Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis

An efficient and practical method for identifying mandarin juice over-blended into not from concentrate (NFC) orange juice was established. Juices were extracted from different cultivars of sweet orange and mandarin fruits. After being pasteurized, the volatile organic compounds (VOCs) in the juice...

Full description

Bibliographic Details
Main Authors: Qi Zhou, Guijie Li, Zhu Ou-Yang, Xin Yi, Linhua Huang, Hua Wang
Format: Article
Language:English
Published: MDPI AG 2020-04-01
Series:Foods
Subjects:
Online Access:https://www.mdpi.com/2304-8158/9/4/505
_version_ 1827718532123590656
author Qi Zhou
Guijie Li
Zhu Ou-Yang
Xin Yi
Linhua Huang
Hua Wang
author_facet Qi Zhou
Guijie Li
Zhu Ou-Yang
Xin Yi
Linhua Huang
Hua Wang
author_sort Qi Zhou
collection DOAJ
description An efficient and practical method for identifying mandarin juice over-blended into not from concentrate (NFC) orange juice was established. Juices were extracted from different cultivars of sweet orange and mandarin fruits. After being pasteurized, the volatile organic compounds (VOCs) in the juice samples were extracted using headspace solid-phase microextraction, and qualitatively and quantitatively analyzed using gas chromatography–mass spectrometry detection. Thirty-two VOCs contained in both the sweet orange juice and mandarin juice were used as variables, and the identification model for discriminating between the two varieties of juice was established by principal component analysis. Validation was applied by using common mandarin juices from Ponkan, Satsuma and Nanfengmiju cultivars blended at series of proportions into orange juices from Long-leaf, Olinda, and Hamlin cultivars. The model can visually identify a blending of mandarin juice at the volume fraction of 10% or above.
first_indexed 2024-03-10T20:26:03Z
format Article
id doaj.art-5495632c1b26465281e1dcde9fa74108
institution Directory Open Access Journal
issn 2304-8158
language English
last_indexed 2024-03-10T20:26:03Z
publishDate 2020-04-01
publisher MDPI AG
record_format Article
series Foods
spelling doaj.art-5495632c1b26465281e1dcde9fa741082023-11-19T21:48:28ZengMDPI AGFoods2304-81582020-04-019450510.3390/foods9040505Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate AnalysisQi Zhou0Guijie Li1Zhu Ou-Yang2Xin Yi3Linhua Huang4Hua Wang5Citrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaCitrus Research Institute, Southwest University, Chongqing 400712, ChinaAn efficient and practical method for identifying mandarin juice over-blended into not from concentrate (NFC) orange juice was established. Juices were extracted from different cultivars of sweet orange and mandarin fruits. After being pasteurized, the volatile organic compounds (VOCs) in the juice samples were extracted using headspace solid-phase microextraction, and qualitatively and quantitatively analyzed using gas chromatography–mass spectrometry detection. Thirty-two VOCs contained in both the sweet orange juice and mandarin juice were used as variables, and the identification model for discriminating between the two varieties of juice was established by principal component analysis. Validation was applied by using common mandarin juices from Ponkan, Satsuma and Nanfengmiju cultivars blended at series of proportions into orange juices from Long-leaf, Olinda, and Hamlin cultivars. The model can visually identify a blending of mandarin juice at the volume fraction of 10% or above.https://www.mdpi.com/2304-8158/9/4/505mandarin juicenot from concentrate (NFC)principal component analysis (PCA)headspace solid-phase microextraction (HS-SPME)
spellingShingle Qi Zhou
Guijie Li
Zhu Ou-Yang
Xin Yi
Linhua Huang
Hua Wang
Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis
Foods
mandarin juice
not from concentrate (NFC)
principal component analysis (PCA)
headspace solid-phase microextraction (HS-SPME)
title Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis
title_full Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis
title_fullStr Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis
title_full_unstemmed Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis
title_short Volatile Organic Compounds Profiles to Determine Authenticity of Sweet Orange Juice Using Head Space Gas Chromatography Coupled with Multivariate Analysis
title_sort volatile organic compounds profiles to determine authenticity of sweet orange juice using head space gas chromatography coupled with multivariate analysis
topic mandarin juice
not from concentrate (NFC)
principal component analysis (PCA)
headspace solid-phase microextraction (HS-SPME)
url https://www.mdpi.com/2304-8158/9/4/505
work_keys_str_mv AT qizhou volatileorganiccompoundsprofilestodetermineauthenticityofsweetorangejuiceusingheadspacegaschromatographycoupledwithmultivariateanalysis
AT guijieli volatileorganiccompoundsprofilestodetermineauthenticityofsweetorangejuiceusingheadspacegaschromatographycoupledwithmultivariateanalysis
AT zhuouyang volatileorganiccompoundsprofilestodetermineauthenticityofsweetorangejuiceusingheadspacegaschromatographycoupledwithmultivariateanalysis
AT xinyi volatileorganiccompoundsprofilestodetermineauthenticityofsweetorangejuiceusingheadspacegaschromatographycoupledwithmultivariateanalysis
AT linhuahuang volatileorganiccompoundsprofilestodetermineauthenticityofsweetorangejuiceusingheadspacegaschromatographycoupledwithmultivariateanalysis
AT huawang volatileorganiccompoundsprofilestodetermineauthenticityofsweetorangejuiceusingheadspacegaschromatographycoupledwithmultivariateanalysis