Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis
An efficient and practical method for identifying mandarin juice over-blended into not from concentrate (NFC) orange juice was established. Juices were extracted from different cultivars of sweet orange and mandarin fruits. After being pasteurized, the volatile organic compounds (VOCs) in the juice...
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MDPI AG
2020-04-01
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Series: | Foods |
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Online Access: | https://www.mdpi.com/2304-8158/9/4/505 |
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author | Qi Zhou Guijie Li Zhu Ou-Yang Xin Yi Linhua Huang Hua Wang |
author_facet | Qi Zhou Guijie Li Zhu Ou-Yang Xin Yi Linhua Huang Hua Wang |
author_sort | Qi Zhou |
collection | DOAJ |
description | An efficient and practical method for identifying mandarin juice over-blended into not from concentrate (NFC) orange juice was established. Juices were extracted from different cultivars of sweet orange and mandarin fruits. After being pasteurized, the volatile organic compounds (VOCs) in the juice samples were extracted using headspace solid-phase microextraction, and qualitatively and quantitatively analyzed using gas chromatography–mass spectrometry detection. Thirty-two VOCs contained in both the sweet orange juice and mandarin juice were used as variables, and the identification model for discriminating between the two varieties of juice was established by principal component analysis. Validation was applied by using common mandarin juices from Ponkan, Satsuma and Nanfengmiju cultivars blended at series of proportions into orange juices from Long-leaf, Olinda, and Hamlin cultivars. The model can visually identify a blending of mandarin juice at the volume fraction of 10% or above. |
first_indexed | 2024-03-10T20:26:03Z |
format | Article |
id | doaj.art-5495632c1b26465281e1dcde9fa74108 |
institution | Directory Open Access Journal |
issn | 2304-8158 |
language | English |
last_indexed | 2024-03-10T20:26:03Z |
publishDate | 2020-04-01 |
publisher | MDPI AG |
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series | Foods |
spelling | doaj.art-5495632c1b26465281e1dcde9fa741082023-11-19T21:48:28ZengMDPI AGFoods2304-81582020-04-019450510.3390/foods9040505Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate AnalysisQi Zhou0Guijie Li1Zhu Ou-Yang2Xin Yi3Linhua Huang4Hua Wang5Citrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaAn efficient and practical method for identifying mandarin juice over-blended into not from concentrate (NFC) orange juice was established. Juices were extracted from different cultivars of sweet orange and mandarin fruits. After being pasteurized, the volatile organic compounds (VOCs) in the juice samples were extracted using headspace solid-phase microextraction, and qualitatively and quantitatively analyzed using gas chromatography–mass spectrometry detection. Thirty-two VOCs contained in both the sweet orange juice and mandarin juice were used as variables, and the identification model for discriminating between the two varieties of juice was established by principal component analysis. Validation was applied by using common mandarin juices from Ponkan, Satsuma and Nanfengmiju cultivars blended at series of proportions into orange juices from Long-leaf, Olinda, and Hamlin cultivars. The model can visually identify a blending of mandarin juice at the volume fraction of 10% or above.https://www.mdpi.com/2304-8158/9/4/505mandarin juicenot from concentrate (NFC)principal component analysis (PCA)headspace solid-phase microextraction (HS-SPME) |
spellingShingle | Qi Zhou Guijie Li Zhu Ou-Yang Xin Yi Linhua Huang Hua Wang Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis Foods mandarin juice not from concentrate (NFC) principal component analysis (PCA) headspace solid-phase microextraction (HS-SPME) |
title | Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis |
title_full | Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis |
title_fullStr | Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis |
title_full_unstemmed | Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis |
title_short | Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis |
title_sort | volatile organic compounds profiles to determine authenticity of sweet orange juice using head space gas chromatography coupled with multivariate analysis |
topic | mandarin juice not from concentrate (NFC) principal component analysis (PCA) headspace solid-phase microextraction (HS-SPME) |
url | https://www.mdpi.com/2304-8158/9/4/505 |
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