Determination of Cr, As, Cd, Hg and Pb in various alcohol samples by inductively coupled plasma mass spectrometry(电感耦合等离子体质谱测定不同酒类中铬、砷、镉、汞、铅含量)
应用微波消解处理酒样,不经富集直接用ICPMS测定Cr、As、Cd、Hg、Pb含量,方法快速,干扰少.测定的33种不同酒样中Cr、As、Cd、Hg、Pb的含量均值分别为 45.84、19.53、2.22、1.92 μg •kg-1和 115.06 µg •kg-1,其中白酒中含量最高,葡萄酒和啤酒居次,黄酒含量最低.Cr、As、Cd、Hg、Pb的检出限分别为0.063、0.082、0.007、0.001 µg •L -1和0.080 µg •L -1,各元素的加标回收率基本在 90%~110%,RSD（n= 10）在 0.25%~6.76%....
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| Format: | Article |
| Language: | zho |
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Zhejiang University Press
2009-11-01
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| Series: | Zhejiang Daxue xuebao. Lixue ban |
| Subjects: | |
| Online Access: | https://doi.org/10.3785/j.issn.1008-9497.2009.06.017 |
| _version_ | 1797236130143272960 |
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| author | CHENGHe-yong(程和勇) XUZi-gang(徐子刚) HUANGXu(黄旭) ZHANGYi(张翼) |
| author_facet | CHENGHe-yong(程和勇) XUZi-gang(徐子刚) HUANGXu(黄旭) ZHANGYi(张翼) |
| author_sort | CHENGHe-yong(程和勇) |
| collection | DOAJ |
| description | 应用微波消解处理酒样,不经富集直接用ICPMS测定Cr、As、Cd、Hg、Pb含量,方法快速,干扰少.测定的33种不同酒样中Cr、As、Cd、Hg、Pb的含量均值分别为 45.84、19.53、2.22、1.92 μg •kg-1和 115.06 µg •kg-1,其中白酒中含量最高,葡萄酒和啤酒居次,黄酒含量最低.Cr、As、Cd、Hg、Pb的检出限分别为0.063、0.082、0.007、0.001 µg •L -1和0.080 µg •L -1,各元素的加标回收率基本在 90%~110%,RSD（n= 10）在 0.25%~6.76%. |
| first_indexed | 2024-04-24T16:58:57Z |
| format | Article |
| id | doaj.art-49a5364290f3418fb1ebf0e66e79ad89 |
| institution | Directory Open Access Journal |
| issn | 1008-9497 |
| language | zho |
| last_indexed | 2024-04-24T16:58:57Z |
| publishDate | 2009-11-01 |
| publisher | Zhejiang University Press |
| record_format | Article |
| series | Zhejiang Daxue xuebao. Lixue ban |
| spelling | doaj.art-49a5364290f3418fb1ebf0e66e79ad892024-03-29T01:58:27ZzhoZhejiang University PressZhejiang Daxue xuebao. Lixue ban1008-94972009-11-0136667968210.3785/j.issn.1008-9497.2009.06.017Determination of Cr, As, Cd, Hg and Pb in various alcohol samples by inductively coupled plasma mass spectrometry(电感耦合等离子体质谱测定不同酒类中铬、砷、镉、汞、铅含量)CHENGHe-yong(程和勇)0XUZi-gang(徐子刚)1HUANGXu(黄旭)2ZHANGYi(张翼)3Department of Chemistry, Zhejiang University, Hangzhou 310027, Chi na(浙江大学化学系，浙江 杭州 310027)Department of Chemistry, Zhejiang University, Hangzhou 310027, Chi na(浙江大学化学系，浙江 杭州 310027)Department of Chemistry, Zhejiang University, Hangzhou 310027, Chi na(浙江大学化学系，浙江 杭州 310027)Department of Chemistry, Zhejiang University, Hangzhou 310027, Chi na(浙江大学化学系，浙江 杭州 310027)应用微波消解处理酒样,不经富集直接用ICPMS测定Cr、As、Cd、Hg、Pb含量,方法快速,干扰少.测定的33种不同酒样中Cr、As、Cd、Hg、Pb的含量均值分别为 45.84、19.53、2.22、1.92 μg •kg-1和 115.06 µg •kg-1,其中白酒中含量最高,葡萄酒和啤酒居次,黄酒含量最低.Cr、As、Cd、Hg、Pb的检出限分别为0.063、0.082、0.007、0.001 µg •L -1和0.080 µg •L -1,各元素的加标回收率基本在 90%~110%,RSD（n= 10）在 0.25%~6.76%.https://doi.org/10.3785/j.issn.1008-9497.2009.06.017白酒啤酒黄酒葡萄酒电感耦合等离子体质谱(icp-ms)铬砷镉汞铅微波消解 |
| spellingShingle | CHENGHe-yong(程和勇) XUZi-gang(徐子刚) HUANGXu(黄旭) ZHANGYi(张翼) Determination of Cr, As, Cd, Hg and Pb in various alcohol samples by inductively coupled plasma mass spectrometry(电感耦合等离子体质谱测定不同酒类中铬、砷、镉、汞、铅含量) Zhejiang Daxue xuebao. Lixue ban 白酒 啤酒 黄酒 葡萄酒 电感耦合等离子体质谱(icp-ms) 铬 砷 镉 汞 铅 微波消解 |
| title | Determination of Cr, As, Cd, Hg and Pb in various alcohol samples by inductively coupled plasma mass spectrometry(电感耦合等离子体质谱测定不同酒类中铬、砷、镉、汞、铅含量) |
| title_full | Determination of Cr, As, Cd, Hg and Pb in various alcohol samples by inductively coupled plasma mass spectrometry(电感耦合等离子体质谱测定不同酒类中铬、砷、镉、汞、铅含量) |
| title_fullStr | Determination of Cr, As, Cd, Hg and Pb in various alcohol samples by inductively coupled plasma mass spectrometry(电感耦合等离子体质谱测定不同酒类中铬、砷、镉、汞、铅含量) |
| title_full_unstemmed | Determination of Cr, As, Cd, Hg and Pb in various alcohol samples by inductively coupled plasma mass spectrometry(电感耦合等离子体质谱测定不同酒类中铬、砷、镉、汞、铅含量) |
| title_short | Determination of Cr, As, Cd, Hg and Pb in various alcohol samples by inductively coupled plasma mass spectrometry(电感耦合等离子体质谱测定不同酒类中铬、砷、镉、汞、铅含量) |
| title_sort | determination of cr as cd hg and pb in various alcohol samples by inductively coupled plasma mass spectrometry 电感耦合等离子体质谱测定不同酒类中铬 砷 镉 汞 铅含量 |
| topic | 白酒 啤酒 黄酒 葡萄酒 电感耦合等离子体质谱(icp-ms) 铬 砷 镉 汞 铅 微波消解 |
| url | https://doi.org/10.3785/j.issn.1008-9497.2009.06.017 |
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