On the Hot-Plate Welding of Reactively Compatibilized Acrylic-Based Composites/Polyamide (PA)-12

Joining of dissimilar thermoplastics and their composites is a challenge for thermal welding techniques due to different melting points. Reactive welding with an auxiliary functional material can offer the clear opportunities to develop joining processes due to robustness to joining dissimilar therm...

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Main Authors: Henri Perrin, Masoud Bodaghi, Vincent Berthé, Sébastien Klein, Régis Vaudemont
Format: Article
Language:English
Published: MDPI AG 2023-01-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/16/2/691
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author Henri Perrin
Masoud Bodaghi
Vincent Berthé
Sébastien Klein
Régis Vaudemont
author_facet Henri Perrin
Masoud Bodaghi
Vincent Berthé
Sébastien Klein
Régis Vaudemont
author_sort Henri Perrin
collection DOAJ
description Joining of dissimilar thermoplastics and their composites is a challenge for thermal welding techniques due to different melting points. Reactive welding with an auxiliary functional material can offer the clear opportunities to develop joining processes due to robustness to joining dissimilar thermoplastic polymers and their composites. The current study employed reactive compatibilization to offer the possibility of joining an acrylic-based glass fiber composite to polyamide (PA)-12 by applying a hot-tool welding technique. For this purpose, composite plates are fabricated by a typical vacuum infusion and thin layer thermoplastic films are formed by a thermostamping of PA12 granules. Subsequently, the reactive welding of the interposed PA12 sheet and Elium<sup>®</sup>-GMA-Glass composite is conducted by hot-plate welding. A glycidyl methacrylate (GMA) as a compatibilizing agent is copolymerized with methyl methacrylate Elium<sup>®</sup> resin. During the hot-tool welding process of dissimilar thermoplastic material, GMA can react with the polyamide end groups. The heat distribution at the Elium<sup>®</sup> GMA/PA-12 interface is responsible for obtaining a strong joint. This study focuses on the functionality of the compatibilizer on the welding of acrylic-based composites with polyamide (PA)-12 while varying the assembly temperature. The flatwise tensile test proved the effectiveness of GMA on the interface bounding. The excellent bounding incompatible polymers Elium<sup>®</sup> resin (PMMA) and PA12 was achieved at 200 °C.
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spelling doaj.art-5532cfd15ce6411faa83e5dda42190462023-11-30T23:16:50ZengMDPI AGMaterials1996-19442023-01-0116269110.3390/ma16020691On the Hot-Plate Welding of Reactively Compatibilized Acrylic-Based Composites/Polyamide (PA)-12Henri Perrin0Masoud Bodaghi1Vincent Berthé2Sébastien Klein3Régis Vaudemont4Luxembourg Institute of Science and Technology (LIST), 5, rue Bommel, L-4940 Hautcharage, LuxembourgLuxembourg Institute of Science and Technology (LIST), 5, rue Bommel, L-4940 Hautcharage, LuxembourgLuxembourg Institute of Science and Technology (LIST), 5, rue Bommel, L-4940 Hautcharage, LuxembourgLuxembourg Institute of Science and Technology (LIST), 5, rue Bommel, L-4940 Hautcharage, LuxembourgLuxembourg Institute of Science and Technology (LIST), 5, rue Bommel, L-4940 Hautcharage, LuxembourgJoining of dissimilar thermoplastics and their composites is a challenge for thermal welding techniques due to different melting points. Reactive welding with an auxiliary functional material can offer the clear opportunities to develop joining processes due to robustness to joining dissimilar thermoplastic polymers and their composites. The current study employed reactive compatibilization to offer the possibility of joining an acrylic-based glass fiber composite to polyamide (PA)-12 by applying a hot-tool welding technique. For this purpose, composite plates are fabricated by a typical vacuum infusion and thin layer thermoplastic films are formed by a thermostamping of PA12 granules. Subsequently, the reactive welding of the interposed PA12 sheet and Elium<sup>®</sup>-GMA-Glass composite is conducted by hot-plate welding. A glycidyl methacrylate (GMA) as a compatibilizing agent is copolymerized with methyl methacrylate Elium<sup>®</sup> resin. During the hot-tool welding process of dissimilar thermoplastic material, GMA can react with the polyamide end groups. The heat distribution at the Elium<sup>®</sup> GMA/PA-12 interface is responsible for obtaining a strong joint. This study focuses on the functionality of the compatibilizer on the welding of acrylic-based composites with polyamide (PA)-12 while varying the assembly temperature. The flatwise tensile test proved the effectiveness of GMA on the interface bounding. The excellent bounding incompatible polymers Elium<sup>®</sup> resin (PMMA) and PA12 was achieved at 200 °C.https://www.mdpi.com/1996-1944/16/2/691fusion boundingElium<sup>®</sup>reactive welding
spellingShingle Henri Perrin
Masoud Bodaghi
Vincent Berthé
Sébastien Klein
Régis Vaudemont
On the Hot-Plate Welding of Reactively Compatibilized Acrylic-Based Composites/Polyamide (PA)-12
Materials
fusion bounding
Elium<sup>®</sup>
reactive welding
title On the Hot-Plate Welding of Reactively Compatibilized Acrylic-Based Composites/Polyamide (PA)-12
title_full On the Hot-Plate Welding of Reactively Compatibilized Acrylic-Based Composites/Polyamide (PA)-12
title_fullStr On the Hot-Plate Welding of Reactively Compatibilized Acrylic-Based Composites/Polyamide (PA)-12
title_full_unstemmed On the Hot-Plate Welding of Reactively Compatibilized Acrylic-Based Composites/Polyamide (PA)-12
title_short On the Hot-Plate Welding of Reactively Compatibilized Acrylic-Based Composites/Polyamide (PA)-12
title_sort on the hot plate welding of reactively compatibilized acrylic based composites polyamide pa 12
topic fusion bounding
Elium<sup>®</sup>
reactive welding
url https://www.mdpi.com/1996-1944/16/2/691
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