Study of the Structural, Morphological, Strength and Shielding Properties of CuBi<sub>2</sub>O<sub>4</sub> Films Obtained by Electrochemical Synthesis
In this research, the formation processes of CuBi<sub>2</sub>O<sub>4</sub> films were examined using atomic force microscopy, energy dispersive analysis and X-ray diffraction analysis methods. The films were synthesized through electrochemical deposition from sulfuric acid so...
| Main Authors: | , , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
MDPI AG
2023-11-01
|
| Series: | Materials |
| Subjects: | |
| Online Access: | https://www.mdpi.com/1996-1944/16/22/7241 |
| _version_ | 1797458506894278656 |
|---|---|
| author | Dauren B. Kadyrzhanov Malik E. Kaliyekperov Medet T. Idinov Artem L. Kozlovskiy |
| author_facet | Dauren B. Kadyrzhanov Malik E. Kaliyekperov Medet T. Idinov Artem L. Kozlovskiy |
| author_sort | Dauren B. Kadyrzhanov |
| collection | DOAJ |
| description | In this research, the formation processes of CuBi<sub>2</sub>O<sub>4</sub> films were examined using atomic force microscopy, energy dispersive analysis and X-ray diffraction analysis methods. The films were synthesized through electrochemical deposition from sulfuric acid solutions at a potential difference of 3.5 V. The duration of film growth was set to between 10 and 90 min to assess the possibility of controlled film growth and preserve the stability of their structural properties during growth over an extended period. An analysis of the data obtained by X-ray diffraction revealed that the resulting film samples are highly ordered structures with a tetragonal CuBi<sub>2</sub>O<sub>4</sub> phase. The results of the connection between the thickness of CuBi<sub>2</sub>O<sub>4</sub> films and strength properties depending on the time of film deposition were obtained. The results of the shielding efficiency of low-energy γ-quanta using CuBi<sub>2</sub>O<sub>4</sub> films were obtained. |
| first_indexed | 2024-03-09T16:39:03Z |
| format | Article |
| id | doaj.art-537380501daa4dea8c3b78eb8c37b8cd |
| institution | Directory Open Access Journal |
| issn | 1996-1944 |
| language | English |
| last_indexed | 2024-03-09T16:39:03Z |
| publishDate | 2023-11-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Materials |
| spelling | doaj.art-537380501daa4dea8c3b78eb8c37b8cd2023-11-24T14:53:58ZengMDPI AGMaterials1996-19442023-11-011622724110.3390/ma16227241Study of the Structural, Morphological, Strength and Shielding Properties of CuBi<sub>2</sub>O<sub>4</sub> Films Obtained by Electrochemical SynthesisDauren B. Kadyrzhanov0Malik E. Kaliyekperov1Medet T. Idinov2Artem L. Kozlovskiy3Engineering Profile Laboratory, L.N. Gumilyov Eurasian National University, Astana 010008, KazakhstanEngineering Profile Laboratory, L.N. Gumilyov Eurasian National University, Astana 010008, KazakhstanNJSC, Shakarim University of Semey, Semipalatinsk 071400, KazakhstanEngineering Profile Laboratory, L.N. Gumilyov Eurasian National University, Astana 010008, KazakhstanIn this research, the formation processes of CuBi<sub>2</sub>O<sub>4</sub> films were examined using atomic force microscopy, energy dispersive analysis and X-ray diffraction analysis methods. The films were synthesized through electrochemical deposition from sulfuric acid solutions at a potential difference of 3.5 V. The duration of film growth was set to between 10 and 90 min to assess the possibility of controlled film growth and preserve the stability of their structural properties during growth over an extended period. An analysis of the data obtained by X-ray diffraction revealed that the resulting film samples are highly ordered structures with a tetragonal CuBi<sub>2</sub>O<sub>4</sub> phase. The results of the connection between the thickness of CuBi<sub>2</sub>O<sub>4</sub> films and strength properties depending on the time of film deposition were obtained. The results of the shielding efficiency of low-energy γ-quanta using CuBi<sub>2</sub>O<sub>4</sub> films were obtained.https://www.mdpi.com/1996-1944/16/22/7241thin filmselectrochemical depositionshielding materialsprotective filmsγ-radiation |
| spellingShingle | Dauren B. Kadyrzhanov Malik E. Kaliyekperov Medet T. Idinov Artem L. Kozlovskiy Study of the Structural, Morphological, Strength and Shielding Properties of CuBi<sub>2</sub>O<sub>4</sub> Films Obtained by Electrochemical Synthesis Materials thin films electrochemical deposition shielding materials protective films γ-radiation |
| title | Study of the Structural, Morphological, Strength and Shielding Properties of CuBi<sub>2</sub>O<sub>4</sub> Films Obtained by Electrochemical Synthesis |
| title_full | Study of the Structural, Morphological, Strength and Shielding Properties of CuBi<sub>2</sub>O<sub>4</sub> Films Obtained by Electrochemical Synthesis |
| title_fullStr | Study of the Structural, Morphological, Strength and Shielding Properties of CuBi<sub>2</sub>O<sub>4</sub> Films Obtained by Electrochemical Synthesis |
| title_full_unstemmed | Study of the Structural, Morphological, Strength and Shielding Properties of CuBi<sub>2</sub>O<sub>4</sub> Films Obtained by Electrochemical Synthesis |
| title_short | Study of the Structural, Morphological, Strength and Shielding Properties of CuBi<sub>2</sub>O<sub>4</sub> Films Obtained by Electrochemical Synthesis |
| title_sort | study of the structural morphological strength and shielding properties of cubi sub 2 sub o sub 4 sub films obtained by electrochemical synthesis |
| topic | thin films electrochemical deposition shielding materials protective films γ-radiation |
| url | https://www.mdpi.com/1996-1944/16/22/7241 |
| work_keys_str_mv | AT daurenbkadyrzhanov studyofthestructuralmorphologicalstrengthandshieldingpropertiesofcubisub2subosub4subfilmsobtainedbyelectrochemicalsynthesis AT malikekaliyekperov studyofthestructuralmorphologicalstrengthandshieldingpropertiesofcubisub2subosub4subfilmsobtainedbyelectrochemicalsynthesis AT medettidinov studyofthestructuralmorphologicalstrengthandshieldingpropertiesofcubisub2subosub4subfilmsobtainedbyelectrochemicalsynthesis AT artemlkozlovskiy studyofthestructuralmorphologicalstrengthandshieldingpropertiesofcubisub2subosub4subfilmsobtainedbyelectrochemicalsynthesis |