Pyridinium 5-[(1,3-diethyl-6-hydroxy-4-oxo-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl)(2-methoxyphenyl)methyl]-1,3-diethyl-4,6-dioxo-2-thioxopyrimidin-5-ide

Pyridinium 5-[(1,3-diethyl-6-hydroxy-4-oxo-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl)(2-methoxyphenyl)methyl]-1,3-diethyl-4,6-dioxo-2-thioxopyrimidin-5-ide

1,3-Diethyl-2-thiobarbituric acid reacts with 2-anisaldehyde to form the Michael addition product 2-anisylbis(1,3-diethyl-2-thiobarbitur-5-yl)methanate, which crystallizes as the title pyridinium salt, C5H6N+&#183;C24H29N4O5S2&#8722;, when it reacts with the pyridine used to catalyse...

Full description

Bibliographic Details
Main Authors:	Abdullah Mohamed Asiri, Salman A. Khan, Seik Weng Ng
Format:	Article
Language:	English
Published:	International Union of Crystallography 2009-08-01
Series:	Acta Crystallographica Section E
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S160053680902618X

Similar Items

N,N-Diethyl-2-hydroxyethanaminium 5-(5-chloro-2,4-dinitrophenyl)-2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-olate hemihydrate
by: Rajamanickam Babykala, et al.
Published: (2012-02-01)

1,3-Diethyl-2-sulfanylidene-5-(2,4,5-trimethoxybenzylidene)-1,3-diazinane-4,6-dione
by: Tariq R. Sobahi, et al.
Published: (2013-01-01)

2-Aminopyridinium 5-(5-chloro-2,4-dinitrophenyl)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-6-olate
by: Vaduganathan Manickkam, et al.
Published: (2011-12-01)

Crystal structure of diethylammonium 5-((4-fluorophenyl)(6-hydroxy-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)methyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-olate, C23H30FN5O6
by: Barakat Assem, et al.
Published: (2016-06-01)

Ethyl 4-(4-cyanophenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
by: De-Hong Wu, et al.
Published: (2009-08-01)

2-[(E)-(6-Amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)iminomethyl]pyridinium chloride monohydrate
by: Irvin Booysen, et al.
Published: (2011-09-01)

1,3-Diethyl-5-(4-methoxybenzylidene)-2-thioxodihydropyrimidine-4,6(1H,5H)-dione
by: Abraham F. Jalbout, et al.
Published: (2004-02-01)

Ethyl 4-(2,4-difluorophenyl)-6-methyl-1-phenyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
by: B. Kalluraya, et al.
Published: (2009-05-01)

Ethyl 4-(2-bromo-5-fluorophenyl)-6-methyl-1-phenyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
by: Hoong-Kun Fun, et al.
Published: (2008-08-01)

1,3-Diethyl-5-(2-methoxybenzylidene)-2-thioxodihydropyrimidine-4,6(1H,5H)-dione
by: Abraham F. Jalbout, et al.
Published: (2004-02-01)

Crystal structure of 4-aminopyridinium 5-(5-chloro-2,4-dinitrophenyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-olate hemihydrate
by: Manickkam Vaduganathan, et al.
Published: (2014-10-01)

N,N-Diethylanilinium 2,4-dioxo-5-(2,4,6-trinitrophenyl)-1,2,3,4-tetrahydropyrimidin-6-olate
by: Manickam Buvaneswari, et al.
Published: (2011-12-01)

5,5'-(1,4-Phenylenedimethylylidene)bis(1,3-diethyl-2-thioxodihydropyrimidine-4,6(1H,5H)-dione)
by: Salman A. Khan, et al.
Published: (2010-03-01)

Trimethylammonium 2,6-dioxo-5-(2,4,6-trinitrophenyl)-1,2,3,6-tetrahydropyrimidin-4-olate
by: D. Kalaivani, et al.
Published: (2012-01-01)

Ethyl 6-(2-chlorophenyl)-4-methyl-1-(3-oxobutyl)-2-thioxo-1,2,3,6-tetrahydropyrimidine-5-carboxylate
by: Ruo-Kun Feng, et al.
Published: (2008-02-01)

Diethyl 1,1-dioxo-3,5-bis(pyridin-2-yl)-1&#955;6,4-thiomorpholine-2,6-dicarboxylate
by: P. Sugumar, et al.
Published: (2011-02-01)

Diethyl 4-(6-Chloroimidazo[2,1-b]thiazol-5-yl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate and Ethyl 4-(6-Chloroimidazo[2,1-b]thiazol-5-yl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
by: Alberto Leoni, et al.
Published: (2012-11-01)

Crystal structure of 5,5′-((3-hydroxy-4-methoxyphenyl)methylene)bis(1,3-diethyl-6-hydroxy-2-thioxo-2,3-dihydropyrimidin-4(1H)-one), C24H30N4O6S2
by: Altowyan Mezna saleh, et al.
Published: (2018-08-01)

