Magnetic stirring in syringe dispersive liquid-liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples: A multivariate analysis approach

A new, rapid, simple, and sensitive preconcentration method and Spectrophotometry determination technique have been presented for the microextraction and determination of trace amount of Tartrazine dye in food samples. In the present system, which is called “Magnetic stirring in syring dispersive li...

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Main Authors: Ali Mohammadzadeh, Mahboobeh Amiri
Format: Article
Language:English
Published: Elsevier 2024-03-01
Series:Heliyon
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2405844024036429
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author Ali Mohammadzadeh
Mahboobeh Amiri
author_facet Ali Mohammadzadeh
Mahboobeh Amiri
author_sort Ali Mohammadzadeh
collection DOAJ
description A new, rapid, simple, and sensitive preconcentration method and Spectrophotometry determination technique have been presented for the microextraction and determination of trace amount of Tartrazine dye in food samples. In the present system, which is called “Magnetic stirring in syring dispersive liquid-liquid microextraction''(MSIS- DLLME), a cloudy state result is formed in a homemade glass syringe by magnetic agitation. In the MSIS-DLLME system, Tartrazine colour was uprooted into an organic detergent (Toluene) after many twinkles. Subsequently, the organic detergent which was placed on top of the result was transferred into a narrow neck by moving the piston overhead. The effective parameters on the extraction recovery were studied and optimized by Central Composite design (CCD). Under the optimum conditions, the estimation cure is direct in the range of 0.1–1(μg L− 1). The limit of detection (LOD), relative standard divagation and enrichment factor were 0.03 μg L −1, ±4.6 (n = 10) and 166, independently. The advanced system was successfully applied for microextraction of Tartrazine in food samples.
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spelling doaj.art-4dc74d53f8aa44ea991c3c0f3ed82cbb2024-03-17T07:58:18ZengElsevierHeliyon2405-84402024-03-01105e27611Magnetic stirring in syringe dispersive liquid-liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples: A multivariate analysis approachAli Mohammadzadeh0Mahboobeh Amiri1Department of Chemistry, Faculty of Science, Islamic Azad University-Arak Branch, Arak, Iran; Corresponding author.Department of Microbiology, Faculty of Science, Shiraz Branch, Islamic Azad University, Shiraz, IranA new, rapid, simple, and sensitive preconcentration method and Spectrophotometry determination technique have been presented for the microextraction and determination of trace amount of Tartrazine dye in food samples. In the present system, which is called “Magnetic stirring in syring dispersive liquid-liquid microextraction''(MSIS- DLLME), a cloudy state result is formed in a homemade glass syringe by magnetic agitation. In the MSIS-DLLME system, Tartrazine colour was uprooted into an organic detergent (Toluene) after many twinkles. Subsequently, the organic detergent which was placed on top of the result was transferred into a narrow neck by moving the piston overhead. The effective parameters on the extraction recovery were studied and optimized by Central Composite design (CCD). Under the optimum conditions, the estimation cure is direct in the range of 0.1–1(μg L− 1). The limit of detection (LOD), relative standard divagation and enrichment factor were 0.03 μg L −1, ±4.6 (n = 10) and 166, independently. The advanced system was successfully applied for microextraction of Tartrazine in food samples.http://www.sciencedirect.com/science/article/pii/S2405844024036429Magnetic stirring in syringeTartrazineCentral composite designFood samplesUV–Vis spectrophotometer
spellingShingle Ali Mohammadzadeh
Mahboobeh Amiri
Magnetic stirring in syringe dispersive liquid-liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples: A multivariate analysis approach
Heliyon
Magnetic stirring in syringe
Tartrazine
Central composite design
Food samples
UV–Vis spectrophotometer
title Magnetic stirring in syringe dispersive liquid-liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples: A multivariate analysis approach
title_full Magnetic stirring in syringe dispersive liquid-liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples: A multivariate analysis approach
title_fullStr Magnetic stirring in syringe dispersive liquid-liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples: A multivariate analysis approach
title_full_unstemmed Magnetic stirring in syringe dispersive liquid-liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples: A multivariate analysis approach
title_short Magnetic stirring in syringe dispersive liquid-liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples: A multivariate analysis approach
title_sort magnetic stirring in syringe dispersive liquid liquid microextraction as an effective method for preconcentration of tartrazine dye from food samples a multivariate analysis approach
topic Magnetic stirring in syringe
Tartrazine
Central composite design
Food samples
UV–Vis spectrophotometer
url http://www.sciencedirect.com/science/article/pii/S2405844024036429
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AT mahboobehamiri magneticstirringinsyringedispersiveliquidliquidmicroextractionasaneffectivemethodforpreconcentrationoftartrazinedyefromfoodsamplesamultivariateanalysisapproach