Synthesis and crystal structure of bis(μ2-acetato-κ2O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18

C58H86Ni3N8O18, triclinic, P1̅ (no. 2), a = 11.4561(8) Å, b = 13.1859(8) Å, c = 13.5063(11) Å, α = 109.620(7)°, β = 101.234(7)°, γ = 114.469(6)°, V = 1611.1(2) Å3, Z = 1, Rgt(F) = 0.0518, wRref(F2) = 0.1315, T = 173.69(10) K.

Bibliographic Details
Main Authors: Zong-Li Ren, Xiao-Xin An, Ling-Zhi Liu, Peng-Fei Lan, Wen-Kui Dong
Format: Article
Language:English
Published: De Gruyter 2018-05-01
Series:Zeitschrift für Kristallographie - New Crystal Structures
Subjects:
Online Access:https://doi.org/10.1515/ncrs-2017-0388
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author Zong-Li Ren
Xiao-Xin An
Ling-Zhi Liu
Peng-Fei Lan
Wen-Kui Dong
author_facet Zong-Li Ren
Xiao-Xin An
Ling-Zhi Liu
Peng-Fei Lan
Wen-Kui Dong
author_sort Zong-Li Ren
collection DOAJ
description C58H86Ni3N8O18, triclinic, P1̅ (no. 2), a = 11.4561(8) Å, b = 13.1859(8) Å, c = 13.5063(11) Å, α = 109.620(7)°, β = 101.234(7)°, γ = 114.469(6)°, V = 1611.1(2) Å3, Z = 1, Rgt(F) = 0.0518, wRref(F2) = 0.1315, T = 173.69(10) K.
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spelling doaj.art-4fe57831046f4bb38971cb18ea6d78252022-12-22T00:30:14ZengDe GruyterZeitschrift für Kristallographie - New Crystal Structures1433-72662197-45782018-05-01233349549710.1515/ncrs-2017-0388Synthesis and crystal structure of bis(μ2-acetato-κ2O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18Zong-Li Ren0Xiao-Xin An1Ling-Zhi Liu2Peng-Fei Lan3Wen-Kui Dong4School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. ChinaSchool of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. ChinaSchool of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. ChinaSchool of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. ChinaSchool of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, P.R. ChinaC58H86Ni3N8O18, triclinic, P1̅ (no. 2), a = 11.4561(8) Å, b = 13.1859(8) Å, c = 13.5063(11) Å, α = 109.620(7)°, β = 101.234(7)°, γ = 114.469(6)°, V = 1611.1(2) Å3, Z = 1, Rgt(F) = 0.0518, wRref(F2) = 0.1315, T = 173.69(10) K.https://doi.org/10.1515/ncrs-2017-03881589692
spellingShingle Zong-Li Ren
Xiao-Xin An
Ling-Zhi Liu
Peng-Fei Lan
Wen-Kui Dong
Synthesis and crystal structure of bis(μ2-acetato-κ2O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18
Zeitschrift für Kristallographie - New Crystal Structures
1589692
title Synthesis and crystal structure of bis(μ2-acetato-κ2O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18
title_full Synthesis and crystal structure of bis(μ2-acetato-κ2O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18
title_fullStr Synthesis and crystal structure of bis(μ2-acetato-κ2O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18
title_full_unstemmed Synthesis and crystal structure of bis(μ2-acetato-κ2O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18
title_short Synthesis and crystal structure of bis(μ2-acetato-κ2O:O′)-di(ethanol)-bis{μ2-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ6O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C58H86Ni3N8O18
title_sort synthesis and crystal structure of bis μ2 acetato κ2o o di ethanol bis μ2 5 n n diethylamine 5 methoxyl 2 2 ethylenediyldioxybis nitrilomethylidyne diphenolato κ6o o n n o o trinickel ii ethanol acetonitrile 1 2 2 c58h86ni3n8o18
topic 1589692
url https://doi.org/10.1515/ncrs-2017-0388
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