Research on Microstructure, Synthesis Mechanisms, and Residual Stress Evolution of Polycrystalline Diamond Compacts

The microstructure and residual stress of polycrystalline diamond compact (PDC) play crucial roles in the performance of PDCs. Currently, in-depth research is still to be desired on the evolution mechanisms of microstructure and residual stress during high pressure high temperature (HPHT) synthesis...

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Main Authors: Peishen Ni, Yongxuan Chen, Wenxin Yang, Zijian Hu, Xin Deng
Format: Article
Language:English
Published: MDPI AG 2023-08-01
Series:Crystals
Subjects:
Online Access:https://www.mdpi.com/2073-4352/13/8/1286
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author Peishen Ni
Yongxuan Chen
Wenxin Yang
Zijian Hu
Xin Deng
author_facet Peishen Ni
Yongxuan Chen
Wenxin Yang
Zijian Hu
Xin Deng
author_sort Peishen Ni
collection DOAJ
description The microstructure and residual stress of polycrystalline diamond compact (PDC) play crucial roles in the performance of PDCs. Currently, in-depth research is still to be desired on the evolution mechanisms of microstructure and residual stress during high pressure high temperature (HPHT) synthesis process of PDCs. This study systematically investigated the influencing mechanisms of polycrystalline diamond (PCD) layer material design, especially the Co content of the PCD layer, on microstructure and residual stress evolution in PDCs via Raman spectroscopy and finite element micromechanical simulation. The research shows that when the original Co content of the PCD layer is higher than 15 wt.%, the extra Co in the PCD layer will migrate backwards towards the carbide substrate and form Co-enrichment regions at the PCD–carbide substrate interface. As the original Co content of the PCD layer increases from 13 to 20 wt.%, the residual compressive stress of diamond phase at the upper surface center of the PCD layer gradually decreases and transforms into tensile stress. When the original Co content of the PCD layer is as high as 30 wt.%, the residual stress transforms back into significant compressive stress again. The microstructure-based micromechanical simulation at the PCD–carbide substrate interface shows that the Co-enrichment region is the key for the transformation of the residual stress of the diamond phase from tensile stress into significant compressive stress.
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spelling doaj.art-4f71724b9eb94c699418d0717fefed4e2023-11-19T00:46:02ZengMDPI AGCrystals2073-43522023-08-01138128610.3390/cryst13081286Research on Microstructure, Synthesis Mechanisms, and Residual Stress Evolution of Polycrystalline Diamond CompactsPeishen Ni0Yongxuan Chen1Wenxin Yang2Zijian Hu3Xin Deng4School of Electromechanical Engineering, Guangdong University of Technology, Guangzhou 510006, ChinaSchool of Electromechanical Engineering, Guangdong University of Technology, Guangzhou 510006, ChinaSchool of Electromechanical Engineering, Guangdong University of Technology, Guangzhou 510006, ChinaSchool of Electromechanical Engineering, Guangdong University of Technology, Guangzhou 510006, ChinaSchool of Electromechanical Engineering, Guangdong University of Technology, Guangzhou 510006, ChinaThe microstructure and residual stress of polycrystalline diamond compact (PDC) play crucial roles in the performance of PDCs. Currently, in-depth research is still to be desired on the evolution mechanisms of microstructure and residual stress during high pressure high temperature (HPHT) synthesis process of PDCs. This study systematically investigated the influencing mechanisms of polycrystalline diamond (PCD) layer material design, especially the Co content of the PCD layer, on microstructure and residual stress evolution in PDCs via Raman spectroscopy and finite element micromechanical simulation. The research shows that when the original Co content of the PCD layer is higher than 15 wt.%, the extra Co in the PCD layer will migrate backwards towards the carbide substrate and form Co-enrichment regions at the PCD–carbide substrate interface. As the original Co content of the PCD layer increases from 13 to 20 wt.%, the residual compressive stress of diamond phase at the upper surface center of the PCD layer gradually decreases and transforms into tensile stress. When the original Co content of the PCD layer is as high as 30 wt.%, the residual stress transforms back into significant compressive stress again. The microstructure-based micromechanical simulation at the PCD–carbide substrate interface shows that the Co-enrichment region is the key for the transformation of the residual stress of the diamond phase from tensile stress into significant compressive stress.https://www.mdpi.com/2073-4352/13/8/1286polycrystalline diamond compactHPHT processresidual stressfinite element analysismicromechanical simulation
spellingShingle Peishen Ni
Yongxuan Chen
Wenxin Yang
Zijian Hu
Xin Deng
Research on Microstructure, Synthesis Mechanisms, and Residual Stress Evolution of Polycrystalline Diamond Compacts
Crystals
polycrystalline diamond compact
HPHT process
residual stress
finite element analysis
micromechanical simulation
title Research on Microstructure, Synthesis Mechanisms, and Residual Stress Evolution of Polycrystalline Diamond Compacts
title_full Research on Microstructure, Synthesis Mechanisms, and Residual Stress Evolution of Polycrystalline Diamond Compacts
title_fullStr Research on Microstructure, Synthesis Mechanisms, and Residual Stress Evolution of Polycrystalline Diamond Compacts
title_full_unstemmed Research on Microstructure, Synthesis Mechanisms, and Residual Stress Evolution of Polycrystalline Diamond Compacts
title_short Research on Microstructure, Synthesis Mechanisms, and Residual Stress Evolution of Polycrystalline Diamond Compacts
title_sort research on microstructure synthesis mechanisms and residual stress evolution of polycrystalline diamond compacts
topic polycrystalline diamond compact
HPHT process
residual stress
finite element analysis
micromechanical simulation
url https://www.mdpi.com/2073-4352/13/8/1286
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