Hydrogen Embrittlement Behavior of Plastically Pre-Strained and Cathodically Hydrogen-Charged 316H Grade Austenitic Stainless Steel

In this work, the effects of electrochemical hydrogen charging of 316H grade austenitic stainless steel were investigated in order to characterize its hydrogen embrittlement (HE) resistance. The as-received 316H material was in a fully recrystallized (solution-annealed) material condition. The susce...

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Main Authors: Ladislav Falat, Lucia Čiripová, Ivan Petryshynets, Ondrej Milkovič, Miroslav Džupon, Karol Kovaľ
Format: Article
Language:English
Published: MDPI AG 2022-10-01
Series:Crystals
Subjects:
Online Access:https://www.mdpi.com/2073-4352/12/10/1419
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author Ladislav Falat
Lucia Čiripová
Ivan Petryshynets
Ondrej Milkovič
Miroslav Džupon
Karol Kovaľ
author_facet Ladislav Falat
Lucia Čiripová
Ivan Petryshynets
Ondrej Milkovič
Miroslav Džupon
Karol Kovaľ
author_sort Ladislav Falat
collection DOAJ
description In this work, the effects of electrochemical hydrogen charging of 316H grade austenitic stainless steel were investigated in order to characterize its hydrogen embrittlement (HE) resistance. The as-received 316H material was in a fully recrystallized (solution-annealed) material condition. The susceptibility to HE of the studied material was evaluated by determination of the embrittlement index from the results of conventional uniaxial tensile tests of nonhydrogenated and hydrogen-charged test specimens. The study was focused on the effects of two selected plastic pre-strain levels of tensile specimens on their resulting HE resistance. The selected pre-strains corresponded to the tensile stress conditions within the “yield stress–ultimate tensile strength” (YS–UTS) range and directly at the UTS point. The obtained embrittlement indices for the presently used pre-straining and hydrogen charging conditions indicated that the HE of the studied material states was small. However, it was revealed that the observed degradation of deformation properties of plastically pre-strained and hydrogen-charged materials was mainly caused by gradual plasticity exhaustion due to tensile straining, which well correlated with the observed effects indicated by electron backscatter diffraction analyses and indentation hardness measurements.
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spelling doaj.art-531e71de0633405db65423fc78187b582023-11-23T23:38:08ZengMDPI AGCrystals2073-43522022-10-011210141910.3390/cryst12101419Hydrogen Embrittlement Behavior of Plastically Pre-Strained and Cathodically Hydrogen-Charged 316H Grade Austenitic Stainless SteelLadislav Falat0Lucia Čiripová1Ivan Petryshynets2Ondrej Milkovič3Miroslav Džupon4Karol Kovaľ5Institute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 04001 Košice, SlovakiaInstitute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 04001 Košice, SlovakiaInstitute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 04001 Košice, SlovakiaInstitute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 04001 Košice, SlovakiaInstitute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 04001 Košice, SlovakiaInstitute of Materials Research, Slovak Academy of Sciences, Watsonova 47, 04001 Košice, SlovakiaIn this work, the effects of electrochemical hydrogen charging of 316H grade austenitic stainless steel were investigated in order to characterize its hydrogen embrittlement (HE) resistance. The as-received 316H material was in a fully recrystallized (solution-annealed) material condition. The susceptibility to HE of the studied material was evaluated by determination of the embrittlement index from the results of conventional uniaxial tensile tests of nonhydrogenated and hydrogen-charged test specimens. The study was focused on the effects of two selected plastic pre-strain levels of tensile specimens on their resulting HE resistance. The selected pre-strains corresponded to the tensile stress conditions within the “yield stress–ultimate tensile strength” (YS–UTS) range and directly at the UTS point. The obtained embrittlement indices for the presently used pre-straining and hydrogen charging conditions indicated that the HE of the studied material states was small. However, it was revealed that the observed degradation of deformation properties of plastically pre-strained and hydrogen-charged materials was mainly caused by gradual plasticity exhaustion due to tensile straining, which well correlated with the observed effects indicated by electron backscatter diffraction analyses and indentation hardness measurements.https://www.mdpi.com/2073-4352/12/10/1419austenitic steelhydrogen embrittlementmicrostructuretensile testfractography
spellingShingle Ladislav Falat
Lucia Čiripová
Ivan Petryshynets
Ondrej Milkovič
Miroslav Džupon
Karol Kovaľ
Hydrogen Embrittlement Behavior of Plastically Pre-Strained and Cathodically Hydrogen-Charged 316H Grade Austenitic Stainless Steel
Crystals
austenitic steel
hydrogen embrittlement
microstructure
tensile test
fractography
title Hydrogen Embrittlement Behavior of Plastically Pre-Strained and Cathodically Hydrogen-Charged 316H Grade Austenitic Stainless Steel
title_full Hydrogen Embrittlement Behavior of Plastically Pre-Strained and Cathodically Hydrogen-Charged 316H Grade Austenitic Stainless Steel
title_fullStr Hydrogen Embrittlement Behavior of Plastically Pre-Strained and Cathodically Hydrogen-Charged 316H Grade Austenitic Stainless Steel
title_full_unstemmed Hydrogen Embrittlement Behavior of Plastically Pre-Strained and Cathodically Hydrogen-Charged 316H Grade Austenitic Stainless Steel
title_short Hydrogen Embrittlement Behavior of Plastically Pre-Strained and Cathodically Hydrogen-Charged 316H Grade Austenitic Stainless Steel
title_sort hydrogen embrittlement behavior of plastically pre strained and cathodically hydrogen charged 316h grade austenitic stainless steel
topic austenitic steel
hydrogen embrittlement
microstructure
tensile test
fractography
url https://www.mdpi.com/2073-4352/12/10/1419
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AT ondrejmilkovic hydrogenembrittlementbehaviorofplasticallyprestrainedandcathodicallyhydrogencharged316hgradeausteniticstainlesssteel
AT miroslavdzupon hydrogenembrittlementbehaviorofplasticallyprestrainedandcathodicallyhydrogencharged316hgradeausteniticstainlesssteel
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