Study on preparation and performance of additive flame retardant DOPO-HQ modified epoxy composite

An additive flame retardant was prepared from DOPO-HQ. Fourier transform infrared spectroscopy (FT-IR) was used to analyze its chemical structure. It was added to the experimental formula to prepare EP composite material, and the limiting oxygen index experiment and thermogravimetric analysis experi...

Full description

Bibliographic Details
Main Authors: Wang Chenghui, Wang Lele, Zhang Yingqiang
Format: Article
Language:English
Published: EDP Sciences 2022-01-01
Series:MATEC Web of Conferences
Subjects:
Online Access:https://www.matec-conferences.org/articles/matecconf/pdf/2022/05/matecconf_msms2022_01026.pdf
_version_ 1811245897825124352
author Wang Chenghui
Wang Lele
Zhang Yingqiang
author_facet Wang Chenghui
Wang Lele
Zhang Yingqiang
author_sort Wang Chenghui
collection DOAJ
description An additive flame retardant was prepared from DOPO-HQ. Fourier transform infrared spectroscopy (FT-IR) was used to analyze its chemical structure. It was added to the experimental formula to prepare EP composite material, and the limiting oxygen index experiment and thermogravimetric analysis experiment were carried out on the material, and the scanning electron microscope experiment was carried out on the residual carbon after combustion. The results show that the modified epoxy resin has a limiting oxygen index of 29.5%, and there is no droplet during combustion; thermogravimetric analysis experiments show that the temperature at which the thermal weight loss is 5%wt decreases, but the residual carbon rate increases. Scanning electron microscopy (SEM) test results show that carbon layer formed by the combustion products of epoxy resin is denser..
first_indexed 2024-04-12T14:46:01Z
format Article
id doaj.art-4ef6d3e0cec04ebeb2e41bb44fcf8faa
institution Directory Open Access Journal
issn 2261-236X
language English
last_indexed 2024-04-12T14:46:01Z
publishDate 2022-01-01
publisher EDP Sciences
record_format Article
series MATEC Web of Conferences
spelling doaj.art-4ef6d3e0cec04ebeb2e41bb44fcf8faa2022-12-22T03:28:38ZengEDP SciencesMATEC Web of Conferences2261-236X2022-01-013580102610.1051/matecconf/202235801026matecconf_msms2022_01026Study on preparation and performance of additive flame retardant DOPO-HQ modified epoxy compositeWang Chenghui0Wang Lele1Zhang Yingqiang2Shanghai Institute of TechnologyShanghai Institute of TechnologyShanghai Institute of TechnologyAn additive flame retardant was prepared from DOPO-HQ. Fourier transform infrared spectroscopy (FT-IR) was used to analyze its chemical structure. It was added to the experimental formula to prepare EP composite material, and the limiting oxygen index experiment and thermogravimetric analysis experiment were carried out on the material, and the scanning electron microscope experiment was carried out on the residual carbon after combustion. The results show that the modified epoxy resin has a limiting oxygen index of 29.5%, and there is no droplet during combustion; thermogravimetric analysis experiments show that the temperature at which the thermal weight loss is 5%wt decreases, but the residual carbon rate increases. Scanning electron microscopy (SEM) test results show that carbon layer formed by the combustion products of epoxy resin is denser..https://www.matec-conferences.org/articles/matecconf/pdf/2022/05/matecconf_msms2022_01026.pdfadditive flame retardantepoxy resinlimiting oxygen index
spellingShingle Wang Chenghui
Wang Lele
Zhang Yingqiang
Study on preparation and performance of additive flame retardant DOPO-HQ modified epoxy composite
MATEC Web of Conferences
additive flame retardant
epoxy resin
limiting oxygen index
title Study on preparation and performance of additive flame retardant DOPO-HQ modified epoxy composite
title_full Study on preparation and performance of additive flame retardant DOPO-HQ modified epoxy composite
title_fullStr Study on preparation and performance of additive flame retardant DOPO-HQ modified epoxy composite
title_full_unstemmed Study on preparation and performance of additive flame retardant DOPO-HQ modified epoxy composite
title_short Study on preparation and performance of additive flame retardant DOPO-HQ modified epoxy composite
title_sort study on preparation and performance of additive flame retardant dopo hq modified epoxy composite
topic additive flame retardant
epoxy resin
limiting oxygen index
url https://www.matec-conferences.org/articles/matecconf/pdf/2022/05/matecconf_msms2022_01026.pdf
work_keys_str_mv AT wangchenghui studyonpreparationandperformanceofadditiveflameretardantdopohqmodifiedepoxycomposite
AT wanglele studyonpreparationandperformanceofadditiveflameretardantdopohqmodifiedepoxycomposite
AT zhangyingqiang studyonpreparationandperformanceofadditiveflameretardantdopohqmodifiedepoxycomposite