi
Anthony Touron
Loïc Toulemonde
Hugues Paradis
Pierre Lapouge
Frédéric Coste
Jean-Paul Garandet
author_facet Adrien Stolidi
Anthony Touron
Loïc Toulemonde
Hugues Paradis
Pierre Lapouge
Frédéric Coste
Jean-Paul Garandet
author_sort Adrien Stolidi
collection DOAJ
description We present an in-situ energy dispersive X-ray fluorescence measurement of the content of Chromium and Nickel in the fumes produced by selective laser melting on an Inconel 625 powder. Significant variations of the intensities of the Chromium and Nickel Kα fluorescence lines were evidenced as a function of the laser power, lasing velocity and chamber atmosphere. Calibration has been carried out using Monte–Carlo particle transport simulations allowed to obtain a quantitative estimate of the Chromium and Nickel mass fraction in the fumes. The experimental data has been compared to the predictions of an analytical physico-chemical model with consistent results. This approach thus also allows to provide information on the temperature of the metallic bath.
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spelling doaj.art-48263016979b4135b0faabfbe2fc22522023-06-19T04:30:35ZengElsevierAdditive Manufacturing Letters2772-36902023-07-016100153Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometryAdrien Stolidi0Anthony Touron1Loïc Toulemonde2Hugues Paradis3Pierre Lapouge4Frédéric Coste5Jean-Paul Garandet6Corresponding author.; Université Paris Saclay, CEA, List, Palaiseau F91120, FranceUniversité Paris Saclay, CEA, List, Palaiseau F91120, FranceUniversité Paris Saclay, CEA, List, Palaiseau F91120, FranceUniversité Paris Saclay, CEA, List, Palaiseau F91120, FranceLaboratoire PIMM, Arts Et Métiers Institute of Technology, CNRS, Cnam, HESAM University, Paris 75013, FranceLaboratoire PIMM, Arts Et Métiers Institute of Technology, CNRS, Cnam, HESAM University, Paris 75013, FranceUniversité Grenoble Alpes, CEA, Liten, Grenoble F-38000, FranceWe present an in-situ energy dispersive X-ray fluorescence measurement of the content of Chromium and Nickel in the fumes produced by selective laser melting on an Inconel 625 powder. Significant variations of the intensities of the Chromium and Nickel Kα fluorescence lines were evidenced as a function of the laser power, lasing velocity and chamber atmosphere. Calibration has been carried out using Monte–Carlo particle transport simulations allowed to obtain a quantitative estimate of the Chromium and Nickel mass fraction in the fumes. The experimental data has been compared to the predictions of an analytical physico-chemical model with consistent results. This approach thus also allows to provide information on the temperature of the metallic bath.http://www.sciencedirect.com/science/article/pii/S2772369023000348In-line monitoringLPBSED-XRF
spellingShingle Adrien Stolidi
Anthony Touron
Loïc Toulemonde
Hugues Paradis
Pierre Lapouge
Frédéric Coste
Jean-Paul Garandet
Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry
Additive Manufacturing Letters
In-line monitoring
LPBS
ED-XRF
title Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry
title_full Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry
title_fullStr Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry
title_full_unstemmed Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry
title_short Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry
title_sort towards in situ fumes composition monitoring during an additive manufacturing process using energy dispersive x ray fluorescence spectrometry
topic In-line monitoring
LPBS
ED-XRF
url http://www.sciencedirect.com/science/article/pii/S2772369023000348
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