Nano crystalline ZnO catalyzed one pot three-component synthesis of 7-alkyl-6H,7H- naphtho[1',2':5,6]pyrano[3,2-c] chromen-6-ones under solvent-free conditions
In the present paper, an efficient one-pot synthesis of 7-alkyl-6H,7H-naphtho[1',2':5,6]pyrano[3,2-c]chromen-6-ones is described by three-component reaction of β-naphthol, aromatic aldehydes and 4-hydroxycoumarin using ZnO nanoparticles under solvent-free conditions. The present method pro...
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Format: | Article |
Language: | English |
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Chemical Society of Ethiopia
2016-08-01
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Series: | Bulletin of the Chemical Society of Ethiopia |
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Online Access: | https://www.ajol.info/index.php/bcse/article/view/140945 |
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author | M. J. Piltan J. S. Ghomi |
author_facet | M. J. Piltan J. S. Ghomi |
author_sort | M. J. Piltan |
collection | DOAJ |
description | In the present paper, an efficient one-pot synthesis of 7-alkyl-6H,7H-naphtho[1',2':5,6]pyrano[3,2-c]chromen-6-ones is described by three-component reaction of β-naphthol, aromatic aldehydes and 4-hydroxycoumarin using ZnO nanoparticles under solvent-free conditions. The present method provides a novel and efficient procedure for the synthesis of chromene derivatives with some advantageous such as short reaction times, easy workup, high yields, wide range of products, reusability of the catalyst, little catalyst loading and green conditions in the presence of ZnO nanoparticles (7 mol%) at 110 ºC. |
first_indexed | 2024-04-12T02:47:29Z |
format | Article |
id | doaj.art-5025e1866ea04131a592efe70a73366b |
institution | Directory Open Access Journal |
issn | 1011-3924 1726-801X |
language | English |
last_indexed | 2024-04-12T02:47:29Z |
publishDate | 2016-08-01 |
publisher | Chemical Society of Ethiopia |
record_format | Article |
series | Bulletin of the Chemical Society of Ethiopia |
spelling | doaj.art-5025e1866ea04131a592efe70a73366b2022-12-22T03:51:08ZengChemical Society of EthiopiaBulletin of the Chemical Society of Ethiopia1011-39241726-801X2016-08-01302289296http://dx.doi.org/10.4314/bcse.v30i2.13Nano crystalline ZnO catalyzed one pot three-component synthesis of 7-alkyl-6H,7H- naphtho[1',2':5,6]pyrano[3,2-c] chromen-6-ones under solvent-free conditionsM. J. PiltanJ. S. GhomiIn the present paper, an efficient one-pot synthesis of 7-alkyl-6H,7H-naphtho[1',2':5,6]pyrano[3,2-c]chromen-6-ones is described by three-component reaction of β-naphthol, aromatic aldehydes and 4-hydroxycoumarin using ZnO nanoparticles under solvent-free conditions. The present method provides a novel and efficient procedure for the synthesis of chromene derivatives with some advantageous such as short reaction times, easy workup, high yields, wide range of products, reusability of the catalyst, little catalyst loading and green conditions in the presence of ZnO nanoparticles (7 mol%) at 110 ºC.https://www.ajol.info/index.php/bcse/article/view/140945ZnO nanoparticlesThree-component reactionsSolvent-freeChromeneHeterogeneous catalysts |
spellingShingle | M. J. Piltan J. S. Ghomi Nano crystalline ZnO catalyzed one pot three-component synthesis of 7-alkyl-6H,7H- naphtho[1',2':5,6]pyrano[3,2-c] chromen-6-ones under solvent-free conditions Bulletin of the Chemical Society of Ethiopia ZnO nanoparticles Three-component reactions Solvent-free Chromene Heterogeneous catalysts |
title | Nano crystalline ZnO catalyzed one pot three-component synthesis of 7-alkyl-6H,7H- naphtho[1',2':5,6]pyrano[3,2-c] chromen-6-ones under solvent-free conditions |
title_full | Nano crystalline ZnO catalyzed one pot three-component synthesis of 7-alkyl-6H,7H- naphtho[1',2':5,6]pyrano[3,2-c] chromen-6-ones under solvent-free conditions |
title_fullStr | Nano crystalline ZnO catalyzed one pot three-component synthesis of 7-alkyl-6H,7H- naphtho[1',2':5,6]pyrano[3,2-c] chromen-6-ones under solvent-free conditions |
title_full_unstemmed | Nano crystalline ZnO catalyzed one pot three-component synthesis of 7-alkyl-6H,7H- naphtho[1',2':5,6]pyrano[3,2-c] chromen-6-ones under solvent-free conditions |
title_short | Nano crystalline ZnO catalyzed one pot three-component synthesis of 7-alkyl-6H,7H- naphtho[1',2':5,6]pyrano[3,2-c] chromen-6-ones under solvent-free conditions |
title_sort | nano crystalline zno catalyzed one pot three component synthesis of 7 alkyl 6h 7h naphtho 1 2 5 6 pyrano 3 2 c chromen 6 ones under solvent free conditions |
topic | ZnO nanoparticles Three-component reactions Solvent-free Chromene Heterogeneous catalysts |
url | https://www.ajol.info/index.php/bcse/article/view/140945 |
work_keys_str_mv | AT mjpiltan nanocrystallineznocatalyzedonepotthreecomponentsynthesisof7alkyl6h7hnaphtho1256pyrano32cchromen6onesundersolventfreeconditions AT jsghomi nanocrystallineznocatalyzedonepotthreecomponentsynthesisof7alkyl6h7hnaphtho1256pyrano32cchromen6onesundersolventfreeconditions |