Effect of Annealing on the Magnetic Properties of Co<sub>2</sub>MnSi-Based Heusler Alloy Glass-Coated Microwires

In the current study, we concentrated on the influence of annealing on the magnetic behavior of Co<sub>2</sub>MnSi-based Heusler microwires. We set the annealing temperature at 1023 K for 2 h, as the sample did not show any significant changes in the magnetic properties at lower temperat...

Full description

Bibliographic Details
Main Authors: Mohamed Salaheldeen, Mihail Ipatov, Paula Corte-Leon, Valentina Zhukova, Arcady Zhukov
Format: Article
Language:English
Published: MDPI AG 2023-02-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/13/2/412
_version_ 1797619297692942336
author Mohamed Salaheldeen
Mihail Ipatov
Paula Corte-Leon
Valentina Zhukova
Arcady Zhukov
author_facet Mohamed Salaheldeen
Mihail Ipatov
Paula Corte-Leon
Valentina Zhukova
Arcady Zhukov
author_sort Mohamed Salaheldeen
collection DOAJ
description In the current study, we concentrated on the influence of annealing on the magnetic behavior of Co<sub>2</sub>MnSi-based Heusler microwires. We set the annealing temperature at 1023 K for 2 h, as the sample did not show any significant changes in the magnetic properties at lower temperatures, while annealing at temperatures above 1023 K damages the glass coating. Strong in-plane magnetocrystalline anisotropy parallel to the microwire axis was evident in the magnetic behavior at room temperature for as-prepared and annealed samples. The coercivity of the annealed sample was four times higher than that of the as-prepared sample across a wide range of measuring temperatures. Both annealed and as-prepared samples exhibit quite stable coercivity behavior with temperature, which may have interesting applications. The an nealed sample did not exhibit magnetic saturation for M-H loops measured below 50 K. Sharp irreversible magnetic behavior has been detected for annealed samples at a blocking temperature of 220 K; at the same time, the blocking temperature for the as-prepared sample was 150 K. The strong internal mechanical stress induced during the fabrication of Co<sub>2</sub>MnSi microwires in addition to the internal stress relaxation caused by the annealing induced the onset of magnetic phases resulting in unusual and irreversible magnetic behavior.
first_indexed 2024-03-11T08:25:03Z
format Article
id doaj.art-4f72f796f78c42a5aa6c4aa5641dff91
institution Directory Open Access Journal
issn 2075-4701
language English
last_indexed 2024-03-11T08:25:03Z
publishDate 2023-02-01
publisher MDPI AG
record_format Article
series Metals
spelling doaj.art-4f72f796f78c42a5aa6c4aa5641dff912023-11-16T22:08:56ZengMDPI AGMetals2075-47012023-02-0113241210.3390/met13020412Effect of Annealing on the Magnetic Properties of Co<sub>2</sub>MnSi-Based Heusler Alloy Glass-Coated MicrowiresMohamed Salaheldeen0Mihail Ipatov1Paula Corte-Leon2Valentina Zhukova3Arcady Zhukov4Departamento de Polímeros y Materiales Avanzados, Facultad Química, Universidad del País Vasco, UPV/EHU, 20018 San Sebastián, SpainDepartamento de Polímeros y Materiales Avanzados, Facultad Química, Universidad del País Vasco, UPV/EHU, 20018 San Sebastián, SpainDepartamento de Polímeros y Materiales Avanzados, Facultad Química, Universidad del País Vasco, UPV/EHU, 20018 San Sebastián, SpainDepartamento de Polímeros y Materiales Avanzados, Facultad Química, Universidad del País Vasco, UPV/EHU, 20018 San Sebastián, SpainDepartamento de Polímeros y Materiales Avanzados, Facultad Química, Universidad del País Vasco, UPV/EHU, 20018 San Sebastián, SpainIn the current study, we concentrated on the influence of annealing on the magnetic behavior of Co<sub>2</sub>MnSi-based Heusler microwires. We set the annealing temperature at 1023 K for 2 h, as the sample did not show any significant changes in the magnetic properties at lower temperatures, while annealing at temperatures above 1023 K damages the glass coating. Strong in-plane magnetocrystalline anisotropy parallel to the microwire axis was evident in the magnetic behavior at room temperature for as-prepared and annealed samples. The coercivity of the annealed sample was four times higher than that of the as-prepared sample across a wide range of measuring temperatures. Both annealed and as-prepared samples exhibit quite stable coercivity behavior with temperature, which may have interesting applications. The an nealed sample did not exhibit magnetic saturation for M-H loops measured below 50 K. Sharp irreversible magnetic behavior has been detected for annealed samples at a blocking temperature of 220 K; at the same time, the blocking temperature for the as-prepared sample was 150 K. The strong internal mechanical stress induced during the fabrication of Co<sub>2</sub>MnSi microwires in addition to the internal stress relaxation caused by the annealing induced the onset of magnetic phases resulting in unusual and irreversible magnetic behavior.https://www.mdpi.com/2075-4701/13/2/412Heusler alloysglass-coated microwiresmagnetic propertiesannealingblocking temperature
spellingShingle Mohamed Salaheldeen
Mihail Ipatov
Paula Corte-Leon
Valentina Zhukova
Arcady Zhukov
Effect of Annealing on the Magnetic Properties of Co<sub>2</sub>MnSi-Based Heusler Alloy Glass-Coated Microwires
Metals
Heusler alloys
glass-coated microwires
magnetic properties
annealing
blocking temperature
title Effect of Annealing on the Magnetic Properties of Co<sub>2</sub>MnSi-Based Heusler Alloy Glass-Coated Microwires
title_full Effect of Annealing on the Magnetic Properties of Co<sub>2</sub>MnSi-Based Heusler Alloy Glass-Coated Microwires
title_fullStr Effect of Annealing on the Magnetic Properties of Co<sub>2</sub>MnSi-Based Heusler Alloy Glass-Coated Microwires
title_full_unstemmed Effect of Annealing on the Magnetic Properties of Co<sub>2</sub>MnSi-Based Heusler Alloy Glass-Coated Microwires
title_short Effect of Annealing on the Magnetic Properties of Co<sub>2</sub>MnSi-Based Heusler Alloy Glass-Coated Microwires
title_sort effect of annealing on the magnetic properties of co sub 2 sub mnsi based heusler alloy glass coated microwires
topic Heusler alloys
glass-coated microwires
magnetic properties
annealing
blocking temperature
url https://www.mdpi.com/2075-4701/13/2/412
work_keys_str_mv AT mohamedsalaheldeen effectofannealingonthemagneticpropertiesofcosub2submnsibasedheusleralloyglasscoatedmicrowires
AT mihailipatov effectofannealingonthemagneticpropertiesofcosub2submnsibasedheusleralloyglasscoatedmicrowires
AT paulacorteleon effectofannealingonthemagneticpropertiesofcosub2submnsibasedheusleralloyglasscoatedmicrowires
AT valentinazhukova effectofannealingonthemagneticpropertiesofcosub2submnsibasedheusleralloyglasscoatedmicrowires
AT arcadyzhukov effectofannealingonthemagneticpropertiesofcosub2submnsibasedheusleralloyglasscoatedmicrowires