| Summary: | The microstructural evolution and mechanical behavior of cast duplex stainless steels (CDSSs) at 400 °C for different thermal aging times were investigated by transmission electron microscope (TEM) and small punch test (SPT). The results showed that the spinodal decomposition in ferrite was the main reason for the decrease in toughness, and G-phase did not play an important role in the embrittlement process. The change of membrane stretching zone (W<sub>m</sub>) played an important role in the SPT load-displacement curve before and after thermal aging. During the deformation process of W<sub>m</sub> in the SPT, for thermal aging for 10,000 h, some completely curved slip bands were generated inside the ferrite phase, which had no contact with the δ/γ phase interface and belonged to the slip bands produced by the independent deformation of ferrite. The combined effect of the curved slip bands and stress concentration led to the initiation of obvious micro-cracks at the δ/γ phase interface. The micro-cracks propagated along the ferrite phase curved slip bands, and eventually penetrated the entire hardened ferrite phase.
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