Detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopy

The use of electronic nose and attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) as rapid tools for detection of orange juice adulteration has been preliminarily investigated and compared. Freshly squeezed orange juices were tentatively adulterated with 100% concentrate...

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Main Authors: Fei Shen, Qifang Wu, Anxiang Su, Peian Tang, Xiaolong Shao, Bing Liu
Format: Article
Language:English
Published: Czech Academy of Agricultural Sciences 2016-06-01
Series:Czech Journal of Food Sciences
Subjects:
Online Access:https://cjfs.agriculturejournals.cz/artkey/cjf-201603-0006_detection-of-adulteration-in-freshly-squeezed-orange-juice-by-electronic-nose-and-infrared-spectroscopy.php
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author Fei Shen
Qifang Wu
Anxiang Su
Peian Tang
Xiaolong Shao
Bing Liu
author_facet Fei Shen
Qifang Wu
Anxiang Su
Peian Tang
Xiaolong Shao
Bing Liu
author_sort Fei Shen
collection DOAJ
description The use of electronic nose and attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) as rapid tools for detection of orange juice adulteration has been preliminarily investigated and compared. Freshly squeezed orange juices were tentatively adulterated with 100% concentrated orange juices at levels ranging from 0% to 30% (v/v). Then the E-nose response signals and FTIR spectra collected from samples were subjected to multivariate analysis by principal component analysis (PCA) and linear discriminant analysis (LDA). PCA indicated that authentic juices and adulterated ones could be approximately separated. For the classification of samples with different adulteration levels, the overall accuracy obtained by LDA in prediction was 91.7 and 87.5% for E-nose and ATR-FTIR, respectively. Gas chromatography-mass spectrometry (GC-MS) results verified that there existed an obvious holistic difference in flavour characteristics between fresh squeezed and concentrated juices. These results demonstrated that both E-nose and FTIR might be used as rapid screening techniques for the detection of this type of juice adulteration.
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spelling doaj.art-5667ea01d1784ff48e846289572a7c462023-02-23T03:28:19ZengCzech Academy of Agricultural SciencesCzech Journal of Food Sciences1212-18001805-93172016-06-0134322423210.17221/303/2015-CJFScjf-201603-0006Detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopyFei Shen0Qifang Wu1Anxiang Su2Peian Tang3Xiaolong Shao4Bing Liu5College of Food Science and Engineering, Nanjing University of Finance and Economics, Nanjing, P.R. ChinaCollege of Food Science and Engineering, Nanjing University of Finance and Economics, Nanjing, P.R. ChinaCollege of Food Science and Engineering, Nanjing University of Finance and Economics, Nanjing, P.R. ChinaCollege of Food Science and Engineering, Nanjing University of Finance and Economics, Nanjing, P.R. ChinaCollege of Food Science and Engineering, Nanjing University of Finance and Economics, Nanjing, P.R. ChinaCollege of Food Science and Engineering, Nanjing University of Finance and Economics, Nanjing, P.R. ChinaThe use of electronic nose and attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) as rapid tools for detection of orange juice adulteration has been preliminarily investigated and compared. Freshly squeezed orange juices were tentatively adulterated with 100% concentrated orange juices at levels ranging from 0% to 30% (v/v). Then the E-nose response signals and FTIR spectra collected from samples were subjected to multivariate analysis by principal component analysis (PCA) and linear discriminant analysis (LDA). PCA indicated that authentic juices and adulterated ones could be approximately separated. For the classification of samples with different adulteration levels, the overall accuracy obtained by LDA in prediction was 91.7 and 87.5% for E-nose and ATR-FTIR, respectively. Gas chromatography-mass spectrometry (GC-MS) results verified that there existed an obvious holistic difference in flavour characteristics between fresh squeezed and concentrated juices. These results demonstrated that both E-nose and FTIR might be used as rapid screening techniques for the detection of this type of juice adulteration.https://cjfs.agriculturejournals.cz/artkey/cjf-201603-0006_detection-of-adulteration-in-freshly-squeezed-orange-juice-by-electronic-nose-and-infrared-spectroscopy.phpchemometricsdiscriminationspectral analysisvolatile compounds
spellingShingle Fei Shen
Qifang Wu
Anxiang Su
Peian Tang
Xiaolong Shao
Bing Liu
Detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopy
Czech Journal of Food Sciences
chemometrics
discrimination
spectral analysis
volatile compounds
title Detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopy
title_full Detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopy
title_fullStr Detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopy
title_full_unstemmed Detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopy
title_short Detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopy
title_sort detection of adulteration in freshly squeezed orange juice by electronic nose and infrared spectroscopy
topic chemometrics
discrimination
spectral analysis
volatile compounds
url https://cjfs.agriculturejournals.cz/artkey/cjf-201603-0006_detection-of-adulteration-in-freshly-squeezed-orange-juice-by-electronic-nose-and-infrared-spectroscopy.php
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AT qifangwu detectionofadulterationinfreshlysqueezedorangejuicebyelectronicnoseandinfraredspectroscopy
AT anxiangsu detectionofadulterationinfreshlysqueezedorangejuicebyelectronicnoseandinfraredspectroscopy
AT peiantang detectionofadulterationinfreshlysqueezedorangejuicebyelectronicnoseandinfraredspectroscopy
AT xiaolongshao detectionofadulterationinfreshlysqueezedorangejuicebyelectronicnoseandinfraredspectroscopy
AT bingliu detectionofadulterationinfreshlysqueezedorangejuicebyelectronicnoseandinfraredspectroscopy