N′-(2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazide
The title compound, C15H12I2N2O3, was synthesized by the condensation of equimolar amounts of 3,5-diiodosalicylaldehyde and 2-methoxybenzohydrazide in a methanol solution. There are two independent molecules, A and B, in the asymmetric unit. The dihedral angle between the two benzene rings is 30.2&a...
| Main Authors: | , |
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2009-06-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S160053680901914X |
| _version_ | 1818999167633063936 |
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| author | San-Jun Peng Fen Zhang |
| author_facet | San-Jun Peng Fen Zhang |
| author_sort | San-Jun Peng |
| collection | DOAJ |
| description | The title compound, C15H12I2N2O3, was synthesized by the condensation of equimolar amounts of 3,5-diiodosalicylaldehyde and 2-methoxybenzohydrazide in a methanol solution. There are two independent molecules, A and B, in the asymmetric unit. The dihedral angle between the two benzene rings is 30.2 (2)° for molecule A and 21.7 (2)° for molecule B. There are intramolecular O—H...N and N—H...O hydrogen bonds in each molecule. The crystal studied was an inversion twin with a 0.59 (3):0.41 (3) domain ratio. |
| first_indexed | 2024-12-20T22:13:07Z |
| format | Article |
| id | doaj.art-52c8af87d155465f99532f64624b02de |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-20T22:13:07Z |
| publishDate | 2009-06-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-52c8af87d155465f99532f64624b02de2022-12-21T19:25:07ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-06-01656o1410o141010.1107/S160053680901914XN′-(2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazideSan-Jun PengFen ZhangThe title compound, C15H12I2N2O3, was synthesized by the condensation of equimolar amounts of 3,5-diiodosalicylaldehyde and 2-methoxybenzohydrazide in a methanol solution. There are two independent molecules, A and B, in the asymmetric unit. The dihedral angle between the two benzene rings is 30.2 (2)° for molecule A and 21.7 (2)° for molecule B. There are intramolecular O—H...N and N—H...O hydrogen bonds in each molecule. The crystal studied was an inversion twin with a 0.59 (3):0.41 (3) domain ratio.http://scripts.iucr.org/cgi-bin/paper?S160053680901914X |
| spellingShingle | San-Jun Peng Fen Zhang N′-(2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazide Acta Crystallographica Section E |
| title | N′-(2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazide |
| title_full | N′-(2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazide |
| title_fullStr | N′-(2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazide |
| title_full_unstemmed | N′-(2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazide |
| title_short | N′-(2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazide |
| title_sort | n amp 8242 2 hydroxy 3 5 diiodobenzylidene 2 methoxybenzohydrazide |
| url | http://scripts.iucr.org/cgi-bin/paper?S160053680901914X |
| work_keys_str_mv | AT sanjunpeng namp82422hydroxy35diiodobenzylidene2methoxybenzohydrazide AT fenzhang namp82422hydroxy35diiodobenzylidene2methoxybenzohydrazide |