Efficient magnetic and antibacterial properties of CdO/ZnO nanocomposites prepared via facile hydrothermal method

The effect of molar composition on the efficiency of antibacterial and magnetic properties of binary transition metal oxide nanocomposites synthesized using pH optimized hydrothermal method is reported. Its response to X-ray diffraction confirmed the crystallinity of nanocomposites. The average crys...

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Main Authors: C. Uthiram, N. Punithavelan
Format: Article
Language:English
Published: Elsevier 2022-08-01
Series:Journal of King Saud University: Science
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S1018364722003433
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author C. Uthiram
N. Punithavelan
author_facet C. Uthiram
N. Punithavelan
author_sort C. Uthiram
collection DOAJ
description The effect of molar composition on the efficiency of antibacterial and magnetic properties of binary transition metal oxide nanocomposites synthesized using pH optimized hydrothermal method is reported. Its response to X-ray diffraction confirmed the crystallinity of nanocomposites. The average crystallite size is observed to be 27.37 nm, 30.21 nm and 32.3 nm for 1:1, 2:1 and 1:2 molar ratioed CdO/ZnO nanocomposites respectively. FT-IR spectroscopy revealed the presence of moisture and other functional groups, which is further confirmed the Thermogravimetric analysis showing approximately 1.5% of thermal decomposition within 200 °C in all composition. The synthesized composites are characterized for surface morphology using High-resolution scanning electron microscopy and Energy dispersive X-ray analysis showed mixed nanorods, nanotubes and spheroid structures. The optical band gap of proposed nanocomposites is characterized by UV-diffused reflectance spectroscopy showing the variation of optical band gap confirming the change in a molar proportion of CdO/ZnO nanocomposites particles. Investigation on magnetic properties displayed its paramagnetic behavior by illustrating the hysteresis curves of all nanocomposites. The antibacterial activities of proposed nanocomposites investigated for both Gram-positive and Gram-negative bacteria showed its efficiency towards antibacterial application.
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spelling doaj.art-4aafbf4dbb5e4987a55c1225e851a3b32022-12-22T03:31:29ZengElsevierJournal of King Saud University: Science1018-36472022-08-01346102162Efficient magnetic and antibacterial properties of CdO/ZnO nanocomposites prepared via facile hydrothermal methodC. Uthiram0N. Punithavelan1Division of Physics, School of Advanced Sciences, Vellore Institute of Technology (VIT), Chennai Campus, Vandalur-Kelmbakkam Road, Chennai 600 127, IndiaCorresponding author.; Division of Physics, School of Advanced Sciences, Vellore Institute of Technology (VIT), Chennai Campus, Vandalur-Kelmbakkam Road, Chennai 600 127, IndiaThe effect of molar composition on the efficiency of antibacterial and magnetic properties of binary transition metal oxide nanocomposites synthesized using pH optimized hydrothermal method is reported. Its response to X-ray diffraction confirmed the crystallinity of nanocomposites. The average crystallite size is observed to be 27.37 nm, 30.21 nm and 32.3 nm for 1:1, 2:1 and 1:2 molar ratioed CdO/ZnO nanocomposites respectively. FT-IR spectroscopy revealed the presence of moisture and other functional groups, which is further confirmed the Thermogravimetric analysis showing approximately 1.5% of thermal decomposition within 200 °C in all composition. The synthesized composites are characterized for surface morphology using High-resolution scanning electron microscopy and Energy dispersive X-ray analysis showed mixed nanorods, nanotubes and spheroid structures. The optical band gap of proposed nanocomposites is characterized by UV-diffused reflectance spectroscopy showing the variation of optical band gap confirming the change in a molar proportion of CdO/ZnO nanocomposites particles. Investigation on magnetic properties displayed its paramagnetic behavior by illustrating the hysteresis curves of all nanocomposites. The antibacterial activities of proposed nanocomposites investigated for both Gram-positive and Gram-negative bacteria showed its efficiency towards antibacterial application.http://www.sciencedirect.com/science/article/pii/S1018364722003433Fuel and capping agent freeMagnetic propertiesAntibacterial activityStreptococcus pyogenesKlebsiella pneumonia
spellingShingle C. Uthiram
N. Punithavelan
Efficient magnetic and antibacterial properties of CdO/ZnO nanocomposites prepared via facile hydrothermal method
Journal of King Saud University: Science
Fuel and capping agent free
Magnetic properties
Antibacterial activity
Streptococcus pyogenes
Klebsiella pneumonia
title Efficient magnetic and antibacterial properties of CdO/ZnO nanocomposites prepared via facile hydrothermal method
title_full Efficient magnetic and antibacterial properties of CdO/ZnO nanocomposites prepared via facile hydrothermal method
title_fullStr Efficient magnetic and antibacterial properties of CdO/ZnO nanocomposites prepared via facile hydrothermal method
title_full_unstemmed Efficient magnetic and antibacterial properties of CdO/ZnO nanocomposites prepared via facile hydrothermal method
title_short Efficient magnetic and antibacterial properties of CdO/ZnO nanocomposites prepared via facile hydrothermal method
title_sort efficient magnetic and antibacterial properties of cdo zno nanocomposites prepared via facile hydrothermal method
topic Fuel and capping agent free
Magnetic properties
Antibacterial activity
Streptococcus pyogenes
Klebsiella pneumonia
url http://www.sciencedirect.com/science/article/pii/S1018364722003433
work_keys_str_mv AT cuthiram efficientmagneticandantibacterialpropertiesofcdoznonanocompositespreparedviafacilehydrothermalmethod
AT npunithavelan efficientmagneticandantibacterialpropertiesofcdoznonanocompositespreparedviafacilehydrothermalmethod