Synthesis and Characterization of ferrous glycinate monohydrate(一水合甘氨酸亚铁螯合物的合成及其表征)
以甘氨酸(Gly)与碳酸亚铁为原料合成了阴离子干扰少、纯度较高的甘氨酸亚铁螯合物.以反应体系的pH值为5.5~6.0、抗氧化剂用量为甘氨酸质量的10%、配位比(Gly/Fe)为2：1、反应温度为80 ℃的优化条件，得到了产率为87.21%、螯合率为86.95%的甘氨酸亚铁螯合物，产物经纯化处理后，测定了它的红外光谱和差热分析，考察了它的摩尔电导率和稳定常数(K)，判断甘氨酸亚铁是带一个结晶水的反式结构螯合物....
| Main Authors: | , , , , |
|---|---|
| Format: | Article |
| Language: | zho |
| Published: |
Zhejiang University Press
2013-05-01
|
| Series: | Zhejiang Daxue xuebao. Lixue ban |
| Subjects: | |
| Online Access: | https://doi.org/10.3785/j.issn.1008-9497.2013.03.011 |
| _version_ | 1827303157708881920 |
|---|---|
| author | YULu(俞露) CUIYan-li(崔艳丽) GUANHai-yue(管海跃) XUMing-han(徐明瀚) MAOJian-wei(毛建卫) |
| author_facet | YULu(俞露) CUIYan-li(崔艳丽) GUANHai-yue(管海跃) XUMing-han(徐明瀚) MAOJian-wei(毛建卫) |
| author_sort | YULu(俞露) |
| collection | DOAJ |
| description | 以甘氨酸(Gly)与碳酸亚铁为原料合成了阴离子干扰少、纯度较高的甘氨酸亚铁螯合物.以反应体系的pH值为5.5~6.0、抗氧化剂用量为甘氨酸质量的10%、配位比(Gly/Fe)为2：1、反应温度为80 ℃的优化条件，得到了产率为87.21%、螯合率为86.95%的甘氨酸亚铁螯合物，产物经纯化处理后，测定了它的红外光谱和差热分析，考察了它的摩尔电导率和稳定常数(K)，判断甘氨酸亚铁是带一个结晶水的反式结构螯合物. |
| first_indexed | 2024-04-24T16:57:11Z |
| format | Article |
| id | doaj.art-49bdb1a685a74c09bcbe68baf93a6ad2 |
| institution | Directory Open Access Journal |
| issn | 1008-9497 |
| language | zho |
| last_indexed | 2024-04-24T16:57:11Z |
| publishDate | 2013-05-01 |
| publisher | Zhejiang University Press |
| record_format | Article |
| series | Zhejiang Daxue xuebao. Lixue ban |
| spelling | doaj.art-49bdb1a685a74c09bcbe68baf93a6ad22024-03-29T01:58:31ZzhoZhejiang University PressZhejiang Daxue xuebao. Lixue ban1008-94972013-05-0140329129610.3785/j.issn.1008-9497.2013.03.011Synthesis and Characterization of ferrous glycinate monohydrate(一水合甘氨酸亚铁螯合物的合成及其表征)YULu(俞露)0CUIYan-li(崔艳丽)1GUANHai-yue(管海跃)2XUMing-han(徐明瀚)3MAOJian-wei(毛建卫)4 1. College of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310014, China( 1.浙江工业大学 化学工程与材料学院，浙江 杭州 310014) 2. Department of Chemistry, Zhejiang University, Hangzhou 310027, China( 2.浙江大学 化学系，浙江 杭州 310027) 2. Department of Chemistry, Zhejiang University, Hangzhou 310027, China( 2.浙江大学 化学系，浙江 杭州 310027) 2. Department of Chemistry, Zhejiang University, Hangzhou 310027, China( 2.浙江大学 化学系，浙江 杭州 310027) 3. Zhejiang Provincial Key Lab for Chemistry & Biological Processing Technology of Farm Produces, Hangzhou 310023, China( 3.浙江省农产品化学与生物加工技术重点实验室，浙江 杭州 310023)以甘氨酸(Gly)与碳酸亚铁为原料合成了阴离子干扰少、纯度较高的甘氨酸亚铁螯合物.以反应体系的pH值为5.5~6.0、抗氧化剂用量为甘氨酸质量的10%、配位比(Gly/Fe)为2：1、反应温度为80 ℃的优化条件，得到了产率为87.21%、螯合率为86.95%的甘氨酸亚铁螯合物，产物经纯化处理后，测定了它的红外光谱和差热分析，考察了它的摩尔电导率和稳定常数(K)，判断甘氨酸亚铁是带一个结晶水的反式结构螯合物.https://doi.org/10.3785/j.issn.1008-9497.2013.03.011甘氨酸亚铁螯合 |
| spellingShingle | YULu(俞露) CUIYan-li(崔艳丽) GUANHai-yue(管海跃) XUMing-han(徐明瀚) MAOJian-wei(毛建卫) Synthesis and Characterization of ferrous glycinate monohydrate(一水合甘氨酸亚铁螯合物的合成及其表征) Zhejiang Daxue xuebao. Lixue ban 甘氨酸 亚铁 螯合 |
| title | Synthesis and Characterization of ferrous glycinate monohydrate(一水合甘氨酸亚铁螯合物的合成及其表征) |
| title_full | Synthesis and Characterization of ferrous glycinate monohydrate(一水合甘氨酸亚铁螯合物的合成及其表征) |
| title_fullStr | Synthesis and Characterization of ferrous glycinate monohydrate(一水合甘氨酸亚铁螯合物的合成及其表征) |
| title_full_unstemmed | Synthesis and Characterization of ferrous glycinate monohydrate(一水合甘氨酸亚铁螯合物的合成及其表征) |
| title_short | Synthesis and Characterization of ferrous glycinate monohydrate(一水合甘氨酸亚铁螯合物的合成及其表征) |
| title_sort | synthesis and characterization of ferrous glycinate monohydrate 一水合甘氨酸亚铁螯合物的合成及其表征 |
| topic | 甘氨酸 亚铁 螯合 |
| url | https://doi.org/10.3785/j.issn.1008-9497.2013.03.011 |
| work_keys_str_mv | AT yuluyúlù synthesisandcharacterizationofferrousglycinatemonohydrateyīshuǐhégānānsuānyàtiěáohéwùdehéchéngjíqíbiǎozhēng AT cuiyanlicuīyànlì synthesisandcharacterizationofferrousglycinatemonohydrateyīshuǐhégānānsuānyàtiěáohéwùdehéchéngjíqíbiǎozhēng AT guanhaiyueguǎnhǎiyuè synthesisandcharacterizationofferrousglycinatemonohydrateyīshuǐhégānānsuānyàtiěáohéwùdehéchéngjíqíbiǎozhēng AT xuminghanxúmínghàn synthesisandcharacterizationofferrousglycinatemonohydrateyīshuǐhégānānsuānyàtiěáohéwùdehéchéngjíqíbiǎozhēng AT maojianweimáojiànwèi synthesisandcharacterizationofferrousglycinatemonohydrateyīshuǐhégānānsuānyàtiěáohéwùdehéchéngjíqíbiǎozhēng |