Ethyl 4-(2-fluorophenyl)-6-methyl-2-thioxo-1-(<i>p</i>-tolyl)-1,2,3,4-tetrahydropyrimidine-5-carboxylate
by: Itamar Luís Gonçalves, et al.
Published: (2018-11-01)

Cytotoxic and antimicrobial activities of some novel heterocycles employing 6-(1,3-diphenyl-1H-pyrazol-4-yl)-4-oxo-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carbonitrile
by: Ramadan Sayed K., et al.
Published: (2019-11-01)

(<i>E</i>)-3-(2,5-Dimethoxyphenyl)-1-{[4-(2,5-dimethoxy-phenyl)-6-((<i>E</i>)-2,5-dimethoxystyryl)-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl]}prop-2-en-1-one and (<i>E</i>)-3-(2,5-Dimethoxyphenyl)-1-{[4-(2,5-dimethoxyphenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidin-5-yl]}prop-2-en-1-one
by: Hery Suwito, et al.
Published: (2019-06-01)

N,N-Diethylanilinium 5-(2,4-dinitrophenyl)-2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-olate
by: Govindan Mangaiyarkarasi, et al.
Published: (2013-01-01)

(3R,4Z)-1,3-Diethyl-4-(2-oxopropylidene)-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one
by: Laila El Foujji, et al.
Published: (2018-04-01)

Diethyl 4-hydroxy-4-methyl-6-oxo-2-phenylcyclohexane-1,3-dicarboxylate
by: Hoong-Kun Fun, et al.
Published: (2010-08-01)

Diethyl 4-(3-chlorophenyl)-2,6-diphenyl-1,4-dihydropyridine-3,5-dicarboxylate
by: K. K. Mohammed Ameen, et al.
Published: (2019-12-01)

Trimethylammonium 5-(2,4-dinitrophenyl)-2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-olate 0.125-hydrate
by: Govindan Mangaiyarkarasi, et al.
Published: (2013-04-01)

Diethyl 4-(2,4-dichlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
by: P. Palakshi Reddy, et al.
Published: (2010-02-01)

Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
by: Yiliang Zhao, et al.
Published: (2012-08-01)

Diethyl 4-(4-ethoxyphenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
by: Hoong-Kun Fun, et al.
Published: (2009-09-01)

1,3-Bis[(5-aminofuran-2-yl)methyl]-3,4,5,6-tetrahydropyrimidin-1-ium hexafluorophosphate
by: Muhammad Nawaz Tahir, et al.
Published: (2013-08-01)

6-(3,5-Dimethylbenzyl)-5-ethyl-1-[(2-phenoxyethoxy)methyl]-1,2,3,4-tetrahydropyrimidine-2,4-dione
by: Nasser R. El-Brollosy, et al.
Published: (2011-11-01)

6-(3,5-Dimethylbenzyl)-5-ethyl-1-[(3-phenylpropoxy)methyl]-1,2,3,4-tetrahydropyrimidine-2,4-dione
by: Nasser R. El-Brollosy, et al.
Published: (2012-02-01)

[(2R,3S,5R)-3-Acetoxy-5-(5-formyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-1-yl)-2,3,4,5-tetrahydrofuran-2-yl]methyl acetate
by: Xue-Fei Jia, et al.
Published: (2011-11-01)

Diethyl 4-(4,5-dihydrofuran-2-yl)-3,5-dimethyl-1-phenyl-1,4-dihydropyrazine-2,6-dicarboxylate
by: Hong Yan, et al.
Published: (2009-05-01)

Diethyl [4-(1,3-benzothiazol-2-yl)benzyl]phosphonate
by: Huisheng Li, et al.
Published: (2010-12-01)

Diethyl 4-(3-chlorophenyl)-2-methyl-6-phenyl-1,4-dihydropyridine-3,5-dicarboxylate
by: F. M. Mashood Ahamed, et al.
Published: (2016-01-01)

Diethyl 1-benzyl-2,2-dioxo-4-phenyl-3,4,6,7,8,8a-hexahydro-1H-pyrrolo[2,1-c][1,4]thiazine-1,3-dicarboxylate
by: A. Chitradevi, et al.
Published: (2011-09-01)

Diethyl trans-2,5-bis(4-methoxybenzylsulfanyl)-1,4-dimethyl-3,6-dioxopiperazine-2,5-carboxylate
by: Nathan W. Polaske, et al.
Published: (2009-07-01)

Diethyl 2,6-dimethyl-4-(naphthalen-1-yl)-1,4-dihydropyridine-3,5-dicarboxylate
by: N. L. Prasad, et al.
Published: (2016-05-01)

Diethyl 2,6-dimethyl-4-p-tolyl-1,4-dihydropyridine-3,5-dicarboxylate
by: Hoong-Kun Fun, et al.
Published: (2009-10-01)