Evolution of the Microstructure and Mechanical Properties of a Ti35Nb2Sn Alloy Post-Processed by Hot Isostatic Pressing for Biomedical Applications

The HIP post-processing step is required for developing next generation of advanced powder metallurgy titanium alloys for orthopedic and dental applications. The influence of the hot isostatic pressing (HIP) post-processing step on structural and phase changes, porosity healing, and mechanical stren...

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Main Authors: Joan Lario, Ángel Vicente, Vicente Amigó
Format: Article
Language:English
Published: MDPI AG 2021-06-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/11/7/1027
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author Joan Lario
Ángel Vicente
Vicente Amigó
author_facet Joan Lario
Ángel Vicente
Vicente Amigó
author_sort Joan Lario
collection DOAJ
description The HIP post-processing step is required for developing next generation of advanced powder metallurgy titanium alloys for orthopedic and dental applications. The influence of the hot isostatic pressing (HIP) post-processing step on structural and phase changes, porosity healing, and mechanical strength in a powder metallurgy Ti35Nb2Sn alloy was studied. Powders were pressed at room temperature at 750 MPa, and then sintered at 1350 °C in a vacuum for 3 h. The standard HIP process at 1200 °C and 150 MPa for 3 h was performed to study its effect on a Ti35Nb2Sn powder metallurgy alloy. The influence of the HIP process and cold rate on the density, microstructure, quantity of interstitial elements, mechanical strength, and Young’s modulus was investigated. HIP post-processing for 2 h at 1200 °C and 150 MPa led to greater porosity reduction and a marked retention of the β phase at room temperature. The slow cooling rate during the HIP process affected phase stability, with a large amount of α”-phase precipitate, which decreased the titanium alloy’s yield strength.
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spelling doaj.art-540dd6ab9aca4b0dad6106b2a79858952023-11-22T01:49:19ZengMDPI AGMetals2075-47012021-06-01117102710.3390/met11071027Evolution of the Microstructure and Mechanical Properties of a Ti35Nb2Sn Alloy Post-Processed by Hot Isostatic Pressing for Biomedical ApplicationsJoan Lario0Ángel Vicente1Vicente Amigó2DIMM ETSII, Universitat Politècnica de València, Camino de Vera s/n, 5E Building, 46022 Valencia, SpainDIMM ETSII, Universitat Politècnica de València, Camino de Vera s/n, 5E Building, 46022 Valencia, SpainDIMM ETSII, Universitat Politècnica de València, Camino de Vera s/n, 5E Building, 46022 Valencia, SpainThe HIP post-processing step is required for developing next generation of advanced powder metallurgy titanium alloys for orthopedic and dental applications. The influence of the hot isostatic pressing (HIP) post-processing step on structural and phase changes, porosity healing, and mechanical strength in a powder metallurgy Ti35Nb2Sn alloy was studied. Powders were pressed at room temperature at 750 MPa, and then sintered at 1350 °C in a vacuum for 3 h. The standard HIP process at 1200 °C and 150 MPa for 3 h was performed to study its effect on a Ti35Nb2Sn powder metallurgy alloy. The influence of the HIP process and cold rate on the density, microstructure, quantity of interstitial elements, mechanical strength, and Young’s modulus was investigated. HIP post-processing for 2 h at 1200 °C and 150 MPa led to greater porosity reduction and a marked retention of the β phase at room temperature. The slow cooling rate during the HIP process affected phase stability, with a large amount of α”-phase precipitate, which decreased the titanium alloy’s yield strength.https://www.mdpi.com/2075-4701/11/7/1027hot isostatic pressingβ-Type titanium alloybiomaterialphase transformationpowder metallurgy
spellingShingle Joan Lario
Ángel Vicente
Vicente Amigó
Evolution of the Microstructure and Mechanical Properties of a Ti35Nb2Sn Alloy Post-Processed by Hot Isostatic Pressing for Biomedical Applications
Metals
hot isostatic pressing
β-Type titanium alloy
biomaterial
phase transformation
powder metallurgy
title Evolution of the Microstructure and Mechanical Properties of a Ti35Nb2Sn Alloy Post-Processed by Hot Isostatic Pressing for Biomedical Applications
title_full Evolution of the Microstructure and Mechanical Properties of a Ti35Nb2Sn Alloy Post-Processed by Hot Isostatic Pressing for Biomedical Applications
title_fullStr Evolution of the Microstructure and Mechanical Properties of a Ti35Nb2Sn Alloy Post-Processed by Hot Isostatic Pressing for Biomedical Applications
title_full_unstemmed Evolution of the Microstructure and Mechanical Properties of a Ti35Nb2Sn Alloy Post-Processed by Hot Isostatic Pressing for Biomedical Applications
title_short Evolution of the Microstructure and Mechanical Properties of a Ti35Nb2Sn Alloy Post-Processed by Hot Isostatic Pressing for Biomedical Applications
title_sort evolution of the microstructure and mechanical properties of a ti35nb2sn alloy post processed by hot isostatic pressing for biomedical applications
topic hot isostatic pressing
β-Type titanium alloy
biomaterial
phase transformation
powder metallurgy
url https://www.mdpi.com/2075-4701/11/7/1027
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