Colloidal Aqueous Synthesis of Cobalt-Doped ZnO Nanoparticles with MSA as Stabilizing Agent

Zinc oxide (ZnO) is an n-type II-VI semiconductor material that has gained prominence in recent decades due to the possibility of its applications in the most diverse scientific areas, such as photonics, optoelectronics, magnetism, and biological systems. In this context, the scientific community se...

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Main Authors: Ítalo Macêdo Gonçalves, Giovannia Araujo de Lima Pereira, Maria Goreti Carvalho Pereira
Format: Article
Language:English
Published: MDPI AG 2022-12-01
Series:Engineering Proceedings
Subjects:
Online Access:https://www.mdpi.com/2673-4591/31/1/53
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author Ítalo Macêdo Gonçalves
Giovannia Araujo de Lima Pereira
Maria Goreti Carvalho Pereira
author_facet Ítalo Macêdo Gonçalves
Giovannia Araujo de Lima Pereira
Maria Goreti Carvalho Pereira
author_sort Ítalo Macêdo Gonçalves
collection DOAJ
description Zinc oxide (ZnO) is an n-type II-VI semiconductor material that has gained prominence in recent decades due to the possibility of its applications in the most diverse scientific areas, such as photonics, optoelectronics, magnetism, and biological systems. In this context, the scientific community seeks alternative synthetic methodologies to those already established in the literature, emphasizing the use of organic solvents, which are increasingly efficient, low-cost, and easy to reproduce. Thus, the present work proposed a method of colloidal aqueous synthesis, using different precursors of zinc and cobalt salts in a molar fraction according to the expression, Zn<sub>1−x</sub>Co<sub>x</sub>O (<i>x</i> = 0.05, 0.075, 0.10), and mercaptosuccinic acid (MSA) as a stabilizing agent. The results confirmed the formation of cobalt-doped ZnO nanoparticles from X-ray diffractometry characterization. To evaluate their properties, studies of compositional analysis and size distribution of ZnO nanoparticles using characterization techniques, such as inductively coupled plasma spectroscopy (ICP) and transmission electron microscopy (TEM), are being carried out to obtain even more promising results in this field.
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spelling doaj.art-523d54748fc0437f9481d2bceb33077e2023-11-18T10:16:17ZengMDPI AGEngineering Proceedings2673-45912022-12-013115310.3390/ASEC2022-13825Colloidal Aqueous Synthesis of Cobalt-Doped ZnO Nanoparticles with MSA as Stabilizing AgentÍtalo Macêdo Gonçalves0Giovannia Araujo de Lima Pereira1Maria Goreti Carvalho Pereira2Programa de Pós-Graduação em Ciência de Materiais, Federal University of Pernambuco, Recife 50740-560, PE, BrazilFundamental Chemistry Department, Federal University of Pernambuco, Recife 50740-560, PE, BrazilFundamental Chemistry Department, Federal University of Pernambuco, Recife 50740-560, PE, BrazilZinc oxide (ZnO) is an n-type II-VI semiconductor material that has gained prominence in recent decades due to the possibility of its applications in the most diverse scientific areas, such as photonics, optoelectronics, magnetism, and biological systems. In this context, the scientific community seeks alternative synthetic methodologies to those already established in the literature, emphasizing the use of organic solvents, which are increasingly efficient, low-cost, and easy to reproduce. Thus, the present work proposed a method of colloidal aqueous synthesis, using different precursors of zinc and cobalt salts in a molar fraction according to the expression, Zn<sub>1−x</sub>Co<sub>x</sub>O (<i>x</i> = 0.05, 0.075, 0.10), and mercaptosuccinic acid (MSA) as a stabilizing agent. The results confirmed the formation of cobalt-doped ZnO nanoparticles from X-ray diffractometry characterization. To evaluate their properties, studies of compositional analysis and size distribution of ZnO nanoparticles using characterization techniques, such as inductively coupled plasma spectroscopy (ICP) and transmission electron microscopy (TEM), are being carried out to obtain even more promising results in this field.https://www.mdpi.com/2673-4591/31/1/53ZnO nanoparticlescobalt dopingcolloidal synthesis
spellingShingle Ítalo Macêdo Gonçalves
Giovannia Araujo de Lima Pereira
Maria Goreti Carvalho Pereira
Colloidal Aqueous Synthesis of Cobalt-Doped ZnO Nanoparticles with MSA as Stabilizing Agent
Engineering Proceedings
ZnO nanoparticles
cobalt doping
colloidal synthesis
title Colloidal Aqueous Synthesis of Cobalt-Doped ZnO Nanoparticles with MSA as Stabilizing Agent
title_full Colloidal Aqueous Synthesis of Cobalt-Doped ZnO Nanoparticles with MSA as Stabilizing Agent
title_fullStr Colloidal Aqueous Synthesis of Cobalt-Doped ZnO Nanoparticles with MSA as Stabilizing Agent
title_full_unstemmed Colloidal Aqueous Synthesis of Cobalt-Doped ZnO Nanoparticles with MSA as Stabilizing Agent
title_short Colloidal Aqueous Synthesis of Cobalt-Doped ZnO Nanoparticles with MSA as Stabilizing Agent
title_sort colloidal aqueous synthesis of cobalt doped zno nanoparticles with msa as stabilizing agent
topic ZnO nanoparticles
cobalt doping
colloidal synthesis
url https://www.mdpi.com/2673-4591/31/1/53
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