2-Hydroxy-N′-(5-hydroxy-2-nitrobenzylidene)-3-methylbenzohydrazide
The title compound, C15H13N3O5, was prepared by condensing 5-hydroxy-2-nitrobenzaldehyde and 2-hydroxy-3-methylbenzohydrazide in methanol. The two benzene rings make a dihedral angle of 3.9 (3)°. An intramolecular O—H...O hydrogen bond is observed. The crysta...
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2012-03-01
|
| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536812002437 |
| Summary: | The title compound, C15H13N3O5, was prepared by condensing 5-hydroxy-2-nitrobenzaldehyde and 2-hydroxy-3-methylbenzohydrazide in methanol. The two benzene rings make a dihedral angle of 3.9 (3)°. An intramolecular O—H...O hydrogen bond is observed. The crystal structure is stabilized by intermolecular O—H...O and N—H...O hydrogen bonds, and C—H...O and π–π interactions [centroid–centroid distances = 3.5658 (17)–3.9287 (19) Å]. |
|---|---|
| ISSN: | 1600-5368 |