Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry
We present an in-situ energy dispersive X-ray fluorescence measurement of the content of Chromium and Nickel in the fumes produced by selective laser melting on an Inconel 625 powder. Significant variations of the intensities of the Chromium and Nickel Kα fluorescence lines were evidenced as a funct...
Main Authors: | , , , , , , |
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Format: | Article |
Language: | English |
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Elsevier
2023-07-01
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Series: | Additive Manufacturing Letters |
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Online Access: | http://www.sciencedirect.com/science/article/pii/S2772369023000348 |
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author | Adrien Stolidi Anthony Touron Loïc Toulemonde Hugues Paradis Pierre Lapouge Frédéric Coste Jean-Paul Garandet |
author_facet | Adrien Stolidi Anthony Touron Loïc Toulemonde Hugues Paradis Pierre Lapouge Frédéric Coste Jean-Paul Garandet |
author_sort | Adrien Stolidi |
collection | DOAJ |
description | We present an in-situ energy dispersive X-ray fluorescence measurement of the content of Chromium and Nickel in the fumes produced by selective laser melting on an Inconel 625 powder. Significant variations of the intensities of the Chromium and Nickel Kα fluorescence lines were evidenced as a function of the laser power, lasing velocity and chamber atmosphere. Calibration has been carried out using Monte–Carlo particle transport simulations allowed to obtain a quantitative estimate of the Chromium and Nickel mass fraction in the fumes. The experimental data has been compared to the predictions of an analytical physico-chemical model with consistent results. This approach thus also allows to provide information on the temperature of the metallic bath. |
first_indexed | 2024-03-13T04:42:15Z |
format | Article |
id | doaj.art-48263016979b4135b0faabfbe2fc2252 |
institution | Directory Open Access Journal |
issn | 2772-3690 |
language | English |
last_indexed | 2024-03-13T04:42:15Z |
publishDate | 2023-07-01 |
publisher | Elsevier |
record_format | Article |
series | Additive Manufacturing Letters |
spelling | doaj.art-48263016979b4135b0faabfbe2fc22522023-06-19T04:30:35ZengElsevierAdditive Manufacturing Letters2772-36902023-07-016100153Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometryAdrien Stolidi0Anthony Touron1Loïc Toulemonde2Hugues Paradis3Pierre Lapouge4Frédéric Coste5Jean-Paul Garandet6Corresponding author.; Université Paris Saclay, CEA, List, Palaiseau F91120, FranceUniversité Paris Saclay, CEA, List, Palaiseau F91120, FranceUniversité Paris Saclay, CEA, List, Palaiseau F91120, FranceUniversité Paris Saclay, CEA, List, Palaiseau F91120, FranceLaboratoire PIMM, Arts Et Métiers Institute of Technology, CNRS, Cnam, HESAM University, Paris 75013, FranceLaboratoire PIMM, Arts Et Métiers Institute of Technology, CNRS, Cnam, HESAM University, Paris 75013, FranceUniversité Grenoble Alpes, CEA, Liten, Grenoble F-38000, FranceWe present an in-situ energy dispersive X-ray fluorescence measurement of the content of Chromium and Nickel in the fumes produced by selective laser melting on an Inconel 625 powder. Significant variations of the intensities of the Chromium and Nickel Kα fluorescence lines were evidenced as a function of the laser power, lasing velocity and chamber atmosphere. Calibration has been carried out using Monte–Carlo particle transport simulations allowed to obtain a quantitative estimate of the Chromium and Nickel mass fraction in the fumes. The experimental data has been compared to the predictions of an analytical physico-chemical model with consistent results. This approach thus also allows to provide information on the temperature of the metallic bath.http://www.sciencedirect.com/science/article/pii/S2772369023000348In-line monitoringLPBSED-XRF |
spellingShingle | Adrien Stolidi Anthony Touron Loïc Toulemonde Hugues Paradis Pierre Lapouge Frédéric Coste Jean-Paul Garandet Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry Additive Manufacturing Letters In-line monitoring LPBS ED-XRF |
title | Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry |
title_full | Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry |
title_fullStr | Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry |
title_full_unstemmed | Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry |
title_short | Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry |
title_sort | towards in situ fumes composition monitoring during an additive manufacturing process using energy dispersive x ray fluorescence spectrometry |
topic | In-line monitoring LPBS ED-XRF |
url | http://www.sciencedirect.com/science/article/pii/S2772369023000348 |
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